• Korean Journal of Food Science and Technology
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• v.17 no.2
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• pp.128-130
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• 1985

Solutions of 4.8 and 12% oxalic and 85% phosphoric acid were used for degumming of crude rice bran oil. 96.6% of total phosphatides was removed by degumming with either 2ml of 85% phosphoric acid or 20ml of 4% oxalic acid when added to 1kg of crude rice bran oil. Yields after degumming with oxalic and phosphoric acids were 63.6% and 61.0%, respectively.

• Journal of the Korean Society of Clothing and Textiles
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• v.27 no.5
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• pp.517-523
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• 2003

We studied the physical properties of silk fabrics after degumming, the dyeability and the color fastness of silk fabrics after degumming and sericin fixing. As the sericin was removed from silk fabrics, the rate of weight loss increased and both the abrasion resistance and the drape coefficient decreased. This means that the amount of the sericin remained in silk fabrics significantly affects the physical properties of silk fabrics. On the surface and the cross-section of silk fabrics, the silk fibers enclosed by the sericin seemed to be in a lump shape. Each fibroin strand, however, got scattered, as the process of degumming went through. The dyeability of silk fabrics degummed decreased at between 20$^{\circ}C$∼80$^{\circ}C$ the dyeing temperature, on the other hand, it significantly increased over 80$^{\circ}C$. The dyeability of the sericin-fixed silk fabrics was lower than that of the non-serin-fixed silk fabrics, to a little extent. The colorfastness of crocking in the dyed-silk fabrics was a little low and that of the sweat was much lower in a basic sweat. Especially, the colorfastness of the partially degummed silk fabrics was low, because the sericin was not stable in the condition of sweat. Therefore, the process of sericin fixing is essentially required, for the partially degummed silk fabrics and the process of degumming itself.

• International Journal of Industrial Entomology and Biomaterials
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• v.25 no.2
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• pp.205-208
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• 2012

Antheraea pernyi silkworm is a well known wild silkworm to produce a valuable silk fiber. A. pernyi silkworm was reared in Korean oak field and examined the cocoon characteristics, such as cocoon weight, cocoon shell weight, and percentage of cocoon shell weight. Degumming loss was also measured after alkali degumming process. A. pernyi silkworm spins tawny color cocoon in oval shape. Cocoon shell weight of A. pernyi silkworm, 0.78 g, was heavier than that of B. mori silkworm, 0.51 to 0.63 g. Cocoon shell percentage of A. pernyi silkworm, 32.8%, was higher than that of B. mori silkworm, 23.4 to 25.2%. Degumming loss percentage of A. pernyi silkworm, 17.1%, was lower than that of B. mori silkworm, 25.0%. SEM showed that the surface of the cocoon filament was coarse and oriented with longitudinal direction.

• Journal of Sericultural and Entomological Science
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• v.8
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• pp.63-67
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• 1968

The aim of this treatise was to find out the factors related to the weight of a have in the original silkworm. The results obtained are as follows: 1. There is no relationship between the degumming rate and cocoon layer rate, but there is related with the weight of cocoon only in chinese strain. 2. There is no difference among the strains, but considerably differente in degumming rate among the species. 3. The degumming rate of female is higher than that of male.

• Textile Coloration and Finishing
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• v.18 no.2 s.87
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• pp.31-38
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• 2006

Silk fabrics are very popular and widely used because of their elegant appearance. However, silk fabrics generally have easy wrinkle, and do not stretch and deform permanently after machine washing. Then the stretched properties of silk fabrics are important for the application of industrial textile materials such as formal and sports wear. Thus, this research surveys the covering, weaving and degumming conditions for stretched silk fabrics. As a result, yarn breaking stress was reduced with increasing spindle speed, and the yarn twists were optimized under the covering condition of polyurethane/silk with PVA pretreatment. In addition, the shrinkage of the silk fabrics treated with star degumming process was reduced by continuous NaOH degumming process. The fabrics showed the fabric physical properties with optimum stretched properties and evenness surfaces.

• Journal of Sericultural and Entomological Science
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• v.35 no.2
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• pp.114-119
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• 1993

The weight loss for the mixture(raw-silk/PET) was tested to investigate the effects of weight loss accelerator on the degumming and weight loss. The degumming loss of raw-silk was decreased while the weight loss polyester(PET) was increased depending on the increase of accelerator concentration. The difference of the weight loss was not significant in raw-silk but the weight loss of PET was increased with the increase of the alkali concentration. The proper degumming of raw-silk was obtained and simultaneously the weight loss of PET was high for the raw-silk/PET "A" and "B" type. The proper degumming of raw-silk was obtained but the weight loss of PET was low for the raw-silk/PET "D" and "E" type. It showed that the typical degumming curve in raw-silk part and the weight loss of PET was increased depending on the treatment time in the weight loss for the fabric composed of raw-silk and PET.

• Journal of Sericultural and Entomological Science
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• v.36 no.1
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• pp.44-52
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• 1994

Degumming with enzyme Degummase can be a viable alternative to the existing methods of degumming. Degumming, carried out with the conventional method of Marseille's soap 25%(owf) for 1.5h at boil gives a weight loss of about 24%. On Comparison, degumming with 10 enzyme at 5$0^{\circ}C$ for 60 min gives a weight loss of about 22%. Treatment with enzyme requires a much lower temperature and also the treatment time is shorter than the conventional process. Processing of silk at these conditions is likely to retain the lustre and softness of silk. To economise on the quantity of enzyme, conditions were optimised for a pad-store process. An enzyme concentration of 0.5% at 5$0^{\circ}C$ for a time period of 5~6h resulted in a weight loss of 22%. Though the concentration of the enzyme used was 20 times less than that used for long liquor method there was some strength loss. At 5$0^{\circ}C$ treatments carried out for 7~8 h resulted in some degradation. Strength loss occurs because enzyme in the absence of any stirring keeps acting at the place where it is deposited. Effect of temperature was more pronounced than time in degrading silk.

• Textile Coloration and Finishing
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• v.21 no.6
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• pp.56-63
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• 2009

In this study we have evaluated the separation characteristics and concentration of sericin using tubular type ultrafiltration membrane in silk degumming solution that extracted from electrolytic reduction water process. Ultrafiltration membranes have used in sericin separation performance and the separation characteristics of membrane satisfied typical Hagen-Poiseuille equation. It had the increase of flux according to the increase of feed pressure and temperature in occasion of pure water flux. And also the flux and solute rejection had about $25{\sim}60{\ell}/m^2{\cdot}h$ and more than 95% in sericin feed solution with concentration 1.00~1.89% at feed pressure force of $3{\sim}8kgf/cm^2$ respectively. In addition, the separation performance of tubular type ultrafiltration membrane for silk degumming solution was very steady-state with long experiment time.

• Journal of Sericultural and Entomological Science
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• v.18 no.1
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• pp.27-39
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• 1976

In this study several kinds of spun silk yarn-synthetic filament compounded yarn was manufactured, and several fabrics woven from above mentioned silk compound yarn for evaluation of serviceability as clothing materials. The following results were obtained: 1. Degumming agents are in the order of sodium silicate, sodium hydroxide, sodium carbornate, soap and water. 2. When the concentration of sodium hydroxide is exceeded 3%, degradation of floss silk property is resulted because of excessive dissolving out of silk protein. 3. Degumming effect is much improved by concentration of degumming agent and less by its treating time. 4. Simultaneous application of more the 2 kinds of degumming agent is desirable for improvement of floss silk. 5. Application of natural organic acid brings very good results in keeping original scooping and color of the silk. 6. Load and elongation it increased by compound with synthetic filament yarn. 7. Even the evenness of compound yarn is largely dependent on the quality of floss silk and extent of degumming, the C.V.% of silk compound yarn in the experiment was 8-12%. 8. Single bath dyeing technique was impossible for their cloth, and dyeing was performed in 2 bath system separately for silk and synthetic fiber. 9. Shrinkage ratio due to the dyeing of fabric was 23% in case of polyester and spun silk fabric. 10. The final woven cloth can be applicable to (a) Blouse in care of thin cloth (compound silk fabric) (b) Korean costume for women in case of thick cloth. (compound hand spun silk fabric)

• Journal of the Korean Society of Food Science and Nutrition
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• v.20 no.3
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• pp.220-224
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• 1991

Six reagents (water, citric acid, phosphoric acid, oxalic acid, acetic anhydride and maleic anhydride) were evaluated for their effectiveness is degumming rice bran oil. All chemical reagents tested were found to be significantly more effective than water in removing phosphatides from crude rice bran oil. Especially acetic anhydride and phosphoric acid were effective in reducing phosphorous levels (92.5% and 93.3% removeal, respectively). Nonhydratable phospholipids, lysophosphatidyl choline, were removed more effectively by the chemical reagents than by the water degumming. The major phospholipid(PL) components were phophatidyl choline. Oleic, linolieic and palmitic acids were the major fatty acids of PL in rice bran acetone insolubles(AI). The AI recovered by acetic anhydride degumming produced the most stable emulsions. However, the AI obtained from phophoric acid or oxalic acid treatments had very poor emulsifying properties.