• Particle and aerosol research
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• v.16 no.4
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• pp.95-105
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• 2020

Vanadium Pentoxide (V2O5) has been emerged as alternative electrode materials for supercapacitors due to their low cost, natural abundance, and environmental friendliness. Graphene (GR) loaded with V2O5 can exhibit enhanced specific capacitance. In this study, we present three-dimensional (3D) crumpled graphene (CGR) decorated with V2O5. The V2O5-graphene composites were synthesized from a colloidal mixture of graphene oxide (GO) and Ammonium metavanadate (NH4VO3), via aerosol spray drying and post heat treatment process. The average size of composite was ranged from 1.82 to 4.6 ㎛. Morphology of the composite changed from a crumpled paper ball to spherical ball having relatively smooth surface as the content of V2O5 increased in the composites. The electrochemical performance of the V2O5-graphene composites was examined. The V2O5-graphene composite electrode showed the specific capacitance of 312 F/g. In addition, the device possessed acceptable cyclic stability, with 84% after 2000 cycles at 2 A/g. These outstanding properties are expected to make the composites prepared in this study as promising electrode materials for supercapacitor applications.

• Fashion & Textile Research Journal
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• v.4 no.4
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• pp.327-338
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• 2002

The analysis and examination of this study are focussed on the external deconstruction trend expressed in the works of Jean Paul Gaultier. The external deconstruction is a way of expression faithful to the literal meaning of 'deconstruction' and is the applied case of exposure, destruction, poverty, and decomposition as they are. The method and scope of this study are from 1980's to present, and the followings are the results of this examination focussed on the various literature of philosophy, aesthetics and literary criticism, and the domestic and foreign fashion journals. The exposure phenomena through the deconstruction expressed repeatedly in the works of Gaultier deconstructed the fixed idea of 'the inner wear should be worn inside the outer wear' and at the same time denied the dichotomical interpretation of the exposure and suppression, the traditional beauty and decadent beauty, the chastity and unchastity, the asceticism and sexuality, and obscured the notion of the inner wear and outer wear. The destructive deconstruction expressed in the works of Jean Paul Gaultier introduced the elements such as hippy, punk, and kitsch, slashed before making dresses, crumpled unseemly like wastepaper, or made dresses with textures like paper scraps, and through destroying textures, yielded shock effects and tension. Poverty, through borrowing from the outwardly poor-looking elements of design, i.e. the patch work, decolor, dye, fading, fringing, incompletion, and handmadeness, liberated dresses and their ornaments from the outside. The traditional dresses were dresses having certain forms with formative beauty, but Gaultier disassembled dresses and raised questions about the logic of dresses themselves.

• Journal of Surface Science and Engineering
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• v.55 no.6
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• pp.398-402
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• 2022

Vacuum Insulation Panel (VIP) is an high energy efficient insulation system that facilitate slim but high insulation performance, based on based on a porous core material evacuated and encapsulated in a multi-barrier envelope. Although VIP has been on the market for decades now, it wasn't until recently that efforts have been initiated to propose a standard on aging testing. One of the issues regarding VIP is its durability and aging due to pressure and moisture dependent increase of the initial low thermal conductivity with time. It is hard to visually determine at an early stage. Recently, a method of analyzing the damage on the a material surface by applying image processing technology has been widely used. These techniques provide fast and accurate data with a non-destructive way. In this study, the surface VIP images were analyzed using the Harris corner detection algorithm. As a result, 171,333 corner points in the normal packaging were detected, whereas 32,895 of the defective packaging, which were less than the normal packaging. were detected. These results are considered to provide meaningful information for the determination of VIP condition.

• Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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• 2007.04a
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• pp.257-263
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• 2007

본 논문은 내구성(durability) 및 내오염성(soiling resistance)이 매우 중요한 성질로 인식되는 유통지의 평가방법을 제안하는데 목적이 있다. 즉, 종이의 내구성 및 내오염성의 측정 및 평가에 있어서, 재현성 및 반복성이 우수하고 합리적인 측정방법 및 평가방법을 구축하는데 목적이 있다. 연구목적에 적합한 시료의 준비, 오염물의 조성, 실험장치 및 실험후의 타당한 평가방법 등에 대하여 선행 연구결과를 고찰하였다. 기존 방법의 수정과 새로운 장치의 제작 및 평가방법의 설정을 통해 재현성이 높은 평가방법을 정립하고자 하였다. 유통지의 내구성을 평가하는 방법으로는 습식, 내오염성, 건식 내오염성, 구김기공도, 내세탁성, 잉크 내마모도 등의 항목을 측정하여 개별항목으로 내구성을 가늠하거나, 몇가지항목에 각기 다른 가중치를 부여하여 구한 내구성 지수(durability index)의 개념으로 내구성을 평가하기도 한다. 본 논문에서는 내구성에 영향하는 요소로 강도적 성질요소(strength property value)와 내오염성 요소(artificial soiling value)로 구분하였다. 강도적 성질요소에서는 전통적으로 내구성과 관련이 깊은 것으로 인식되어 온 내절도(folding endurance), 인열강도(tearing resistance) 및 구김기공도(crumpled porosity)를 인쇄하기 전 용지상태에서 측정하여 4:4:2의 가중치를 주어 구하였다. 내오염성 요소는 국가별 기후특성에 따라 연평균 상대습도가 60% 이상인 경우 인쇄 시료를 대상으로하여 습식 내오염성, 건식 내오염성 및 내석검성을 평가한 후 6:3:1의 가중치를 주어 구하였다. 또한 연평균 60% 미만인 국가의 경우 3:6:1의 가중치를 부여하였다. 이렇게 구해진 강도적 성질요소와 내오염성 요소에 있어 강도적 성질요소는 궁극적으로 내오염성 요소에 영향하기 때문에 3:7의 비율로 가중치를 부여하여 최종적으로 내구성 지수를 구하였다. 이때의 점수가 60점 이상이면 내구성 용지로 정의하였다. 본 논문에서는 현장실험을 통하여 시제품을 제조하였다. 상기 설명된 방법으로 내구성 지수를 구한 결과, 일반 유통지 제조방법으로 제조한 경우 내구성 지수가 약 45점이었다. 반면, 새로 개발된 방법에 의한 고내구성용지(durability paper)의 경우 70점 이상을 나타내어 내구성이 향상되었음을 확인할 수 있었다.

• Particle and aerosol research
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• v.10 no.2
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• pp.53-59
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• 2014

Palladium (Pd) nanoparticles attached graphene (GR) composite was synthesized for an enhanced glucose biosensor. Aerosol spray pyrolysis (ASP) was employed to synthesize the GR-Pd composite using a colloidal mixture of graphene oxide (GO) and palladium chloride ($PdCl_2$) precursor. The effects of the weight ratio of the Pd/GR on the particle properties including the morphology and crystal structure were investigated. The morphology of GR-Pd composites was generally the shape of a crumpled paper ball, and the average composite size was about $1{\mu}m$. Pd nanoparticles less than 20 nm in diameter were deposited on GR sheets and the Pd nanoparticles showed clear crystallinity. The characteristic of the glucose biosensor fabricated with the as-prepared GR-Pd composite was tested through cyclic voltammetry measurements. The biosensor exhibited a high current flow as well as clear redox peaks, which resulted in a superior ability of the catalyst in terms of an electrochemical reaction. The highest sensitivity obtained from the amperometric response of the glucose biosensor was $14.4{\mu}A/mM{\cdot}cm^2$.

• Particle and aerosol research
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• v.14 no.3
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• pp.65-72
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• 2018

Core-shell structured $Fe_3O_4/graphene$ composites were synthesized by aerosol spray drying process from a colloidal mixture of graphene oxides and $Fe_3O_4$ nanoparticles. The structural and electrochemical performance of $Fe_3O_4/graphene$ were characterized by the field-emission scanning electron microscopy, X-ray diffraction, Raman spectroscopy, cyclic voltammetry, and galvanometric discharge-charge method. Core-shell structured $Fe_3O_4/GR$ composites were synthesized in different mass ratios of $Fe_3O_4$ and graphene oxide. The composite particles were around $3{\mu}m$ in size. $Fe_3O_4$ nanoparticles were encapsulated with a graphene. Morphology of the $Fe_3O_4/graphene$ composite particles changed from a spherical ball having a relatively smooth surface to a porous crumpled paper ball as the content of GO increased in the composites. The $Fe_3O_4/GR$ composite fabricated at the weight ratio of 1:4 ($Fe_3O_4:GO$) exhibited higher specific capacitance($203F\;g^{-1}$) and electrical conductivity than as-fabricated $Fe_3O_4/GR$ composite.

• Particle and aerosol research
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• v.15 no.4
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• pp.127-137
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• 2019

Recently, high electrochemical performance anode materials for lithium ion secondary batteries are of interest. Here, we present silicon-carbon-graphene (Si-C-GR) composites for high performance anode materials of lithium ion secondary battery (LIB). Aerosol process and heat-treatment were employed to prepare the Si-C-GR composites using a colloidal mixture of silicon, glucose, and graphene oxide precursor. The effects of the size of the silicon particles in Si-C-GR composites on the material properties including the morphology and crystal structure were investigated. Silicon particles ranged from 50 nm to 1 ㎛ in average diameter were employed while concentration of silicon, graphene oxide and glucose was fixed in the aerosol precursor. Morphology of as-fabricated Si-C-GR composites was generally the shape of a crumpled paper ball and the Si particles were well wrapped in carbon and graphene. The size range of composites was about from 2.2 to 2.9 ㎛. The composites including silicon particles larger than 200 nm in size exhibited higher performance as LIB anodes such as capacity and coulombic efficiency than silicon particles less than 100 nm, which were about 1500 mAh/g at 100 cycles in capacity and 99% in coulombic efficiency, respectively.

• Particle and aerosol research
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• v.12 no.4
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• pp.127-134
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• 2016

A multiwall carbon nanotube (MWCNT)/graphene (GR) composite was synthesized for an enhanced supercapacitor. Aerosol spray pyrolysis (ASP) was employed to synthesize the MWCNT/GR composites using a colloidal mixture of MWCNT and graphene oxide (GO). The effect of the weight ratio of the MWCNT/GO on the particle properties including the morphology and layered structure were investigated. The morphology of MWCNT/GR composites was generally the shape of a crumpled paper ball, and the average composite size was about $5{\mu}m$. MWCNT were uniformly dispersed in GR sheets and the MWCNT not only increase the basal spacing but also bridge the defects for electron transfer between GR sheets. Thus, it was increasing electrolyte/electrode contact area and facilitating transportation of electrolyte ion and electron in the electrode. Electrochemical data demonstrate that the MWCNT/GR (weight ratio=0.1) composite possesses a specific capacitance of 192 F/g at 0.1 A/g and good rate capability (88% capacity retention at 4 A/g) using two-electrode testing system.

• Conservation Science in Museum
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• v.14
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• pp.61-67
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• 2013

Lacquerware of Goryeo period was variously developed from the early 10th century to the 14th century and became lacquerware inlaid with mother-of-pearl which shows creativity with splendid heyday. For characteristics, splendid and close mother-of-pearl. Characteristic of decoration method is to use gold painting method, Tortoise shell and metal line. Drawing is done with gold dust and gold painting method decorating lacquerware are very splendid from an artistic and decorative aspect, but gold painting is easily lost. So, it's currently difficult to find in relics succeeded. Therefore, there are domestically insufficient studies on gold painting method in Goryeo period, so this researcher intended to observe gold painting of lacquerware excavated in Goryeo period through the microscope, investigate characteristics, mixture, etc. of gold dust and provide data of studies on the recovery of ancient technology. As the result, gold dust particle has various shapes such as irregular square, polygon and triangle under the size from 2 ㎛ to 20 ㎛. The end of gold dust is rolled and overlapped and irregular particle seems to be similar to the shape of crumpled paper. This research showed that gold dust used in gold painting of Goryeo period had used gold dust made by grinding gold leaf to gold painting.

• Journal of Conservation Science
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• v.37 no.6
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• pp.723-737
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• 2021

This study analyzed the composition and structure of materials with Buddhist paper scriptures excavated from architectural sites in 'Sum Tolgoi' of the 17^th century and carried out conservation treatment base on the result of the analysis. The scriptures were covered in dust and foreign sub stances, and were so crumpled that it was impossible to identify the form. The damage, loss, and discoloration have been identified. Buddhist scriptures written in Tibetan used indigo and ink sticks on paper as a result of UV-Vis analysis, and ink sticks as black character materials from scriptures written ancient Mongolian. SEM-EDS and Micro-XRF analyses revealed that the outlines were drawn with red lines using a mix of Minium (Pb₃O₄) and Cinnabar (HgS), or Cinnabar (HgS) alone, and the contents of the scriptures were written with silver paint. Silver chloride (AgCl) and Calcium (Ca) were identified in the silver paint component of the characters, while Calcium and Orpiment (As₂S₃) were identified in the yellow lines. Concerning the paper ground, Buddhist scriptures written in ancient Mongolian were characterized by herbal plant fiber and bast fiber, and those written in Tibetan, by bast fiber. Radiocarbon dating indicates that the paper for the scriptures was produced between the 15^th and 17^th centuries. Conservation treatment of the scriptures was carried out based on the experiment on the production of pre-coated paper and how to coat that to prevent the second damage due to the deformation and fragility of the excavated paper. The scriptures were preserved and mounted, and a neutral box was made to identify the contents of the scriptures recorded on both sides after the treatment. This conservation treatment is the result of a study that applied new conservation treatment materials and methods according to the principle of conservation treatment reversibility.