• Title/Summary/Keyword: conductivity measurement

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Effects of Y2O3 and Al2O3 Addition on the Properties of Hot Pressed AlN Ceramics (AlN 세라믹의 hot pressing에 사용되는 Y2O3 및 Al2O3 소결조제의 효과)

  • Kong, Man-Sik;Hong, Hyun-Seon;Lee, Sung-Kyu;Seo, Min-Hye;Jung, Hang-Chul
    • Korean Journal of Materials Research
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    • v.17 no.10
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    • pp.560-566
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    • 2007
  • AlN plates were fabricated by hot pressing at $1700-1900^{\circ}C$ using yttria and alumina (3 and $10\;{\mu}m$ particle size) powders as additives and characterized: density, thermal conductivity, transverse rupture strength, and grain size measurement by SEM and EDS. Density values of $3.31-3.34\;g/cm^3$ are largely attributed to hot pressing of powder mixtures in carbon mold under $N_2$ atmosphere which caused effective degree of oxygen removal from yttrium-aluminate phase expected to form at $1100^{\circ}C$. The grain size of hot pressed AlN was almost homogeneous, with size approximately from 3.2 to $4.0\;{\mu}m$ after hot pressing. $Al_2O_3$ powder of $3\;{\mu}m$ particle size resulted in better transverse rupture strength and finer grain size compared to $10\;{\mu}m$ $Al_2O_3$ powder. The thermal conductivity of AlN ranged between $83-92.7\;W/m{\cdot}K$ and decreased with $Al_2O_3$ addition. Fine grain size is preferred for better mechanical properties and thermal conductivity.

Effect of Calcination Temperature on Ionic Conductivity of All-solid State Battery Electrolytes (하소 온도가 전고체 전지 전해질의 이온전도도에 미치는 영향)

  • Yu Taek Hong;Ji Min Im;Ki Sang Baek;Chan Gyu Kim;Seung Wook Baek;Jung Hyun Kim
    • New & Renewable Energy
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    • v.20 no.2
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    • pp.71-81
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    • 2024
  • In this study, the electrochemical properties of garnet-structured all-solid-state battery electrolytes (Li6.4La3Zr1.4Ta0.6O12, hereafter LLZTO) were assessed by altering the calcination temperature, while maintaining a consistent sintering duration. Among the various heat treatment conditions employed for sample fabrication, the '700_1100' condition, denoting a calcination temperature of 700℃ and a sintering temperature of 1100℃, resulted in the most exceptional ionic conductivity of 4.89 × 10-4 S/cm and a relative density of 88.72% for the LLZTO material. This is attributed to the low calcination temperature of 700℃, leading to reduced grain size and enhanced cohesiveness, thus resulting in a higher sintered density. In addition, a microstructure similar to the typical sintering characteristics observed in Spark Plasma Sintering (SPS) methods was identified in the SEM analysis results under the '700_1100' condition. Consequently, the '700_1100' heat treatment condition was deemed to optimal choice for enhancing ionic conductivity.

Onset of Natural Convection in Transient Hot Wire Device for Measuring Thermal Conductivity of Nanofluids (비정상열선법을 이용한 나노유체 열전도도 측정 시 자연대류 개시점에 대한 연구)

  • Lee, Seung-Hyun;Kim, Hyun-Jin;Jang, Seok-Pil
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.35 no.3
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    • pp.279-285
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    • 2011
  • We perform a numerical study to determine the time of onset of natural convection in a transient hot wire (THW) device for measuring the thermal conductivity of nanofluids. The samples used in this simulation are water-based $Al_2O_3$ nanofluids with volume fractions of 1%, 4%, and 10%, and the properties are calculated by theoretical models and experimental correlations. The THW apparatus using coated wire is modeled by the control-volume-based finite difference method, and the start of natural convection is determined by observing the temperature rise of the wire under a gravity field. The onset time is 11.5 s for water and 41.6 s for water-based $Al_2O_3$ nanofluids predicted by Maxwell thermal conductivity model with a 10% volume fraction. We confirm that the onset time of natural convection of nanofluids in the cylinder increases with the nanoparticle volume fraction. We suggest a correlation for predicting the onset time on the basis of the numerical results. Finally, it is shown that the measurement error due to natural convection is negligible if the measurement using the transient hot wire method is completed before the onset of natural convection in the base fluid.

Effect of Lithium Ion Concentration on Electrochemical Properties of BF3LiMA-based Self-doping Gel Polymer Electrolytes (BF3LiMA기반 자기-도핑형 겔 고분자 전해질의 전기화학적 특성에 미치는 리튬이온 농도의 영향)

  • Kang, Wan-Chul;Ryu, Sang-Woog
    • Journal of the Korean Electrochemical Society
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    • v.13 no.3
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    • pp.211-216
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    • 2010
  • Boron trifluoride lithium methacrylate ($BF_3$LiMA)-based gel polymer electrolytes (GPEs) were synthesized with various $BF_3$LiMA concentration to elucidate the effect on ionic conductivity and electrochemical stability by a AC impedance and linear sweep voltammetry (LSV). As a result, the highest ionic conductivity reached $5.3{\times}10^{-4}Scm^{-1}$ at $25^{\circ}C$ was obtained for 4 wt% of $BF_3$LiMA. Furthermore, high electrochemical stability up to 4.3 V of the $BF_3$LiMA-based GPE was observed in LSV measurement since the counter anion was immobilized in this self-doped system. On the other hand, it was assumed that there was a rapid decomposition of electrolytes on a lithium metal electrode which results in a high solid electrolyte interface (SEI) resistance. However, a high stability toward graphite or lithium cobalt oxide (LCO) electrode thereby a low SEI resistance was observed from the AC impedance measurement as a function of storage time at $25^{\circ}C$. Consequently, the high ionic conductivity, good electrochemical stability and the good interfacial compatibility with graphite and LCO were achieved in $BF_3$LiMA-based GPE.

Use of Electromagnetic Inductance for Salinity Measurement in Reclaimed Saline Land (전자장 유도 장치를 이용한 간척지 토양의 염농도 측정)

  • Jung, Yeong-Sang;Lee, Won-Ho;Joo, Jin-Ho;Yu, Il-Ho;Shin, Wan-Sik;Ahn, Yeol;Yoo, Sun-Ho
    • Korean Journal of Soil Science and Fertilizer
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    • v.36 no.2
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    • pp.57-65
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    • 2003
  • Mapping of salinity distribution in the reclaimed lands was attempted by using the electromagnetic inductance technique. Field study was conducted to monitor ground conductivity with an electromagnetic inductance, EM 38 (Geonics), and electrical conductivity of the saturated extract, ECe of the soils, at the Daeho reclaimed land. EM values of horizontal mode, EMh, and vertical mode, EMv, mode were recorded at the interval of $2m{\times}2m$ from the ground. Soil samples were taken through the profile down to 100cm for calibration. ECe of poor drained area of Daeho, were in the range of $19.50-91.50ds\;m^{-1}$, while ECe of well-drained area ranged from $1.10-34.40ds\;m^{-1}$. Multiple regression equations for the measured EMv, EMh, and ECe were highly significant. The EMh showed higher correlation with ECe than EMv. With the multiple equation, ECgM could be calculated. Correlation between ECe and ECgM was the highest ($r=0.753^{***}$), when EMI readings were taken on the ground. The relationships were highly significant below 30 cm height of measurement, With the EM38 measurement, the salinity distribution was effectively expressed for the experimental filed in Daeho reclaimed land.

Application of Taguchi's Robust Design Method in Optimization of Measuring Electrical Properties on Acupoints: A Pilot Study (Taguchi 실험계획법을 이용한 경혈점의 피부전기특성 최적화조건 선정 : A Pilot Study)

  • Nam, Tong-Hyun;Shin, Sang-Hoon
    • Korean Journal of Acupuncture
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    • v.25 no.3
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    • pp.15-27
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    • 2008
  • Objectives : The objective of the current study is to optimize an acupoint electrical property measurement system by using the procedures and strengths of the Taguchi method. Methods : Taguchi method was applied in the optimization of the acupoint electrical property measurement system, as in the following steps: (1) determine evaluation index; (2) execute the 1st gage R&R; (3) identify controllable and uncontrollable factors; (4) design Taguchi crossed array layout; (5) execute experiments according to trial conditions; (6) analyze testing results; (7) determine optimum run; (8) execute the 2nd gage R&R; (9) confirm optimum run. Results : The results showed that electrodes with larger diameter and efferent electric current, with music played, can produce the larger different electrical conductivity between the acupoints and the non-acupoints under various conditions. Taguchi process optimization improved repeatability and reproducibility of the acupoint electrical property measurement system. Conclusions : In the optimized condition, repeatability and reproducibility of the acupoint electrical property measurement system was acceptable.

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Doping Diamond for Electronic Application

  • Kalish, R.
    • The Korean Journal of Ceramics
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    • v.2 no.4
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    • pp.188-192
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    • 1996
  • Diamond based electronic devices promise to exhibit unique properties. In order to realize devices diamond has to be doped to render it electrically conductive. In the present work the doping of diamond and of polycrystalline CVD diamond films are reviewd with particular emphasis to ion-implantation doping and to attempts to dope diamond by in-diffusion of the dopants. The quest for finding ways to obtain n-type conductivity in diamond will be critically examined.

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Signal Analysis Software for DGPS Station (DGPS 기준국 신호분석 소프트웨어)

  • Hwang, Ho-Yon
    • Journal of the Korean Society for Aviation and Aeronautics
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    • v.15 no.2
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    • pp.1-8
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    • 2007
  • In this research, algorithm and software for the medium frequency signal analysis of DGPS(Differential Global Positioning System) station were developed. Based on new MF(Medium Frequency) algorithm, the software of NDGPS(National DGPS) signal analysis was developed for coverage analysis. Predicted MF propagation data from this software was compared to the measurement data for the verification of a developed MF algorithm. GIS(Geographic Information System) techniques including digital map with elevation data were used because MF propagation is closely related to ground conductivity, mountains, building intensity.

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Measurement on Nutrient Solution (양액 상태의 계측)

  • 류관희
    • Journal of Bio-Environment Control
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    • v.2 no.2
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    • pp.147-149
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    • 1993
  • 양액재배에 있어서 배양액 중에 있는 질소, 칼륨, 인, 칼슘, 마그네슘 등 식물 영양성분의 함유량을 항상 알맞게 유지시키는 일은 매우 중요하다. 아울러, 양액의 산도(pH)와 용존산소량(dissolved oxygen;DO)도 식물 생장에 큰 영향을 미치기 때문에 적절히 유지하지 않으면 안된다. 양액의 상태를 항상 작물 생육에 알맞게 유시키기 위해서는 먼저 양액의 조성과 관계가 있는 물리량을 정확히 측정할 필요가 있다. 특히 양액관리를 자동화하기 위해서는 정확도와 함께 신속하고도 간편한 측정방법이 필요하다. 양액 상태에 관한 주요 측정항목에는 전기전도도(electric conductivity : EC), 산도(pH), 용존산소량(DO)이 있다.

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The discharge characteristics and ICP-AES analysis of insulators by surface deterioration (애자 표면열화에 의한 방전특성과 ICP-AES 분석)

  • Shong, Kil-Mok;Kim, Young-Seok;Jung, Jin-Soo
    • Proceedings of the KIEE Conference
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    • 2009.07a
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    • pp.1408_1409
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    • 2009
  • It's described the discharge characteristics and ICP-AES analysis of insulators by surface deterioration in this paper. For the assessment of insulators, there are applied the conductivity of dusts, contact angle measurement of the insulator surfaces and the ingredient analysis in each area. Through the analysis of pollutants attached to insulators inside the tunnel, the cleaning cycle is discussed. As the results, it would be expected to the electrical safety.

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