• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2003년도 봄 학술발표회 논문집
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• pp.277-280
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• 2003

Material, mix proportion, curing condition, temperature, humidity and wind velocity have an influence on drying shrinkage of concrete. In this paper, to evaluate the effect of curing condition at early age on the drying shrinkage of concrete was investigated varying curing age for different binder. The principal conclusions from this research were as follows: 1) In case of 14 days of water curing, the drying shrinkage of concrete is smaller than 7 days of water curing, independence of type of binder. 2) In case of 4 days of water curing, the ratio of increase of drying shrinkage of concrete using fly-ash and slag powder is more remarkable than using portland cement alone, comparing the drying shrinkage of 7 days of water curing.

• 한국산업융합학회 논문집
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• 제13권2호
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• pp.99-106
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• 2010

The effects of additive and shrinkage reducing agent on the drying and autogenous shrinkage of high strength concrete are investigated in this study. As results, when the ratio of W/B(low water to binder ratio) increase, the compressive strength is decreased. Comparing with PC(portland cement) concrete, the strength is 2.8%, 3.2% and 3.8% lower respectively than that of PC when concrete mixing ratio is 0.2%, 0.3% and 0.4% in 28 days curing. Drying shrinkage strain of PC concrete showed $-650{\times}10^{-6}$ in 91 days curing. When SR(shrinkage reducing agent) of 0.2%, 0.3% and 0.4% is mixed, the drying shrinkage strains are 21%, 34% and 41% lower than those of PC in 91 days curing. Autogenous shrinkage strain of PC concrete appeared $-480{\times}10^{-6}$ in 56 days curing. When SR of 0.2%, 0.3% and 0.4% is mixed, the autogenous drying shrinkage strain are 12.5%, 19.8% and 33.3% lower than those of PC in 56 days curing. In cases of using the mineral and shrinkage agent or only using a shrinkage reducing agent also appeared same reducing effects for drying shrinkage and autogenous shrinkage.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2005년도 추계 학술발표회 제17권2호
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• pp.647-650
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• 2005

This paper is to investigate the shrinkage properties of ultra high strength concrete(UHSC) incorporating $5\%$ of expansive additives(EA) along with $1\%$ of shrinkage reducing agent(SRA). UHSC subjected to steam curing and incorporated with steel fiber exhibited higher compressive strength than control UHSC by as much as50MPa at 7days, while at 28days, noticeable change in compressive strength was not observed between UHSC mixtures. Control UHSC subjected to steam curing had a $922{\times}10^6$ of autogenous shrinkage strain value, which was 6.7 times of drying shrinkage strain value at 42 days. The combination of EA and SRA resulted in a decrease in autogenous shrinkage by as much as half of control mixture. Steam curing contributed to the reduction of autogenous shrinkage by as much as $11\%$ compared with that of standard curing.

• 대한치과기공학회지
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• 제29권2호
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• pp.9-15
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• 2007

As the development of nanotechnology, the use of composite resins which containing nanofillers becomes popular. The purpose of this study was to test the degree of polymerization of nanofillercontaining composite resins. For the study, three different nanofiller-containing composite resins and two different light-curing units were used. To evaluate the degree of polymerization, the maximum polymerization shrinkage taking place during the light curing, and the microhardness, after the light curing, were measured. As results, two light-curing units exhibited a similar emission spectrum to that of the included photoinitiator, camphorquinone. The only difference between the light-curing units were the width of the emission spectrum. Three different composite resins showed different microhardness values. Among them, Grandio showed the greatest microhardness value. However, there was less microhardness difference on the top and bottom surfaces due to the difference of the light-curing units. The maximum polymerization shrinkage values were also similar in the tested specimens regardless of the difference of the light-curing units. However, Grandio showed the least polymerization shrinkage. According to the manufacturers' data, Grandio showed the highest filler content(vol%).

• Restorative Dentistry and Endodontics
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• 제26권4호
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• pp.316-325
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• 2001

The purpose of this study was to evaluate the effect of adhesive curing timing on the direction of polymerization shrinkage of light-curing composite resin. In this study, the curing times of adhesive and composite resin were measured by differential scanning calorimeter(DSC). 28 extracted human molars were embedded in clear resin and box-type cavities were prepared. Based on DSC data, the experimental teeth were divided into 4 groups. Group 1: no bond; Group 2: late curing; Group 3: Intermediate curing; Group 4: Early curing. After treating with adhesive, the buccal cavities were filled with Z-100 hybrid composite resin and the lingual ones were filled with AEliteflo flowable composite resin. The depressions at the surface were measured by surface profilometer, then the specimens were embedded in clear resin and sectioned. Impressions were obtained and used to get epoxy resin replicas. The epoxy replicas were gold-coated and observed under SEM. Average Maximum Gap(AMG), Gap Proportion(GP), Average Marginal Index(AMI) were used to compare the shrinkage gap of each group. The results were statistically analyzed using the Kruskal-Wallis One Way ANOVA, Student-Newman-Keuls method. The results of this study were as follows. 1. Average Maximum Gap, Gap Proportion, Average Marginal Index and depression at the surface or Z-100 hybride composite resin were smaller than those of AEliteflo flowable composite resin(P<0.05). 2. When the bonding between composite resin and tooth structure was strong, the shrinkage gap was small, and depression at the surface was deep(P<0.05). 3. In the well-bonded group, light-curing composite resin shrank toward bonded cavity wall, not toward light source. The result suggested that the direction of polymerization shrinkage was affected by the quality of bonding in the dentin-resin interface. The strong was the bonding between composite resin and tooth structure, the smaller was the gap and the deeper was the depression at the surface. Then the flow to compensate the polymerization shrinkage proceeded from surface to bonded cavity wall.

• Restorative Dentistry and Endodontics
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• 제28권4호
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• pp.326-333
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• 2003

Ormocer has organic-inorganic compound polymers. One of advantages of ormocer is reduced polymerization shrinkage. The purpose of this study was to compare the amount of contraction shrinkage of composite resins and ormocers. Additionally, the time of each material when there is no further change of contraction shrinkage was analysed. Four brands of composite resins (P-60. Surefil, Z-250 and Denfil) and two brands of ormocers (Definite and Admira) were used. 20 seconds, 40 seconds and 60 seconds of curing times were given. Contraction shrinkage of them were measured using a linometer for 80 seconds. The effect of material and curing time to contraction shrinkage at the time of 80 seconds was analysed by two-way ANOVA. The effect of time to contraction shrinkage was analysed by one-way ANOVA and the time when there was no further change of the contraction shrinkage was analysed. The results are as follows: 1. P-60, Definite, Z-250 and Denfil had no further change of contraction shrinkage from the time of 20 seconds, and Surefil and Admira had no further change of contraction shrinkage from the time of 10 seconds. 2. Statistical analysis revealed volumetric shrinkage varied among material (p<0,05). No significant difference of contraction shrinkage among different curing times was found, and there was no effect of interaction between materials and curing times to contraction shrinkage. 3. Definite and Admira showed the statistically same contraction shrinkage with those of Z-250 and P-60. which is higher than that of Surefil and lower than that of Denfil (p<0.05).

• International Journal of Concrete Structures and Materials
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• 제4권1호
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• pp.9-15
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• 2010

Silica fume is a common addition to high performance concrete mix designs. The use of silica fume in concrete leads to increased water demand. For this reason, Florida Department of Transportation (FDOT) allows only a 72-hour continuous moist cure process for concrete containing silica fume. Accelerated curing has been shown to be effective in producing high-performance characteristics at early ages in silica-fume concrete. However, the heat greatly increases the moisture loss from exposed surfaces, which may cause shrinkage problems. An experimental study was undertaken to determine the feasibility of steam curing of FDOT concrete with silica fume in order to reduce precast turnaround time. Various steam curing durations were utilized with full-scale precast prestressed pile specimens. The concrete compressive strength and shrinkage were determined for various durations of steam curing. Results indicate that steam cured silica fume concrete met all FDOT requirements for the 12, 18 and 24 hours of curing periods. No shrinkage cracking was observed in any samples up to one year age. It was recommended that FDOT allow the 12 hour steam curing for concrete with silica fume.

• 한국산학기술학회논문지
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• 제16권11호
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• pp.7910-7916
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• 2015

본 연구에서는 팽창재 및 수축저감제 사용량 변화에 따른 초고성능 콘크리트(UHPC)의 양생조건별 역학적 특성 및 자기수축 특성에 대해 검토하였다. 그 결과 양생조건에 따른 UHPC의 역학적 특성으로 $90^{\circ}C$ 증기양생을 한 시험체는 모두 190 MPa 이상의 압축강도를 나타냈고 $20^{\circ}C$ 수중양생을 한 경우에는 재령 91일에서 증기양생을 한 시험체와 동등한 수준으로 발현되었다. 인장강도는 $90^{\circ}C$ 증기양생의 경우 23.4 MPa의 높은 수준으로 나타났으며 $20^{\circ}C$에서는 다소 저하하였다. 자기 수축 특성으로 양생조건에 따른 최종 수축량의 변화는 나타나지 않았다. 팽창재 및 수축저감제 사용에 따른 UHPC의 압축강도는 $90^{\circ}C$ 증기양생을 한 경우 190 MPa 이상 발현하였다. 자기수축 특성은 팽창재와 수축저감제를 복합 사용한 경우 약 45% 정도 수축저감 효과가 있는 것으로 나타났고 양생조건에 따른 차이는 발생하지 않았다.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2004년도 춘계 학술발표회 제16권1호
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• pp.132-135
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• 2004

High-performance concrete (HPC) may be expected to differ from usual concrete with respect to shrinkage behavior, and it shows high autogenous shrinkage due to the use of very low water-binder ratio (w/b) and various admixtures. Therefore, in order to minimize the shrinkage stress and to ensure the service life of concrete structure, volumetric change of HPC should be understood. In this study, small prisms made of HPC with w/b of 0.32 and blast-furnace slag content of $0\%,\;30\%,\;and\;50\%$ were prepared to measure the volumetric changes such as autogenous shrinkage, drying shrinkage, and swelling under three different curing conditions. It was observed that the concrete cured. sealed condition showed only autogenous shrinkage while the concrete let to dry condition at temperature of $20^{\circ}C$ and relative humidity of $60\%$ during the test period showed both autogenous and drying shrinkage. Moreover, the concrete exposed to dry condition after 2-day water curing swelled and then started to shrink with age. The total shrinkage (autogenous+drying) of this concrete was smaller than that of the concrete cured dry condition, especially at early-age. Therefore, the early-age moisture curing is very effective to control or minimize the volumetric change and its induced stress of HPC.

• 한국건설순환자원학회논문집
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• 제6권4호
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• pp.127-133
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• 2012

본 연구에서는 양생온도가 혼화재 치환 고강도 모르타르의 자기수축에 미치는 영향에 대하여 실험적으로 고찰하였다. 혼화재료는 실리카흄, 고로슬래그, 플라이애시의 3종류로서 치환률은 10, 20, 30%의 3수준으로 하였고 양생온도는 5, 20 및 $35^{\circ}C$의 3수준으로 계획하였다. 연구결과 양생온도가 높아질수록 혼화재 치환률이 감소할수록 응결시간은 단축되는 것으로 나타났으며, 양생온도에 따른 자기수축의 경우 양생온도가 증가할수록 수화반응속도 증가에 의해 자기수축이 커지는 것으로 나타났다. 또한 SF나 BS를 사용한 경우 자기수축이 플레인보다 증가하는 것으로 나타났고, FA의 경우는 플레인과 큰차이가 없거나 약간 감소하는 경향을 보였다. 또한 적산온도에 의한 자기수축 평가결과 동일한 적산온도에서 양생온도별 자기수축량의 차이가 크게 나타나 온도민감도를 보다 정확하게 고려할 수 있는 방법이 요구되었다.