• Title/Summary/Keyword: concentration measuring test

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An Experimental Study on Miscibility and Vapor Pressure of R-744/Oil Mixtures (R-744/오일 혼합물의 상용성 및 증기압에 관한 실험적 연구)

  • 최희성;강병하;박경근;김석현
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.16 no.2
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    • pp.150-157
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    • 2004
  • Carbon dioxide ($CO_2$, R-744) has become a very popular issue in application to refrigeration and air conditioning systems as a natural refrigerant. An experimental study has been carried out to investigate miscibility and the vapor pressure of refrigerant R-744 in the presence of lubricant oil. This is of particular interest in the selection of the lubricant oil for the compressor of a refrigeration system or an air conditioning system using the refrigerant R-744. The experimental set-up consists of the equilibrium cell, measuring devices, the vacuum pump, the constant temperature bath and relevant connecting pipes made of stainless steel. Five lubricant oils, such as mineral oil (Naphthenic), AB (Alkyl Benzene) oil, PAO (Poly Alpha Olefin) oil, PAG (Poly Alkylene Glycol) oil and POE (Polyol Ester) oil are considered in the present study. Test runs were conducted with the oil concentration range from 5 to 50 wt%, and the temperature range from -10 to 1$0^{\circ}C$ with 2$^{\circ}C$ intervals. The miscibility results are visualized and correlated with the vapor pressure for the individual test components.

Self-Decomposition Characteristic of Concentrated Hydrogen Peroxide with Temperature and Stabilizer (저장 온도와 안정제 양에 따른 고농도 과산화수소의 자연 분해 특성)

  • Chung, Seung-Mi;An, Sung-Yong;Kwon, Se-Jin
    • Journal of the Korean Society of Propulsion Engineers
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    • v.13 no.4
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    • pp.16-21
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    • 2009
  • This paper introduces the methods of hydrogen peroxide storage test and storability of concentrated hydrogen peroxide is estimated. Using the method of simple concentration measuring, storability was evaluated. Experiment variables were the amount of stabilizer in hydrogen peroxide, storage temperature, and caps of vessels. The experiments were performed during 8 months to 24 months. High purity hydrogen peroxide had much better storability than hydrogen peroxide with much stabilizer. In addition, the case using paraffin film which did not react with hydrogen peroxide for covering showed better storability. The temperature is very important variable in hydrogen peroxide storage. So, when hydrogen peroxide was under $10^{\circ}C$ storability of hydrogen peroxide is much improved.

Evaluation on Design Factors of Electrolytic Flotation Reactor by Measuring Polarization Curve (분극곡선 측정을 통한 전해부상조의 설계인자 평가)

  • Lim, Bong-Su;Jin, Jing-Zhu;Choi, Chan-Soo
    • Journal of Korean Society on Water Environment
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    • v.23 no.2
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    • pp.244-250
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    • 2007
  • This study was carried out to obtain the optimum design factors for an eletrolytric flotation reactor. When the effluent of the leachate treatment facility was treated under the condition of 10 volts, 30 minutes, at the Al-Al electrode system; COD removal efficiency was 45%, and total phosphorus removal efficiency was 98%. The high removal efficiency was caused by the fact that phosphate was removed by leaching $Al^{3+}$ from two electrodes. The leachate containing high ammonium nitrogen concentration was treated by a batch test under the condition of 60 minutes reaction time and added chloride ion; ammonium nitrogen removal efficiency was 89%. This high efficiency was affected by added chloride ion to wastewater. To find the optimum current density and voltage of the leachate containing chloride ion (ratio of $Cl^-/NH_4-N$ is 11) a electrochemical polarization curve was used. These values were found to be $4.5mA/cm^2$ and about 2.1 V, respectively. When C-Al electrode system was used at a batch test, the total nitrogen removal efficiency was increased by 1.8 to 3.3 times, compared to Al-Al electrode system due to high $Cl_2$ gas production.

An Experimental Study on Variations of Exhaust Gas Temperature and Concentration with Synthetic Gas Combustion in Exhaust Manifold (배기관에서의 합성가스 연소에 따른 배기가스 온도 및 농도 변화에 관한 실험적 연구)

  • Cho, Yong-Seok;Lee, Seang-Wock;Yang, Seung-Il;Song, Chun-Sub;Park, Young-Joon
    • Transactions of the Korean Society of Automotive Engineers
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    • v.16 no.4
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    • pp.56-62
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    • 2008
  • A synthetic gas reformed from hydrocarbon-based fuels consists of $H_2$, CO and $N_2$. Hydrogen contained in the synthetic gas is a very useful species in chemical processes, due to its wide flammability range and fast burning speed. The ESGI (Exhaust Synthetic Gas Injection) technology is developed to shorten the light-off time of three way catalysts through combustion of the synthetic gas in the exhaust manifold during the cold start period of SI engines. Before the ESGI technology is applied to the test engine, the authors set a test rig that consists of gas temperature and composition controllers, an exhaust pulse generator and an exhaust manifold with a visualization window, in order to optimize the point and conditions of injection of the synthetic gas. Through measuring burned gas temperatures and taking photographs of synthetic gas combustion at the outlet of the exhaust manifold, the authors tried to find the optimal injection point and conditions. Analysis of burned gas composition has been performed for various $O_2$ concentrations. As a result, when the synthetic gas is injected at the port outlet of the cylinder No. 4 and $O_2$ concentration exceeds 4%, combustion of the synthetic gas is strong and effective in the exhaust manifold.

An Assessment of Measurement of Serum Free $T_3,\;T_4$ by Radioimmunoassay (방사 면역측정법에 의한 혈청내 갑상선 유리홀몬 측정의 임상적의의에 대한 기본적 검토)

  • Kim, Young-Hun;Lee, Hyung-Ho;Ahn, Hee-Kwon;Kim, Sook-Joo;Kim, Jun-Suk;Ahn, Il-Min;Lee, Chang-Hong;Park, Seung-Chull
    • The Korean Journal of Nuclear Medicine
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    • v.19 no.1
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    • pp.113-117
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    • 1985
  • The present study was undertaken to examine serum concentration of free $T_3,\;T_4$, in various functional states of the thyroid by Amerlex RIA kit method, which uses unidentified $T_3,\;T_4-labelled$ analogues, said to be unreactive with $T_3,\;T_4-binding$ proteins in serum, together with an antibody that binds both analogue and $T_3,\;T_4$. The test method has been compared with free $T_4$ index, which was product of total serum thyroxine and $T_3$ resin uptake ratio. Free $T_4$ value by this method was found to have a highly significant positive correlation with a free $T_4$ index (r; 0.957, p<0.005) and total $T_4$ (r:0.89, p<0.005) also, it was similar to other free $T_4$ measuring methods previously reported. So, it was showen to have the clinical utility as the screening test for thyroid function because it was a rapid; convinient, and reliable method for quantifying the free $T_4,\;T_3$ concentration in various thyroidal functional states.

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Comparative Analysis between Direct-reading Meter of PID and GC-FID using the Active Type Air Sampler for VOCs Measurement (직독식 측정기 PID와 능동식 시료채취기에 의한 GC-FID 정량분석법의 VOCs 농도 비교 연구)

  • Yeo, Jin-Hee;Choi, Kwang-Min
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.26 no.3
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    • pp.301-306
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    • 2016
  • Objectives: Direct-reading instrument(Photoionization detectors, PID) and quantitative analysis using active type air sampling (Gas chromatography-flame ionization detector, GC-FID) were tested to evaluate their ability to detect volatile organic compounds(VOCs) in a semiconductor manufacturing plant. Methods: The organic compounds used were acetone and ethanol which are normally used as cleaning solutions in the semiconductor manufacturing. The evaluation was based on the preparation of test solutions of known acetone and ethanol concentration in a chamber($600{\times}600{\times}1150mm$). Samples were prepared that would be equivalent to 5~100 ppm for acetone and 10~ 200 ppm ethanol. GC-FID and PID were evaluated simultaneously. Quantitative analysis was performed after sampling and the direct-reading instrument was checked using real-time data logging. Results: Positive correlations between PID and GC-FID were found for acetone and ethanol at 0.04~2.4% for acetone(TLV: 500 ppm) and 0.1~8.3% for ethanol(TLV: 1000 ppm). When the sampling time was 15 min, concentration of test solution was the most similar between measurement methods. However, the longer the sampling time, the less similar the results. PID and GC-FID had similar exposure patterns. Conclusions: The results indicate that PID and GC-FID have similar exposure pattern and positive correlation for detection of acetone and ethanol. Therefore, PID can be used for exposure monitoring for VOCs in the semiconductor manufacturing industry. This study has significance in that it validates measuring occupational exposure using a portable device.

Emission Characteristics of Greenhouse Gases (CH4, N2O) in Mechanically Ventilated Swine Farm during Winter Season (겨울철 강제환기식 돈사 내 온실가스 (CH4, N2O) 배출 특성 연구)

  • Park, Junyong;Jung, Minwoong;Jo, Gwanggon;Jang, Yu-Na
    • Journal of The Korean Society of Agricultural Engineers
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    • v.63 no.4
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    • pp.33-41
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    • 2021
  • The emission characteristics and emission factors were determined by measuring the concentration of methane (CH4) and nitrous oxide (N2O), the amount of ventilation, etc. in the two fattening rooms which have the same environment in winter. As a result of monitoring, the average concentration of CH4 and N2O was 20.7-26.7 ppm and 1.4-1.6 ppm. The average temperature inside the room was measured at 20.0-21.4℃, and the average ventilation was 1345.4-1567.3 m3/h. The daily emission of CH4 for the first 30 days showed a constant emission of 3.6-8.2 g/d/m2/pig, but thereafter, the emission increased rapidly. The daily emission of N2O was 0.7-1.3 g/d/m2/pig, showing stable emission during the test period, and relatively insignificant emission compared to the emission of CH4. After repeated test, it was confirmed that there was no significant difference between the two rooms. As a result, the CH4 6. 21 g/d/m2/pig and N2O 1.02 g/d/m2/pig average emission for each room was derived.

Effect of YGF251 on Secretion Of IGF-1 in Human Blood (YGF251 투여에 의한 인체내 혈중의 IGF-1 분비량 변화 효과)

  • 김재수;박준홍;조한성;박점석;홍억기
    • KSBB Journal
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    • v.17 no.4
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    • pp.403-408
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    • 2002
  • For stimulating the in vivo secretion of IGF-1 (insulin-like growth factor-1) which is well known to promote the various physiological actions in human body, the natural herbal extract, YGF251 (young growth factor 251), was developed and evaluated for its effect as IGF-1 secretagogue in this study. The clinical study was peformed as double blind test, and 31 adult female and male volunteers between the age of 40 and 70 were investigated for their changes of concentration of IGF-1 , insulin level, weight, blood pressure, and liver and kidney functions. As the result of paired sample test on the change of the concentration of IGF-1, in YGF251 treated group, it was 245.6 ng/mL before dosing. The concentration of IGF-1 was increased to 269.3 ng/mL after a month and to 275.6 ng/mL after two months, and both were statistically significant (p〈0.05). While in control group, the concentration of IGF-1 was 280.0 ng/mL before dosing, but decreased to 239.2 ng/mL after a month and to 230.2 ng/mL after two months, and both were also statistically significant (p〈0.05). In YGF251 treated group, the concentration of insulin in blood increased about 2 times after a month dosing as an average level, but in control group, it showed a decrease of 36% compared with before dosing. And there were little changes regarding to the measured weight and blood pressure. Various measured data in order to observe the alteration in liver and kidney functions by the administration of YGF251 showed a little change within measuring error range.

An Experimental Study on Thermal Conductivity Change of Water-Al2O3 Nanofluid with the Elapse of Time, Stirring, and Adding Dispersing Agent (시간경과, 교반 및 분산제 첨가에 따른 물-Al2O3 나노유체 열전도도 변화에 관한 실험적 연구)

  • Park, Dong-Uk;Park, Chang Yong
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.22 no.3_1spc
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    • pp.537-543
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    • 2013
  • A water-$Al_2O_3$ nanofluid was manufactured, and its thermal conductivity was measured in this study. The measurement was performed at volumetric concentrations of 0.5%, 1%, 2%, and 3%, and the nanoparticle sizes were 20 nm and 70 nm. Experimental test equipment, using the transient hot wire method, was installed to measure the thermal conductivity of the nanofluid, and the measured results were confirmed by measuring pure water with a measurement error of 0.92% at $20^{\circ}C$. The thermal conductivity enhancement ranged from 4.8% to 13.6% for the 20 nm particle size, and from 3.1% to 8.8% for the 70 nm particle size at a concentration range of 0.5% to 3%. The enhancement increased with a decrease in particle size and an increase in concentration. With the elapse of time after manufacturing the nanofluid, the thermal conductivity enhancement decreased significantly from 5 to 9 h, and this trend was measured under all of the measurement conditions. After 24 h, the enhancement ranged from 1.2% to 3.5% for the 20 nm particles, and from 0.6% to 2.3% for the 70 nm particles. The enhancement trends with the elapse of time were almost identical with and without stirring the nanofluid. SDBS (Sodium Dodecyl Benzene Sulfonate) was added as a dispersing agent, and the decrease in the thermal conductivity enhancement was delayed.

INFLUENCES OF SILANE CONCENTRATION FOR FILLER SILANIZATION ON THE PROPERTIES OF COMPOSITES (필러의 실란처리농도가 복합레진의 특성에 미치는 영향)

  • 조태희;박상진
    • Restorative Dentistry and Endodontics
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    • v.26 no.1
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    • pp.23-31
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    • 2001
  • The purpose of this study was to search the optimal silane concentrations for filler- silanization of seven experimental composites. Silica filer was a 25micron crushed type. 0.0%, 0.5%, 1.0%, 1.5%, 2.0%, 2.5%, and 3.0% silane($\gamma$-methacrylooxypropyltrimethoxysilane)were added into silica-filler with weight percentage (wt%). Mixtures(silica filler/silane)were reacted at 6$0^{\circ}C$ for 72hours, and crushed into fine particles those were used as fillers for 7 experimental composites. Monomer was a 3 : 1 mixture of Bis-GMA and TEGDMA containing 0.2% tertiary amine and 0.4% camphoroquinone for light curability. A ratio for mixing the monomer and filler was 75% and 25% respectively. Seven experimental composites was classified with the concentration of silane treated, and the specimen number for each test was 10. Specimens with 6mm diameter and 3mm height dimension for measuring the diametral tensile strength were destroyed with 1mm/min cross-head speed on Instron universal testing machine (No. 4467, USA). Shear bond strength was measured on the specimens bonded to bovine enamel etched with 37% phosphoric acid solution for 1 minute Fractured surfaces were observed by SEM (Hitachi S-3200, Japan) among that of the highest values measured from each groups. Following results were obtained: 1. Experimental composites containing silanized filter showed the significantly higher diametral tensile strength and shear bond strength than the composites containing un-silanized fillers(Group1) (p<0.05). 2. In silanized filler composite resins(Group 2~7), Diametral tensile strength of Group 3 showed the significantly higher than that of Group 2 and Group 6(p<0.05). 3. Shear bond strength was higher in Group 3 than that of Group 7 (p<0.05)in silanized fillers composite resins. 4. Fracture surface was formed in resin matrixes on the specimens from composites containing the fillers treated with 0.5% 1.0%, and 1.5% silane. These results mean that the optimal silane concentrations are exist for each fillet with its size and surface area, and that 1.0% is a optimal value for concentration to coat the 25$\mu\textrm{m}$ filler with silane.

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