• Journal of Technologic Dentistry
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• v.9 no.1
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• pp.67-72
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• 1987

This experimental study presented the study on the dimensional changes of occuring for the denture curing methods. The method is as follows: 1. The master die was made of wax. 2. The Silicon Rubber Mold was made into the same 80 casts. 3. The 80 Wax Plate were made of using the Base Plate Wax. 4. Flasking, Wax-wash, & Resin-packing were performed by the general procedures. 5. The curing method is performed through the four curing methods. (A, B, C, D). Table 2 shows the dimensional change after a day. Table 3 shows the dimensional change after soaking for 30 days in water of the degree of 36 Centigrade. As a result, the A curing method is the most denture curing.

• Design & Manufacturing
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• v.16 no.2
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• pp.60-65
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• 2022

In the pultrusion process for the CFRP (Carbon fiber reinforced plastic) rectangular pipe, the drawing device is eseential which can continuously produces products and draws the carbon fiber tow. In addition, since the degree of cure changes depending on the temperature and the temperature ditribution of the curing mold changes depending on the pultrusion speed, the temperature distribution of the curing mold under certain conditions must be studied before processing. In this study, in the pultrusion process using a closed impregnation method, which has several advantages compared to the general pultrusion process using a open bath impregnation method, the drawing force required to pull the carbon fiber tows and the temperature distribution of the curing mold was analyzed to design the drawing device and the curing mold efficiently.

• Journal of the Korea Concrete Institute
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• v.14 no.2
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• pp.137-147
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• 2002

Maturity models involving curing temperature and curing ages have been widely used to predict concrete strength, which can accurately estimate concrete strength. However, they may not consider physical quantities such as the characteristics of hydrates and the capillary porosity of microstructures associated with strength development. In order to find out the effects of both factors on a strength increment, the hydration model and the estimation method of the amount of capillary porosity were established, and the compressive strength test of concrete nth various water/cement ratios was carried out considering two test parameters, curing temperature and curing age. In this study, by analyzing the experimental results, a strength estimation model for early-age concrete that can consider the microstructural characteristics such as hydrates and capillary porosity was proposed. Measured compressive strengths were compared with estimated strengths and good agreements were obtained. Consequently, the proposed strength model can estimate compressive strength of concrete with curing age and curing temperature within an acceptable error.

• Journal of the Korean Geotechnical Society
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• v.19 no.2
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• pp.7-14
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• 2003

A series of laboratory tests, which can show how different curing conditions influence an aging effect on clay, were carried out for the clay samples collected in the area of Kwangyang Bay and Mokpo. Clay samples were remolded and reconsolidated under three different curing temperatures (20, 50, and 80 degree Celsius) and low different curing durations (1, 7, 14, and 40 days). To find out an aging effect and geotechnical characteristics between undisturbed samples and reconsolidated samples, laboratory tests, consisting of uniaxial compression tests, CU triaxial test, and consolidation tests, were preformed. Results showed that the compression index ratio is very useful factor to indicate the aging effect of natural clays. Also geotechnical characteristics of clays reconsolidated at high temperature were very similar to those of undisturbed clays. Finally, curing temperature and curing duration influenced an aging effect on clays. The best curing condition was 80 degree Celsius and 27 days.

• Textile Coloration and Finishing
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• v.30 no.3
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• pp.180-189
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• 2018

To study the effect of stereoisomeric structures of curing agents on curing behaviors, thermal and mechanical properties of epoxy resins, DGEBA(diglycidyl ether of bisphenol A) epoxy resin and 3,3'- and 4,4'-DDS(diaminodiphenyl sulfone) curing agents were selected. The curing initiation temperature and activation energy of DGEBA/3,3'-DDS was lower than DGEBA/4,4'-DDS. DGEBA/3,3'-DDS has a faster curing rate and higher degree of cure than DGEBA/4,4'-DDS, suggesting that 3,3'-DDS has higher reactivity than 4,4'-DDS. Tensile strength and fracture toughness of DGEBA/3,3'-DDS was lower than those of DGEBA/4,4'-DDS, indicating that mechanical properties of the epoxy resin can be different only by the stereoisomeric difference in chemical structure of the curing agent.

• Korean Chemical Engineering Research
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• v.46 no.1
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• pp.200-204
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• 2008

The curing kinetics of diglycidyl ether of bisphenol F (DGEBF) with an asymmetric cycloaliphatic amine curing agent were examined by thermal analysis in both isothermal and dynamic curing conditions. From the residual curing of the samples partially cured in isothermal condition and from the dynamic curing with various heating rates, it was found that there exist two kinds of reactions such as at low temperature and at high temperature regions. It was thus also found that the cure parameters obtained from the isothermal curing kinetic model hardly estimate experimental results for a degree of cure larger than 0.6. The activation energies and frequency factors of these two kinds of reactions were obtained from the dynamic curing experiments with various heating rates. From the curing analysis, it was verified that the total cure kinetics for low degrees of cure is dominated by the cure reaction in the low temperature region.

• The Journal of the Korean dental association
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• v.51 no.1
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• pp.12-17
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• 2013

Curing methods for denial resin-based materials are limited because of the need to polymerize quickly in the oral cavity at an ambient temperature. At present, most dental restorative composites use a camphorquinone-amine complex initiation, visible light-cure, one-component systems. Clinically, it is important to try to optimize the degree of conversion of res in composites using proper manipulation and adequate light-curing techniques to ensure the best outcome.

• Proceedings of the Korea Concrete Institute Conference
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• 2004.11a
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• pp.501-504
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• 2004

This paper proposes degree of hydration based shrinkage prediction model of 40MPa HPC. This model shows degree of hydration which is defined as the ratio between the hydrated cement mass and the initial mass of cement is very closely related to shrinkage deformation. In this study, degree of hydration was determined by CEMHYD-3D program of NIST. Verification of the predicted degree of hydration is performed by comparison between test results of compressive strength and estimated one by CEMHYD-3D. Proposed model is determined by statistical nonlinear analysis using the program Origin of Origin Lab. Co. To get coefficients of the model, drying shrinkage tests of four specimen series were followed with basic material tests. Testes were performed in constant temperature /humidity chamber, with difference moisture curing ages to know initial curing time effect. Verification with another specimen, collected construction field of FCM bridge, was given in the same condition as pre-tested specimens. Finally, all test results were compared to propose degree of hydration based model and other code models; AASHTO, ACI, CEB-FIP, JSCE, etc.

• Journal of Environmental Science International
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• v.27 no.11
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• pp.1023-1028
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• 2018

Shape memory materials are widely used in high-tech industries. Although shape memory polymers have been developed, they have a disadvantage, only unidirectional resilience. Shape memory polymers with bi-directional recovery resilience have been actively studied. In this study, a bidirectional shape memory polyurethane was synthesized using poly(${\varepsilon}$-caprolactone) diol, methylene dicyclohexyl diisocyanate, and hydroxyethyl acrylate. The first physical curing occurred between hard segments and hydrogen bondings when the solution was dried. The second curing in acrylate groups was performed by UV exposure. A degree of curing was analyzed by infrared spectroscopy. The shape memory properties of 2 step-cured polyurethanes were investigated as a function of UV curing time.

• Design & Manufacturing
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• v.16 no.3
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• pp.9-15
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• 2022

In order to reduce the manufacturing costs of the glass lens, it is necessary to manufacture a lens using a UV curable resin or a thermosetting resin, which is a curable material, in order to replace a glass lens. In the case of forming a lens using a thermosetting material, it is necessary to form several lenses at once using the wafer-level lens manufacturing technologies due to the long curing time of the material. When a lens is manufactured using a curable material, an error in the shape of the lens due to the shrinkage of the material during the curing process is an important cause of defects. The major factors for these shape errors and deformations are the shrinkage and the change of mechanical properties in the process of changing from a liquid material during curing to a solid state after complete curing. Therefore, it is necessary to understand the curing process of the material and to examine the shrinkage rate and change of physical properties according to the degree cure. In addition, it is necessary to proceed with CAE for lens molding using these and to review problems in lens manufacturing in advance. In this study, the viscoelastic properties of the material were measured during the curing process using a rheometer. Using the results, Rheological investigation of cure kinetics was performed. At the same time, The shrinkage of the material was measured and simple mathematical models were created. And using the results, the molding process of a single lens was analyzed using Comsol, a commercial S/W. In addition, the experiment was conducted to compare and verify the CAE results. As a result, it was confirmed that the shrinkage rate of the material had a great influence on the shape precision of the final product.