• Title/Summary/Keyword: constituent

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이중복합 주조체의 제조에 미치는 구성 재질과 주조 조건의 영향 (Influences of Casting Conditions and Constituent Materials on the Production of Duo-castings)

  • 정재영
    • 한국주조공학회지
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    • 제38권1호
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    • pp.16-26
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    • 2018
  • In this study, the effects of the pouring temperature, preheating temperature, surface condition and fraction of the wear resistant part on the production of duo-castings were investigated using a high Cr white cast iron with excellent abrasion resistance and a low Cr alloy steel with good toughness. The constituent materials of the duo-castings were designed to have high hardness, fracture toughness and abrasive wear resistance for the replacement of high Mn alloy steels with low abrasive wear resistance. In particular, the amount of abrasive wear of 17% Cr white cast iron was about 1/20 of that of high Mn alloy steel. There was an intermediate area of about 3mm due to local melting at the bonding interface of the duo-castings. These intermediate regions were different from those of the constituent materials in chemical composition and microstructure. This region led to fracture within the wear resistant part rather than at the bonding interface in the bending strength test. The bending fracture strengths were 516-824 MPa, which were equivalent to the bending proof strength of high Mn steel. The effects of various casting conditions on the duo-cast behavior were studied by simple pouring of low Cr alloy steel melt, but the results proved practically impossible to manufacture duo-castings with a sound bonding interface. However, the external heating method was suitable for the production of duo-castings with a sound bonding interface.

Microstructural Characterization of Composite Electrode Materials in Solid Oxide Fuel Cells via Image Processing Analysis

  • Bae, Seung-Muk;Jung, Hwa-Young;Lee, Jong-Ho;Hwang, Jin-Ha
    • 한국세라믹학회지
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    • 제47권1호
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    • pp.86-91
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    • 2010
  • Among various fuel cells, solid oxide fuel cells (SOFCs) offer the highest energy efficiency, when taking into account the thermal recycling of waste heat at high temperature. However, the highest efficiency and lowest pollution for a SOFC can be achieved through the sophisticated control of its constituent components such as electrodes, electrolytes, interconnects and sealing materials. The electrochemical conversion efficiency of a SOFC is particularly dependent upon the performance of its electrode materials. The electrode materials should meet highly stringent requirements to optimize cell performance. In particular, both mass and charge transport should easily occur simultaneously through the electrode structure. Matter transport or charge transport is critically related to the configuration and spatial disposition of the three constituent phases of a composite electrode, which are the ionic conducting phase, electronic conducting phase, and the pores. The current work places special emphasis on the quantification of this complex microstructure of composite electrodes. Digitized images are exploited in order to obtain the quantitative microstructural information, i.e., the size distributions and interconnectivities of each constituent component. This work reports regarding zirconia-based composite electrodes.

실 단면 형상과 니트 구조 인자가 흡한속건 소재의 수분이동 특성에 미치는 영향 (Effect of Yarns Cross-Sections and Structure Parameters of Its Knitted Fabrics to Moisture Transport of Perspiration Absorption and Fast Dry Fabrics)

  • 김현아
    • 한국의류산업학회지
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    • 제20권4호
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    • pp.457-463
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    • 2018
  • This study examined the water absorption and drying properties of the thirteen types of the knitted fabrics for sports wear. These physical properties were analysed with relation to the constituent fiber cross-sectional shape and structure parameters of the knitted fabrics by regression analysis. Absorption and drying properties of the knitted fabric specimens were increased with increasing the porosity of the constituent yarns, which was attributed to the capillary channels in the yarns. The water absorption and drying properties were increased and decreased with increasing tightness factor and stitch density of the knitted fabric. The absorption property of the knitted fabric for perspiration absorption and fast dry sport-wear clothing was mostly influenced mostly by fiber cross-sectional shape and its characteristics, whereas, drying property was dependent on the structural parameters of the knitted fabric such as tightness factor and stitch density. Therefore, superior perspiration absorption and fast drying knitted fabric could be obtained in the fabric structure with optimum tightness factor and stitch density, and constituent yarn structure with non-circular fiber crosssection and high porosity. GATS method and MMT method are used to measure sweating fast drying properties and it is necessary to carry out studies using these measurement methods in order to compare with the results of this study.

산사 분획의 혈관이완 활성과 성분분석에 관한 연구 (Vasodilatory Effect of the Fractions from Crataegus pinnatifida and Isolation of the Active Component)

  • 최호정;신동훈;김길훤;신흥묵
    • 동의생리병리학회지
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    • 제17권5호
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    • pp.1235-1242
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    • 2003
  • This study was performed for the investigation of vasodilatory effects of Crataegus pinnatifida Bunge and for isolation and structure determination of the constituent from the active fraction. The fruits of this herbal drug were extracted with 80% methanol, then fractioned successively with methylene chloride, ethylacetate and n-butanol. Among the fractions, ethyl acetate fraction exhibited the most effective vascular relaxation against phenylephrine-induced arterial contraction. In order to isolate the active constituent by activity-guided fractionation, this fraction was chromatographed on silica gel to yield seven subfractions. Among the subfractions, the active one showing the most potent vascular relaxation activity was further separated by prep. HPLC with reversed phase Microsorb C-18 column using 1 % acetic acid and methanol gradient solvent system to afford one pure compound, which revealed a potent vasodilatory effect. Instrumental analyses (NMR and mass spectrometry) of the isolated constituent indicated this compound to be (-)-epicatechin. The vasodilatory action mechanism of this compound should be further investigated.

Effects of Constituent Amino Acids of Glutathione and Ammonium Sulfate added to Hydroponic Solution on the Synthesis of Glutathione in Lettuce

  • Kim Ju-Sung;Seo Sang-Gyu;Kim Sun-Hyung;Usui Kenji;Shim Le-Sung
    • Journal of Plant Biotechnology
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    • 제7권3호
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    • pp.195-202
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    • 2005
  • The effects of constituent amino acids of glutathione (GSH), glutamate (Glu), cysteine (Cys) and glycine (Gly), on GSH synthesis in lettuce seedlings were examined in this study. The GSH concentration of the seedlings was increased to 5.1-fold and 1.6-fold the concentration of the control in the first leaves and roots, respectively, by simultaneous application of these constituent amino acids (Glu+Cys+Gly) at 100 mg/l to the culture solution for two days. In the first leaves and roots of these seedlings, the concentration of GSH was 180.4 and 14.6 nmole/gFW, and non-essential amino acids including Glu, Cys and Gly occupied 93.2% and 84.0% of the total free amino acids, respectively. Application of Cys greatly increased the concentration of GSH in the roots, and application of 50 mg/l Cys increased it to 26.1-fold the concentration in the control. The activity of GSH synthetase was higher in the leaves than in the roots, whereas the activity of ${\gamma}$-glutamylcysteine synthetase was higher in the roots than in the leaves.

해양구조용 강재의 국부취화영역에 관한 연구 (Local brittle zone of offshore structural steel welds)

  • 김병천;엄정현;이종섭;이성학;이두영
    • Journal of Welding and Joining
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    • 제7권2호
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    • pp.35-48
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    • 1989
  • This study is concerned with a correlation of microstructure and local brittle zone (LBZ) in offshore structural steel welds. The influence of the LBZ on fracture toughness was investigated by means of simulated heat-affected zone (HAZ) tests as well as welded joint tests. Micromechanical processes involved in void and cleavage microcrack formation were also identified using notched round tensile tests and subsequent SEM observations. The LBZ in the HAZ of a multiphase welded joint is the interstitially reheated coarse grained HAZ, which is influenced by metallurgical factors such as effective grain size, the major matrix structure and the amount of high-carbon martensite-austenite (M-A) constituents. The experimental results indicate that Chirpy energy was found to scale monotonically with the amount of M-A constituents, confirming that the M-A constituent is the major microstructural factor controlling the HAZ toughness. In addition, voids and microcracks are observed to initiate at M-A constituents by the shear cracking process. Thus, the M-A constituent played an important role in initiating the voids and microcracks, and consequently caused brittle fracture.

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Analysis on Constituent Elements and Microstructure of Fiberglass Splint and Cast

  • Ham, Joo Hyun;Jung, Han Suk
    • 한국재료학회지
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    • 제31권8호
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    • pp.433-438
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    • 2021
  • In this study, microstructural characteristics and constituent elements of fiberglass splint and cast are examined using a scanning electron microscope and an energy dispersive X-ray spectrometer. As observed by the scanning electron microscope, fiberglass splint and cast had a porous structure with many bundles of fiberglass textures well assembled. Spaces between bundles of the fiberglass splint are triangular or elliptical shaped and the long-axis diameter is measured at about 1 mm. The thickness of fiber bundles covered with plaster is measured at 600 ㎛ and the diameter of a single strand of fiberglass is up to 10 ㎛. The thickness of the fiberglass bundle of the fiberglass splint is measured at about 700 ㎛. Spaces between bundles are formed in the shape of triangles with gentle edges and long-axis diameter of up to 1.4 mm, which is larger than that of the splint. The thickness of a single strand of fiberglass of the plaster-coated cast is 11.5 ㎛, which is thicker than that of fiberglass of the splint. As a result of analyzing constituent elements of the fiberglass cast and the splint with an energy dispersive X-ray spectrometer, Ca, Si, and Al components are identically detected. This result shows that the fiberglass cast has a smoother surface with hardened plaster than the fiberglass splint. The thickness of the fiberglass bundle and the thickness of a single strand of the fiberglass are also larger than those of the fiberglass splint.

전통 장류 유래 Bacillus subtilis SCJ4의 특성확인 및 통계학적 방법을 이용한 배양조건 최적화 (Identification of characterization and statistical optimization of medium constituent for Bacillus subtilis SCJ4 isolated from Korean traditional fermented food)

  • 정수지;양희종;정성엽;정도연
    • 미생물학회지
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    • 제51권1호
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    • pp.48-60
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    • 2015
  • 순창군에서 제조된 전통 장류로부터 612종의 다양한 미생물을 분리하였고, 612종의 미생물 중에서 생리활성 분석 및 biogenic amine 생성여부를 조사하여 최종적으로 Bacillus subtilis SCJ4를 선별하였다. 최종 선별한 균주 SCJ4의 생화학적 특성과 16S rRNA 염기서열 분석에 의해 B. subtilis SCJ4로 명명하였으며, B. subtilis SCJ4의 산업적으로 사용이 적합한 최적배지조성을 확립하기 위하여 통계학적 방법인 반응표면 분석법을 사용하였다. 실험계획법은 배지조성을 예측하기 위해 Plackett-Burman design을 사용하여 모델을 설정하였다. 실험 모델을 통하여 선별된 배지 조성으로는 tryptone, peptone, $MgSO_4$로 예측되었으며, 배지조성에 대한 농도를 설정하기 위해 중심합성계획법을 사용하여 최적화를 수행하였다. 최종 예측된 배지 조성의 농도는 tryptone 15.35 g/L, peptone 12.235 g/L, $MgSO_4$ 3.5 g/L로 예측되었다. 이때 최대 균체량은 1.07497 g/L로 예측되었으며, 모델의 검증실험을 통하여 예측된 모델과 실제 결과가 동일함을 확인하였으며, 기본배양배지와 비교하였을 때 균체량이 0.8767 g/L에서 1.1222 g/L으로 약 28%증가하였다.