• 제목/요약/키워드: columnar structure

검색결과 277건 처리시간 0.038초

Cobalt Oxide Nanorods Prepared by a Template-Free Method for Lithium Battery Application

  • Kim, Seong-Jun;Kim, Eun-Ji;Liu, Meilin;Shin, Heon-Cheol
    • Journal of Electrochemical Science and Technology
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    • 제7권3호
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    • pp.206-213
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    • 2016
  • Transition metal oxide-based electrodes for lithium ion batteries have recently attracted much attention because of their high theoretical capacity. Here we report the electrochemical behavior of cobalt oxide nanorods as anodes, prepared by a template-free, one-step electrochemical deposition of cobalt nanorods, followed by an oxidation process. The as-deposited cobalt has a slightly convex columnar structure, and controlled thermal oxidation produces cobalt oxides of different Co/O ratios, while the original shape is largely preserved. As an anode in a rechargeable lithium battery, the Co/O ratio has a strong effect on initial capacity and cycling stability. In particular, the one-dimensional Co@CoxOy core shell structure obtained from a mild heat-treatment results in superior cycling stability.

亞鉛電着層의 현미경조직에 미치는 電解液흐름의 影響 (The effect of electrolyte flow on the microstructure of zinc electrodeposits)

  • 예길재;김용웅;안덕수
    • 한국표면공학회지
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    • 제18권4호
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    • pp.164-183
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    • 1985
  • The microstructure of the zinc electrodeposits was investigated by changing the flow rate of electrolyte in zinc sulfate Bath. The cathode current efficiency increased with increasing flow rate of electrolyte. The preferred orientation of zinc electrodeposit changed from (11.2) texture to (10.3) or (10.1)+(10.2) texture with increasing current density in the range of flow rate, 0.2-1.2m/sec. The morphology of the deposits changed from the sponge deposit to the blocks of hexagonal crystallites packed together through the structures of find polycrystallite with increasing current density. The microstructure of the cross-section of the above deposits are granular structure and columnar structure respectively. The surface roughness of zinc electrodeposits decreased with increasing current density and flow rate of electrolyte.

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수직자기기록매체 CoCrMo 박막의 구조와 자기적 성질 (Structural and Magnetic Properties of perpendicular Recording Medium CoCrMo thin Film)

  • 남인탁;홍양기
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1988년도 추계학술대회 논문집
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    • pp.46-46
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    • 1988
  • Structural and magnetic properties of Co-Cr-Mo films were investigated in connection with sputtering conditions. Films were prepared using a convention RF sputtering system. X-ray diffractometry, scanning electron microscopy and transmission electron microscopy were employed to investigate structure properties. Vibrating sample magnetometry was used for coercivity and saturation magnetization measurements. Co-Cr-Mo films displayed reasonable values of perpendicular coercivity and saturation magnetization for perpendicular recording media and showed good perpendicular orientation of the hcp c-axis to the film surface. Perpendicular coercivity was strongly dependent upon substrate technique showed better c-axis orientation than hose using the stationary substrate. Co-Cr-Mo films of 2.9 at. % Mo content showed maximum perpendicular coercivity and saturation magnetization. The films deposited at lower Ar pressure showed good magnetic properties. There was no explicit relationship between the columnar structure and c-axis orientation. Co-Cr-Mo films was found to have suitable structural and magnetic properties for perpendicular recording media.

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SNMP 기반 NMS에서 네트웍 관리를 위한 NE MIB의 자동 Import System 설계 (Automatic import system of NE MIB for network management at NMS based on SNMP)

  • 강광석;김영진;박상대;정성현;조종신
    • 대한전자공학회:학술대회논문집
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    • 대한전자공학회 2002년도 하계종합학술대회 논문집(1)
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    • pp.109-112
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    • 2002
  • SNMP is generally used protocol for network management. SNMP need MIB for exchanging management information But, method for sharing MIB is not automatic. General MIB sharing architecture is done by network management operator by manually. In this paper we describe exchanging MIB automatically using meta-MIB. We will formalize SMI as MIB structure. This meta MIB represent information about MIB of NE Agent. Meta MIB has Information of object in the MIB, Structure and index information fur columnar object, meaning of subtype at INTEGER syntax. Also, trap related information is represented too. In this paper, MIB information is represented as instance of meta MIB. This architecture will provide a method for automatic MIB exchanging

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원심 주조 스텐레스 강에서의 이론적 모델을 통한 Beam Skewing 영향 고찰 (A study on the effect of ultrasonic beam skewing based on theoretical model approach in CCSS)

  • 이삼래;임형택;이윤상
    • 비파괴검사학회지
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    • 제10권1호
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    • pp.24-28
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    • 1990
  • Centrifugally Cast Stainless Steel generally shows similar structure to the weld in austenitic stainless steel in the point of casting. When examining this material ultrasonically, the beam does not generally propagate straightforward but rather deviates from its original direction and this phenomenon called skewing is originally caused by anisotropic material. In order to calculate the beam skewing effect theoretically, work has been performed based on a model approach which has regarded material itself as having been composed of multi-layered columnar dendrite structure and the result was compared with the one from experiment. The result from both theory and experiment showed good correlation and ultrasonic beam showed the least skewing with around 45 degree incident angle.

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Variation of Magnetic Properties of Electrodeposited CoPtP thin films by Electrochemically Multilayered Structure

  • S. W. Kang;Lee, K. H.;W. Y. Jeung
    • 한국자기학회:학술대회 개요집
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    • 한국자기학회 2002년도 동계연구발표회 논문개요집
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    • pp.206-207
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    • 2002
  • 전기도금방식으로 구현된 자기박막 재료로서 CoPtP 박막은 이제까지 보고된 재료 중 가장 높은 보자력 (H$_{c}$ > 5 kOe)과 뛰어난 각형비 (S*≒0.7)를 가지고 있는 3원계 합금 박막재료이며[1], 차세대 고밀도 자기저장매체로서 [2] 각광받고 있다. 하지만 이제까지 보고된 연구결과는 CoPtP 박막을 전기도금방식으로 제작했을 때, 두께가 약 1$\mu\textrm{m}$ 이상일 경우, 결정립이 큰 칼럼구조(columnar structure)가 성장하여 보자력이 현저히 떨어지는 현상[3]을 보여왔으며, 이러한 이유 때문에 MEMS 등에 응용되는데 많은 제약을 받아왔다. (중략)

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천연기념물 제411호 경남 고성 덕명리 공룡화석 산지 일원 병풍바위의 형성에 관한 암석학적 연구 (A petrological study on the formation of geological heritage around Sangjogam County Park, Goseong, Gyeongsangnam-do)

  • 공달용;조형성;김재환;유영완;정승호;김태형;김종선;정종옥;김건기;권창우;손문
    • 헤리티지:역사와 과학
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    • 제51권2호
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    • pp.78-91
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    • 2018
  • 경남 고성 상족암 일대는 화석, 연흔, 암맥, 주상절리 등 다양한 지질유산이 분포하고 있어 천연기념물 제411호(고성 덕명리 공룡과 새발자국 화석산지)로 지정되었다. 이 중 상족암의 주상절리는 해안에 인접하고 있어 아름다운 해안 경관을 이루고 있으며, 전체적인 형상은 거대한 병풍 모양을 연상케 하여 병풍바위라 불린다. 병풍바위에는 하위 퇴적층과의 경계면에 수직한 방향으로 주상절리가 특징적으로 발달하고 있다. 이번 연구에서는 병풍바위에 나타나는 주상절리를 대상으로 야외 및 현미경 관찰, 전암대자율 분석, X-선 회절 분석, 지화학 분석 등 암석 광물학적 연구와 대자율이방성(AMS) 분석을 통한 자기미세구조 연구를 수행하여 병풍바위와 주상절리의 형성과정에 대해 논의하였다. 병풍바위에 나타나는 산성 암상의 화학조성은 유문암의 조성을 가지며, 석영, 장석, 백운모, 견운모, 불투명광물 등이 관찰된다. 병풍바위에 대한 대자율이방성 분석 결과, 각 지점에서 입자들의 장 단축 방향을 나타내는 $k_1$$k_3$의 군집도가 매우 높게 나타나며, 납작한 형태의 엽리구조가 발달하고 있는데 이는 암맥, 용암류보다는 암상에서 발달하는 석리(rock fabric)로 해석된다. 결론적으로 병풍바위는 퇴적층의 층리면을 따라 관입한 암상이며, 주상절리는 관입한 유문암질 마그마의 냉각에 따른 수축에 의해 형성되었다. 이번 연구는 향후 국내에 분포하는 주상절리의 형성 메커니즘을 이해하는데 기초 자료로 활용할 수 있을 것이라 판단된다.

저탄소성 용접금속의 응고균열에 미치는 탄소함량의 영향 (The effect of carbon content on hot cracking of low carbon steel weld)

  • 정호신;엄동석
    • Journal of Welding and Joining
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    • 제6권4호
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    • pp.16-26
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    • 1988
  • The effect of carbon content on hot cracking of welded carbon steel was investigated Eight steel plates whose carbon content range from 0.02 to 0.23 percent were welded by autogeous gas tungsten are process. Constant strain was applied to the hot crack test specimen under the strain rate of 0.15 mm per second during welding. The hot cracking susceptibility ws high in the rnage of 0.02-0.05 and 0.12-0.23 percent carbon contents. The critical carbon content immune to hot cracking is in the range from 0.07 to 0.12 percent carbon. By electron probe microanalyser, amanganese segregation was not seen significantly in the whole carbon range. But segregation of silicon was higher in the region of low carbon contents. However, sulphur was segregated remarkably in the region betwen 0.18 and 0.23 percent carbon by peritectic reaction. Very smal lamount of dnedritic structure was observed in the region from 0.02 to 0.05 percent carbon by peritectic reaction. Very small amount of dendritic structure was observed in the region from 0.02 to 0.05 percent carbon but the predominant solidification structure was smooth by cellular growth. The higher the carbon content is, the more the columnar dendritic structure was observed.

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전선의 단면분석을 통한 단락특성에 관한 연구 (A Study on the Characteristics of Short Circuit through the Cross Section Analysis of Electric Wire)

  • 송길목;최충석;김윤회;김상현;박남규
    • 한국조명전기설비학회:학술대회논문집
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    • 한국조명전기설비학회 2005년도 춘계학술대회논문집
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    • pp.51-56
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    • 2005
  • For a fire cause judgement this paper describes the short circuit characteristics of a electric wire through the cross section analysis under ac condition. The cower wires prepared for the experiment were 1.2mm, 1.6mm, and 2.0mm in diameter. Through the cross section analysis(CSA), it was confirmed that the dendrite structure grew at the angle of about $40^{\circ}\;or\;60^{\circ}$ when the fusing current was applied to the wires. The larger the fusing current is, the more decreased the growth angle of the dendrite structure is. It was confirmed that the dendrite structure was arranged like the columnar structure. In this paper, the characteristics analysis of short circuit was carried out in the range of transient duration and the correlation constant k was investigated by measuring the short circuit duration and the fusing current.

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유도결합 플라즈마 파워가 VN 코팅막의 미세구조, 결정구조 및 기계적 특성에 미치는 영향에 관한 연구 (Effect of Inductively Coupled Plasma on the Microstructure, Structure and Mechanical Properties of VN Coatings)

  • 전성용;이소연
    • 한국표면공학회지
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    • 제49권4호
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    • pp.376-381
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    • 2016
  • The effects of ICP (Inductively Coupled Plasma) power, ranging from 0 to 200 W, on the crystal structure, microstructure, surface roughness and mechanical properties of magnetron sputtered VN coatings were systematically investigated with FE-SEM, AFM, XRD and nanoindentation. The results show that ICP power has a significant influence on coating microstructure and mechanical properties of VN coatings. With the increasing of ICP power, coating microstructure evolves from a porous columnar structure to a highly dense one. Average crystal grain size of single phase cubic fcc VN coatings was decreased from 10.1 nm to 4.0 nm with increase of ICP power. The maximum hardness of 28.2 GPa was obtained for the coatings deposited at ICP power of 200 W. The smoothest surface morphology with Ra roughness of 1.7 nm was obtained from the VN coating sputtered at ICP power of 200 W.