• 분석과학
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• 제24권3호
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• pp.200-211
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• 2011

본 연구에서는 저온농축열탈착법을 이용하여, 4가지 유기지방산 및 9가지 휘발성유기화합물을 포함하는 13가지 성분의 분석기법을 비교연구하였다. 저온농축열탈착법을 이용한 유기지방산의 분석기법을 평가하기 위해, 5가지 흡착소재 각각에 대해 5점 검량에 기초한 비교를 시도하였다. 그 결과, 유기지방산 및 휘발성 유기화합물에서 Carbopack X를 충진한 고체흡착관의 response factor (RF)가 가장 높은수준을 유지하면서, 유기지방산과 휘발성유기화합물의 동시분석에 가장 적합한 것으로 나타났다. 그러나 Tenax TA 단일소재를 제외하면, 조사에 이용한 대부분의 흡착제도 양호한 것으로 나타났다. 저온농축열 탈착법의 검정을 위한 임의의 방안으로 기체상 표준시료를 저온농축열탈착법과 알칼리흡수법으로 동시에 비교분석하였다. 그 결과, 유기지방산에서 저온농축열탈착법 대비 알칼리흡수법의 비율 (T/S비)이 0.46 (valeric acid)~0.71 (isovaleric acid)으로 나타나 저온농축열탈착법의 결과가 상대적으로 낮게 나타났다. 보다 안정적인 분석조건을 찾기 위한 연구를 추가적으로 지속한다면, 유기지방산의 분석법을 향상시키는 것이 가능할 것으로 사료된다.

• 소성∙가공
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• 제18권2호
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• pp.166-171
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• 2009

In this paper, a basic study on micro cutting process with SM20C at low temperature environment was performed. In macro cutting fields, the cryogenic cutting process has been applied to cut the refractory metal but, the serious problem may be generated in micro cutting fields by the cryogenic environment. However, if the proper low temperature is applied to micro cutting area, the cooling effect of cutting heat is expected. Such effect can make the reduction of tool wear and burr formation. For verifying this possibility, the micro cutting experiment at low temperature was performed and SEM images were analyzed.

• 한국초전도저온공학회:학술대회논문집
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• 한국초전도저온공학회 1999년도 제1회 학술대회논문집(KIASC 1st conference 99)
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• pp.34-38
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• 1999

An acoustic emission(AE) technique has been used to monitor and diagnose quenching phenomenon in racetrack shaped superconducting magnets at cryogenic environment of 4.2K. The ultimate goal is to ensure the safety and reliability of large superconducting magnet systems by being able to identity and locate the sources of quench in superconducting magnets. The characteristics of AE parameters have been analyzed by correlating with quench number, winding tension of superconducting coil and charge rate by transport current. It was found in this study stat there was good correlation between quench current and AE parameters. The source location of quenching in superconducting magnet was also discussed on the correlation between magnet voltage and AE energy.

• 한국대기환경학회지
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• 제13권5호
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• pp.355-360
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• 1997

The atmospheric concentration of dimethylsulfide (DMS), known as the predominant volatile organic. sulfur compound, is determined at subnanogram level by a combined application of non-cryogenic preconcentration method and gas chromatography with flame photometric detection (GC/FPD). The volatile DMS in air is preconcentrated using a trapping tube containing adsorbent like Molecular Sieve 5A (or gold-coated sands). The tube is then connected to the GC/FPD system via a six-way rotary valve, thermally desorbed at 40$0^{\circ}C$, separated on OV101 column, and detected by a flame photometric detector. The DMS peak elutes at about 2.5 mins and is integrated electronically. The analytical precision, if expressed in terms of relative standard error, is around 5%. The detection limit of our GC/FPD system is ca 1 ng of DMS. Details of our analytical system are presented.

• 한국기계기술학회지
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• 제20권6호
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• pp.865-871
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• 2018

The 3-way valve have been used as a valve for opening and closing the valve by the flow control in the pressure system of the cryogenic and high pressure environment. In this paper, numerical analysis and experimental study on fracture nipple of 3-way ultra high pressure valve applied to space launch vehicle was carried out. We have developed a 3-way valve numerical simulation modeler of cryogenic environment using commercial software ANSYS 18.2. As results of numerical analysis, optimum nipple condition was derived. In addition, a 3-way valve prototype was fabricated and the fracture test was performed and compared with the numerical analysis results.

• Composites Research
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• 제33권5호
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• pp.309-314
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• 2020

우주 발사체용 극저온 추진제 탱크 경량화를 위한 고분자복합재료의 적용은 방향성을 가지는 복합재의 특성으로 인해 기체 투과도 성능 규명이 선행되어야 한다. 이러한 특성은 탱크 안정성 및 탑재 연료량 산정과 같은 성능 및 경제성과 직결된 지표다. 본 연구에서는 구조해석을 통해 도출된 극저온 추진제 탱크의 구조에 대하여 2가지 두께에 대한 투과도를 실험적으로 평가하였으며, 나아가 극저온-상온 환경에 노출된 열충격 횟수에 따른 시편의 비가역적 특성에 대한 투과도 분석 결과를 포함한다. 연구에 사용된 복합재는 두께에 반비례하며 열충격 횟수에 비례하는 투과도 특성을 보였으며, 우주 발사체용 극저온 추진제 탱크 소재로 적절한 투과도 성능을 가지는 것을 검증하였다.

• 한국초전도ㆍ저온공학회논문지
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• 제20권4호
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• pp.11-15
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• 2018

Torque tubes in High Temperature Superconducting (HTS) motor transfer torque from superconducting field winding rotor to the room temperature shaft. It should have minimum heat conduction property for minimizing the load on cryo-refrigerator. Generally, these torque tubes are made with stainless steel material because of high strength, very low outgassing and low thermal contraction properties at cryogenic temperatures and vacuum conditions. With recent developments in composite materials, these torque tubes could be made of composites such as Kevlar and S-Glass, which have the required properties like high strength and low thermal conductivity at cryogenic temperatures, but with a reduced weight. Development and testing of torque tubes made of these composites for HTS motor are taken up at Bharat Heavy Electricals Limited (BHEL), Hyderabad in collaboration with Central Institute of Plastics and Engineering Technology (CIPET), Chennai and Indian Institute of Technology (IIT), Kharagpur. As these materials are subjected to vacuum, it is important to measure their outgassing rates under vacuum conditions before manufacturing prototype torque tubes. The present study focusses on the outgassing characteristics of Kevlar and S-Glass, using an Outgassing Measurement System (OMS), developed at IIT Kharagpur. The OMS facility works under vacuum environment, in which the test samples are exposed to vacuum conditions over a sufficient period of time. The outgassing measurements for the composite samples were obtained using pressure-rise technique. These studies are useful to quantify the outgassing rate of composite materials under vacuum conditions and to suggest them for manufacturing composite torque tubes used in HTS motors.

• Composites Research
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• 제19권4호
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• pp.23-30
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• 2006

극저온 추진제 탱크를 개발하는 과정에서 복합재와 알루미늄 라이너를 접합하기 위한 접착제의 선택은 탱크의 안전성과도 직결된 매우 중요한 문제이다. 따라서 적합한 극저온용 접착제를 선택하기 위해 3종류의 접착필름이 선정되었으며 극저온용으로 개발된 탄소섬유/에폭시와 라이너 재료로 사용되는 알루미늄으로 구성된 양면 겹치기 조인트 시편을 제작하였다. 제작된 시편을 극저온 환경챔버를 사용하여 상온과 $-150^{\circ}C$에서 인장실험을 수행하여 각 접착제의 접착강도를 비교하였으며 파손 특성을 분석하였다. 또한 양면 겹치기 조인트 시편의 각 구성재료의 온도에 따른 기계적 물성변화를 측정하였으며 이를 이용하여 ABAQUS를 통한 유한요소해석을 수행하여 양면 겹치기 조인트 시편의 인장시험결과를 분석하였다.

• 한국수소및신에너지학회논문집
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• 제33권5호
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• pp.534-540
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• 2022

Liquid hydrogen has the best storage capacity per unit mass and is economical among storage methods for using hydrogen as fuel. As the demand for hydrogen increases, the need to develop a storage and supply system of liquid hydrogen is emphasizing. In order to liquefy hydrogen, it is necessary to pre-cool it to a maximum inversion temperature of -253℃. The Gifford-McMahon (GM) refrigerator is the most reliable and commercialized refrigerator among small-capacity cryogenic refrigerators, which can extract high-efficiency hydrogen through liquefied hydrogen production and boil of gas re-liquefaction. Therefore, in this study, the optimal conditions for liquefying gas hydrogen were sought using the GM cryocooler. The process was simulated by PRO/II under various cooling capacities of the GM refrigerator. In addition, the flow rate of hydrogen was calculated by comparing with specific refrigerator capacity depending on the pressure and flow rate of a refrigerant medium, helium. Simulations were performed to investigate the optimal values of the liquefaction flow rate and compression pressure, which aim for the peak refrigeration effect. Based on this, a liquefaction system can be selected in consideration of the cycle configuration and the performance of the refrigerator.

• Journal of Astronomy and Space Sciences
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• 제13권2호
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• pp.94-104
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• 1996

The satellite experiences the launch environment such as vibration, acceleration, shock induced by rocket and the orbit environment such as high vacuum, no gravity, high temperature and cryogenic. Therefore, the satellite should be designed and manufactured to endure such environments. Also, special care must be taken on the assembly of parts and subsystem. Finally, we describe the environment test of microsatellite to ensure the reliable operation during launch period as well as in-orbit operation.