• 대한치과보철학회지
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• 제36권5호
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• pp.772-785
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• 1998

This study was undertaken to clarify the microstructure of the different IPS Empress ingots by etching and to observe the change of leucite crystal structure according to subsequent heat treatment and the crystal distribution according to sprue types(${\phi}2.8mm$, single sprue; ${\phi}1.8mm$, double sprue) by scanning electron microscopy. IPS Empress T1, O1 ingots used for staining technique, and Dentin(A2) ingots used for layering technique were selected for this study. To observe the microstructures of these ingots before pressing, the specimens were prepared in splinters($3{\times}3{\times}3mm$) taken from the original ingots. And to estimate crystal distribution and microstructural change by sprue type and subsequent heat treatment. the specimens($3{\times}3{\times}3mm$) were heat-pressed through the two types of sprues with different diameters and numbers, and all specimens were fired according to the recommended firing schedule. The observed surface was ground with waterproof papers($#800{\sim}#1800$) on the grind polisher and was cleaned ultrasonically. All specimen were etched with 0.5% hydrofluoric acid. After etching, the surface was treated by ion sputter coating for SEM observation at an accelerating voltage of 20kV. In all specimens, the central area of ground surface was observed because there was less difference in microstructure between the peripheral area and the central area. The results were as follows ; 1. In the microstructure according to the ingot type, there was a wide difference between the staining (T1,O1) and layering(Dentin A2) ingots, but there was not a considerable difference between the T1 ingot and the O1 ingot for staining technique. 2. In all specimens, the crystal dispersion of IPS Empress ceramic using double sprue was significantly more scattered than that of IPS Empress ceramic using single sprue. The degree of scattering was strongest in the Dentin(A2) specimen and weakest in the O1 ingot. 3. In the microstructural change according to the subsequent heat treatment, all of ingots had some microcracks in the inside of the leucite crystal and the glass matrix after pressing. The inner splinters of the leucite crystal became smaller, and more microcracks occurred in the glass matrix due to increasing heat treatment times. 4. The size of leucite crystals varied from $1{\mu}m\;to\;5{\mu}m$. The mean size of mature crystals was about $5{\mu}m$. The form of the crystal was similar to a circle when it was smaller and similar to an ellipse when it was larger.

• Journal of the Optical Society of Korea
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• 제2권2호
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• pp.54-57
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• 1998

A noncollinear-phase-matching cone of second harmonic generation(SHG) was observed in a LiNbO3 crystal doped with l mol% MgO. Birefringence refractive indices can be accurately evaluated by analysing the temperature phase matching characteristic for SHG combined with the measurement of the half cone angle. The electro-optic coefficient can also be determined form the observed change of the half cone angle when a DC electric field is applied along the optic axis.

• 전자공학회논문지D
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• 제34D권4호
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• pp.54-61
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• 1997

In this paper, a new holographic display system that can in real-time reconstruct the complex hologram without the bias and the conjugate image, which is obtained form the modified triangular interferometer, is presented. The proposed system is made of adding liquid crystal displays(LCDs), a $\lambda$/2 wave plate, and a polarizing beam splitter to the conventional mach-zehnder interferontric configuration. We demonstrate through theoretical analysis and experiment that real-time image reconstruction from the complex hologram is possible using the proposed system.

• 한국염색가공학회지
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• 제3권4호
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• pp.17-21
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• 1991

A rigid polymer, cellulose triacetate (CTA) dissolved in a combination of trifluoroacetic acid (TFA) and methylene chloride (MC) solution are liguid crystalline above a certain concentration. A flexible polymer, polyethylene terephthalate (PET) also dissolves in TFA/MC, but does not form liguid crystal phase. Ternary solutions, CTA/PET/TFA-MC which CTA and PET were mixed in a same solvent TFA/MC (6/4 : v/v) showed phase separation and mesophase formation.

• 약학회지
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• 제12권3_4호
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• pp.41-49
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• 1968

The optimum reaction conditions for the preparation of the precipitated calcium carbonate of an average particle size of 0.05.mu. in diameter was set in which the Box-Wilson Plan was applied. The reaction conditions are as follows; 1) concentration of milk of lime; 6.56% w/w 2) temperature; 14.24.deg. C #) velocity of carbon dioxide introducing; 1.95l/min. The crystal form was found that of calcite in X-ray diffraction analysis. The particle size was determined by the sedimentation volume measurement. The shape was identified by the elctron micro-diffraction pattern and the electron microscopic photographs.

• 한국정보디스플레이학회:학술대회논문집
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• 한국정보디스플레이학회 2007년도 7th International Meeting on Information Display 제7권1호
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• pp.911-914
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• 2007

We developed the laser annealing system using green laser of 261W(5kHz) and 75.5mJ/pulse(2kHz). We confirmed that this system makes it possible to form two kinds(large or uniformed grain) of poly-Si by changing its polarized directions. By using ${\mu}-crystal-Si$ as irradiated films, grain size uniformity is better than that using a-Si.

• 대한전기학회논문지
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• 제35권1호
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• pp.1-7
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• 1986

The GaAs bulk single crystals are grown by the Horizontal Bridgman method. During the growth, one of the problems in Bridgman method is the boat wetting between GaAs molten and silica boat. This boat wetting may result in another nucleation to form twin crystals. In this study, We find that the optimal size for sand blasting is 320 mesh. Backfilling the ampoule with argon gas during the vaccum bake-out decreaes the boat wetting. The reaction mechanism of Ga with quartz to produce suboxide, Ga2O, and sillion is discussed.

• Bulletin of the Korean Chemical Society
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• 제11권3호
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• pp.245-248
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• 1990

A series of compounds were synthesized that contain varying number of mesogenic units, 4-n-butylazobenzene moiety, attached to the central benzene ring through ester bond. These compounds were subjected to thermal analysis on a differential scanning calorimeter (DSC) and also on a polarizing microscope. It was found from this study that the presence of mesogenic units in a multi-mesogenic compound does not guarantee for the compound to become mesomorphic and that the linear molecular shape is conducive to form a liquid crystalline phase.

• 한국염색가공학회지
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• 제14권6호
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• pp.335-341
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• 2002

The physical properties and the dyeability of the nylon S fibers Prepared by high speed spinning according to godet roller draw ratio form 1.1 to 1.6 were investigated. The strains of nylon 6 fibers were decreased against the increase of the godet roller draw ratio. The stresses of nylon 6 fibers were increased with the increase of the godet roller draw ratio. Birefringences, densities and crystallinities of the nylon 6 fibers were increased with the increase of godet roller draw ratio In DSC diagrams, the $\gamma$ form of crystal became dominant at higher godet roller draw ratio. The dye uptakes of C. 1. Acid Blue 113 on the fibers were decreased against the increase of godet roller draw ratio.

• Korean Chemical Engineering Research
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• 제52권1호
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• pp.75-80
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• 2014

The convective flow structures in the vapor phase on earth are shown to be single unicellular, indicating the solutally dominant convection is important. These findings reflect that the total molar fluxes show asymmetrical patterns in a viewpoint of interfacial distributions. With decreasing the gravitational level form $1g_0$ down to $1.0{\times}10^{-4}g_0$, the total molar fluxes decay first order exponentially. It is also found that the total molar fluxes decay first order exponentially with increasing the partial pressure of component B, PB (Torr) form 5 Torr up to 400 Torr. Under microgravity environments less than $1g_0$, a diffusive-convection mode is dominant and, results in much uniformity in front of the crystal regions in comparisons with a normal gravity acceleration of $1g_0$.