• Korean Chemical Engineering Research
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• 제58권1호
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• pp.36-43
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• 2020

생분해성 금속인 마그네슘 합금 와이어를 이용하여 담관용 스텐트를 제작하였다. 생체 내에서 마그네슘 합금의 문제점인 빠른 분해 및 부식을 제어하기 위하여 마그네슘 합금 와이어를 생분해성 고분자인 polycaprolactone (PCL), poly(propylene carbonate) (PPC), poly(L-lactic acid) (PLLA), poly(D,L-lactide-co-glycolide) (PLGA) 등으로 코팅하였다. 표면분해가 이루어지는 고분자인 PPC의 경우는 전분해 거동을 보이는 다른 고분자들(PCL, PLLA, PLGA)에 비해 크랙이나 박리가 없어 가장 효율적으로 마그네슘 와이어의 분해 속도를 지연시켰다. 또한 생분해성 고분자 코팅이 마그네슘 합금 스텐트의 기계적 물성인 축 방향 힘에 미치는 영향에 대하여 조사하였다. 대부분의 생분해성 고분자(PCL, PLLA, PLGA)로 코팅된 스텐트는 코팅되지 않은 스텐트에 비해 축 방향의 힘이 증가하여 스텐트의 유연성을 감소시켰으나, PPC로 코팅된 스텐트는 코팅되지 않은 스텐트와 비슷한 축 방향의 힘을 나타내 스텐트의 유연성을 감소시키지 않았다. 이상의 결과로부터 PPC가 가장 효율적인 생분해성 고분자로 판단된다.

• 한국세라믹학회지
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• 제32권12호
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• pp.1357-1368
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• 1995

Nasigels of composition Na0.75Zr2PSi2O12 and Na3Zr2PSi2O12 have been synthesized by the sol-gel technique using metal alkoxide precursors. The monolithic dry gels of Na0.75Zr2PSi2O12 with no crack have been prepared by the control of the shrinkage rte, but gels of Na3Zr2PSi2O12 were impossible to prepare without cracking. The gels treated up to 80$0^{\circ}C$ led to the formtion of glass but the glasses were converted to the crystalline phases at above this temperature. Crystaline phases precipitated from the Na0.75Zr2PSi2O12 glass were NASICON-like phase, Na2Si2O5, and free Zirconia. Phase that precipitated from the Na3Zr2PSi2O12 was only rhombohedral NASICON. For Na0.75Zr2PSi2O12 gels, framework of PO4 tetrahedra and SiO4(PO4) tetrahedra formed at low temperature but changed to that of SiO4 and SiO4(PO4) tetrahedras as it were crystallized. In the case of Na3Zr2PSi2O12 gel, framework of isolated PO4 and SiO4 tetrahedras formed at low temperature but changed to SiO4(PO4) tetrahedra framework which usually formed in the NASICON crystal after crystallization at high temperature. The gels treated up to 80$0^{\circ}C$ contained the residual water. The ionic conduction was attributed to the motion of proton and Na+ ion at low (up to 150~20$0^{\circ}C$) and high temperatures, respectively. As the temperature of heat treatment increased, ionic conductivity gradaully increased with the extent of precipitation of crystalline phase.

• Structural Engineering and Mechanics
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• 제43권2호
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• pp.179-197
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• 2012

This study presents the findings of the structural health monitoring and the real time system identification of one of the first large scale building instrumentations in Turkey for earthquake safety. Within this context, a thorough review of steps in the instrumentation, monitoring is presented and seismic performance evaluation of structures using both nonlinear pushover and nonlinear dynamic time history analysis is carried out. The sensor locations are determined using the optimal sensor placement techniques used in NASA for on orbit modal identification of large space structures. System identification is carried out via the stochastic subspace technique. The results of the study show that under ambient vibrations, stocky buildings can be substantially stiffer than what is predicted by the finite element models due to the presence of a large number of partitioning walls. However, in a severe earthquake, it will not be safe to rely on this resistance due to the fact that once the partitioning walls crack, the bare frame contributes to the lateral stiffness of the building alone. Consequently, the periods obtained from system identification will be closer to those obtained from the FE analysis. A technique to control the validity of the proportional damping assumption is employed that checks the presence of phase difference in displacements of different stories obtained from band pass filtered records and it is confirmed that the "proportional damping assumption" is valid for this structure. Two different techniques are implemented for identifying the influence of the soil structure interaction. The first technique uses the transfer function between the roof and the basement in both directions. The second technique uses a pre-whitening filter on the data obtained from both the basement and the roof. Subsequently the impulse response function is computed from the scaled cross correlation between the input and the output. The overall results showed that the structure will satisfy the life safety performance level in a future earthquake but some soil structure interaction effects should be expected in the North South direction.

• 박물관보존과학
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• 제7권
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• pp.43-51
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• 2006

광주 신창동 저습지유적에서 다양한 목재유물과 더불어 목재표면에 옻칠이 된 칠기들이 다량으로 출토되었다. 칠기들은 목질부가 열화 되어 취약하며 칠층이 들떠있어 박락과 갈라짐의 발생우려가 높다. 따라서 진공 동결건조에 효과적인 PEG#4000 40%로 함침처리 하였고 동결건조의 종료온도를 0℃이하로 하였다. 동결건조 직후 목제와 칠기의 중량과 상대습도 60% 의 밀폐공간에서 방치 후 중량을 비교하였다. 그 결과 중량변화가 없었으므로 동결건조 중 종료 온도 조절로써 건조 후 목재함유수분조절과 대기 중 습도변화에 안정성을 확인하였다. 칠도막 분석결과 밑층에 흑색안료를 혼합하여 목재표면에 밑칠을 하고 칠층의 상부에 옻칠과 흑색안료를 혼합하여 3~4회 칠한 것과 검은 밑칠을 하지 않고 칠층에 옻칠과 흑색 안료를 혼합하여 3~4회 칠한 것으로 확인되었다.

• 소성∙가공
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• 제19권6호
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• pp.337-343
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• 2010

Current need of weight reduction in automotive part increases the application for high strength steel (HSS). The various types of high strength steels have been used to produce chassis part, control arms and trailing arms for weight reduction and increasing of fatigue durability such as dual phase steel (DP) and ferrite bainite steel (FB). But, DP and FB steels have proven to show inferiority in durability as well as press formability. Edge cracking occurred often in flange forming and hole expansion processes is the major failure encountered. This paper discussed the behavior of edge stretchability of high strength steel of DP and FB steels. Experimental works have been conducted to study the effect of punch clearance and burr direction on hole expansion ratio (HER). Also finite element simulation (FEM) has been preformed to clarify the mechanism of flange crack and support the experimental results on HER of DP and FB steels. It was simulated the whole process of blanking process following by hole expansion process and ductile fracture criterion named the modified Cockcroft-Latham model which was used to capture the fracture initiation. From the hole expansion tests and FEM simulation studies it was concluded that ferrite bainite steel showed better stretch-flangeability than dual phase steel. It was attributed to the lower work hardening rate of ferrite bainite steel than dual phase steel at the sheared edge.

• Journal of Welding and Joining
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• 제27권4호
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• pp.49-53
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• 2009

For Al 6k21-T4 alloy, linear laser welding produced the lower shear-tensile strength than the base metal. This study improved the shear-tensile strength by using the weaving laser at the optimized welding condition, i.e., 2mm weaving width and 25Hz frequency. The large weaving width increased the weld width, therefore improving the joint strength. For the specimen of low strength, the porosity was distributed continuously along the intersection between the plates and fusion line. However, for the optimized welding condition, large oval-shaped porosities were located only in the advancing track of the concave part. Regardless of the welding condition, solidification cracking was initiated at the intersection and propagated through small porosities in the weld part. furthermore, the concave part had more significant porosity in the weld and HAZ, respectively than the convex part. The continuity of porosities played a key role to determine the strength. And, the weaving width was an important parameter to control the strength.

• 콘크리트학회논문집
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• 제24권3호
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• pp.241-248
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• 2012

이 연구에서는, 철근콘크리트 기둥 실험체를 대상으로 기둥의 휨 위험 단면부에 국부적으로 강섬유 시멘트모르타르를 적용함으로서 기존 철근콘크리트 기둥에 비해 내진성능이 우수한 강섬유 모르타르 적용 철근콘크리트 복합기둥공법에 관해 제시하였다. 제시된 적용공법의 성능검증을 위하여 기존 철근콘크리트 기둥 1개 및 소성힌지구간에 국부적으로 강섬유 모르타르를 적용한 복합기둥 실험체 2개를 제작하여 일정 축하중 하에서 횡방향 반복하중을 받는 재하시험을 수행하였다. 콘크리트 및 강섬유 모르타르는 모두 현장타설되었다. 재하시험 결과 기존 철근콘크리트 기둥 실험체와 비교하여 강섬유 모르타르 적용 철근콘크리트 복합기둥 실험체의 경우 휨 및 전단 균열의 제어에 우수할 뿐만 아니라 기둥의 횡하중 내력 및 횡방향 변형 능력 향상에서도 우수한 것으로 평가되었다.

• 콘크리트학회논문집
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• 제23권3호
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• pp.385-392
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• 2011

이 연구에서는 기존 철근콘크리트 건물의 보-기둥 접합부 및 내진 성능의 개선을 위해 보-기둥 접합부 영역을 기존의 강판 및 FRP보강재(탄소섬유 쉬트, 매입형 탄소섬유봉)를 사용하여 보강한 후 내진 성능을 평가 하였다. 총 6개의 실험체를 제작하고 실험을 수행하여 내진 성능을 평가하였으며, 이 연구의 실험 결과를 근거로 다음과 같은 결론을 얻었다. 기존 철근콘크리트 보-기둥 접합부의 접합부 영역(LBCJ 시리즈)를 보강한 결과 초기 재하시 접합부 영역의 균열 억제 효과와 재하 전 과정을 통하여 보강재의 구속 효과로 인하여 균열 억제 효과가 커서 안정적인 파괴 형태 및 내력 향상 효과를 나타내었다. 기존 철근콘크리트 보-기둥 접합부의 내진 성능을 개선하기 위하여 철근콘크리트 보-기둥 접합부 FRP보강 기술 적용 실험체 LBCJ 시리즈는 표준실험체 LBCJC와 비교하여 최대 내력은 26~50% 증가하였다. 그리고 에너지 소산 능력은 변위 연성 4에서 13.0~14.4% 증가하였다.

• 전기전자학회논문지
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• 제21권4호
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• pp.404-407
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• 2017

에어로졸 증착 공정을 이용하여 ZnO, AZO 및 ITO 막을 증착하고 코팅막의 미세구조, 광학적 및 전기적 특성을 연구하였다. 상온에서 PET 기판 위에 약 400 nm의 두께를 가지는 ZnO, AZO 및 ITO 막을 성공적으로 제조할 수 있었으며 캐리어 가스 유량이 증가하면서 ZnO, AZO 및 ITO 막의 광학적 특성 및 전기적 특성이 향상되었다. 기계적인 유연 내구성 시험에 있어 ZnO 막은 5,000회의 굽힘에도 파괴가 발생하지 않은 반면 AZO 및 ITO 막은 5000회 굽힘 시험 후 막의 파괴가 발생하고 투과도 및 저항의 성능이 저하되었다. 결론적으로 AZO 및 ITO 막의 성능은 ZnO 막에 비하여 약간 열세이나, 입자크기 제어 및 공정 최적화를 통해 성능을 향상시킬 수 있을 것으로 판단된다.

• KIEAE Journal
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• 제10권5호
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• pp.115-121
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• 2010

Lime was the solidifier mostly used at the fields of construction and civil works in the past. however, the development of Portland cement remarkably reduced the use of it. Recently as the concernment on circumstances gets higher, lime wined attention again as an eco-friendly material and was used at earth-using construction. This study examined the physical and chemical capacity of lime complexes with lime capacity improved, and performed fundamental study on the way to concretize by mixing it with earth. As a result, lime complex pressure strength was lower than cement pressure strength but it showed the possibility that its strength was improved by W/B control. The measurement of XRD after paste formation confirmed a compound generated by the reaction of Ca2+ion and Si, Al, and Fe from pozzolan reaction. A earth wall experiment by using lime complexes and earth showed that the higher, WB or the lower the quantity of unit combined materials, the lower the pressure strength was. The maximum pressure strength was maximum 11MPa when the quantity of unit combined materials was 450. It is because the composed earth particles had a high content of micro powder less than silt, so a lot of combination are demanded to secure fluidity. As a result of peptization experiment, after hardening, the material was not dissolved, which informed of the possibility of use as an outer subsidiary material. If the material is hardened by mold formation method, natural hardening crack appears. Cast expresses smart surface quality and enables to design for multiple purpose. The result shows the possibility of construction of low-story structures by using earth wall made of lime complexes and earth.