• 제목/요약/키워드: coefficients of determination

검색결과 755건 처리시간 0.028초

Physical and nuclear shielding properties of newly synthesized magnesium oxide and zinc oxide nanoparticles

  • Rashad, M.;Tekin, H.O.;Zakaly, Hesham MH.;Pyshkina, Mariia;Issa, Shams A.M.;Susoy, G.
    • Nuclear Engineering and Technology
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    • 제52권9호
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    • pp.2078-2084
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    • 2020
  • Magnesium oxide (MgO) and Zinc oxide (ZnO) nanoparticles (NPs) have been successfully synthesized by solid-solid reaction method. The structural properties of ZnO and MgO NPs were studied using X-ray diffraction (XRD) and scanning electron microscopy (SEM). XRD results indicated a formation of pure MgO and ZnO NPs. The mean diameter values of the agglomerated particles were around to be 70 and 50 nm for MgO and ZnO NPs, respectively using SEM analysis. Further, a wide-range of nuclear radiation shielding investigation for gamma-ray and fast neutrons have been studied for Magnesium oxide (MgO) and Zinc oxide (ZnO) samples. FLUKA and Microshield codes have been employed for the determination of mass attenuation coefficients (μm) and transmission factors (TF) of Magnesium oxide (MgO) and Zinc oxide (ZnO) samples. The calculated values for mass attenuation coefficients (μm) were utilized to determine other vital shielding properties against gamma-ray radiation. Moreover, the results showed that Zinc oxide (ZnO) nanoparticles with the lowest diameter value as 50 nm had a satisfactory capacity in nuclear radiation shielding.

Advanced Method for Determination of Omeprazole in Plasma by HPLC

  • Kang, Won-Ku;Kim, Dong-Sup;Kwon, Dwang-Il
    • Archives of Pharmacal Research
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    • 제22권1호
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    • pp.86-88
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    • 1999
  • An advance d and sensitive high-performance liquid chromatographic (HPLC) method for determination of omeparzole in human plasma has been developed. After omeprazole was extracted from plasma with diethylether, the organic phase was transferred to another tube and trapped back with 0.1 N NaOH solution. The alkaline aqueous layer was injected into a reversed-phase C8 column. Lansoprazole was used as an internal standard. The mobile phase consisted of 30% of acetonitrile and 70% of 0.2 M $ KH_{2}PO_{4}$, pH 7.0. Recoveries of the analytes and internal standard were >75.48%. The coefficients of variation of intra- and inter-day assay were <5.78 and 4.59% for plasma samples. The detection limit in plasma was 2 ng/ml. The clinical applicability of this assay method was evaluated by determining plasma concentration-time courses of the respective analytes in 24 healthy volunteers after oral administration 40 mg of omeprazole. The present assay is considered to be simple, accurate, economical and suitable for the study of the kinetic disposition of omeprazole in the body.

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Nondestructive and Rapid Estimation of Chlorophyll Content in Rye Leaf Using Digital Camera

    • 한국작물학회지
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    • 제49권1호
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    • pp.41-45
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    • 2004
  • We have developed and tested a new method for nondestructive estimation of chlorophyll- and nitrogen-contents in rye leaf. It was found that the relation-ships among nitrogen, chlorophyll content and fresh weight were significantly positive correlated. Nitrogen and chlorophyll content were positively correlated whereas correlation coefficients among R, G, R-B and G-B on the basis of photo-numerical values were negative. We have found that R/(R-B) obtained from data of digital camera is the best criterion to estimate the chlorophyll content of leaves. The regression curves of the relation between R/(R-B) and chlorophyll content were also calculated from the data collected on cloudy days. The coefficients of determination ($\textrm{r}^2$) were ranged from 0.33 to 0.99. In this study, the accuracy in estimating chlorophyll content from the color data of digital camera image could be improved by correcting with R, G, and B values. It is suggested that, for practical purposes, the image values estimated with sufficient accuracy using a portable digital camera can be applied for determining chlorophyll content and nitrogen status in plant leaves.

Mean wind loads on T-shaped angle transmission towers

  • Guohui Shen;Kanghui Han;Baoheng Li;Jianfeng Yao
    • Wind and Structures
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    • 제38권5호
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    • pp.367-379
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    • 2024
  • Compared with traditional transmission towers, T-shaped angle towers have long cross-arms and are specially used for ultrahigh-voltage direct-current (UHVDC) transmission. Nevertheless, the wind loads of T-shaped towers have not received much attention in previous studies. Consequently, a series of wind tunnel tests on the T-shaped towers featuring cross-arms of varying lengths were conducted using the high-frequency force balance (HFFB) technique. The test results reveal that the T-shaped tower's drag coefficients nearly remain constant at different testing velocities, demonstrating that Reynolds number effects are negligible in the test range of 1.26 × 104-2.30 × 104. The maximum values of the longitudinal base shear and torsion of the T-shaped tower are reached at 15° and 25° of wind incidence, respectively. In the yaw angle, the crosswind coefficients of the tower body are quite small, whereas those of the cross-arms are significant, and as a result, the assumption in some load codes (such as ASCE 74-2020, IEC 60826-2017 and EN 50341-1:2012) that the resultant force direction is the same as the wind direction may be inappropriate for the cross-arm situation. The fitting formulas for the wind load-distribution factors of the tower body and cross-arms are developed, respectively, which would greatly facilitate the determination of the wind loads on T-shaped angle towers.

Determination of lateral strength and ductility characteristics of existing mid-rise RC buildings in Turkey

  • Ucar, Taner;Merter, Onur;Duzgun, Mustafa
    • Computers and Concrete
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    • 제16권3호
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    • pp.467-485
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    • 2015
  • This paper presents a comprehensive work on determination of yield base shear coefficient and displacement ductility factor of three to eight story actual reinforced concrete buildings, instead of using generic frames. The building data is provided by a walkdown survey in different locations of the pilot areas. Very detailed three dimensional models of the selected buildings are generated by using the data provided in architectural and reinforcement projects. Capacity curves of the buildings are obtained from nonlinear static pushover analyses and each capacity curve is approximated with a bilinear curve. Characteristic points of capacity curve, the yield base shear capacity, the yield displacement and the ultimate displacement capacity, are determined. The calculated values of the yield base shear coefficients and the displacement ductility factors for directions into consideration are compared by those expected values given in different versions of Turkish Seismic Design Code. Although having sufficient lateral strength capacities, the deformation capacities of these typical mid-rise reinforced concrete buildings are found to be considerably low.

인체 혈장에서 염산시프로플록사신(시프로플록사신으로서 250 mg) 정량을 위한 HPLC 분석법의 유효성검토 (Validation of a Simple HPLC Method for Determination of Ciprofloxacin Hydrochloride in Human Plasma)

  • 하용화;조성희;천성국;서성훈;류재환;최영욱;이경태
    • Journal of Pharmaceutical Investigation
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    • 제34권4호
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    • pp.327-331
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    • 2004
  • A simple HPLC method with ultraviolet detection of ciprofloxacin in human plasma was developed and validated. After protein precipitation with trichloroacetic acid, chromatographic separation of ciprofloxacin in plasma was achieved at $50^{\circ}C$ with a $C_{18}$ column and methanol-phosphate mixture (pH 2.5), as mobile phase. Quantitative determination was performed by ultraviolet detection at 278 nm. The method was specific and validated with a limit of quantification of 100 ng/ml. The intra- and inter-day coefficients of variation were between 1.67% and 10.55% and accuracy between 92.01 % and 106.09%. The method has been successfully applied in a bioavailability study of 250 mg ciprofloxacin hydrochloride tablet.

능이버섯의 건조 방정식 (Drying Equations of Sarcodon Aspratus)

  • 금동혁;노정근;정태영;홍성렬;박기문;김훈;한재웅
    • Journal of Biosystems Engineering
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    • 제29권1호
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    • pp.59-64
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    • 2004
  • This study was performed to determine drying equations of sarcodon aspratus. Drying tests for sarcodon aspratus were conducted in an experimental dryer equiped with an air conditioning unit. The drying tests were performed at three air temperatures of 30$^{\circ}C$, 40$^{\circ}C$ and 50$^{\circ}C$, and two relative humidities of 30% and 50%. Measured moisture ratio data were fitted with the selected four drying models(Page, Thompson, Lewis and simplified diffusion models) using stepwise multiple regression analysis. When the coefficients of determination and root mean square errors of moisture ratio were evaluated for four drying models, the Page model was found to fit adequately to all the drying test data with coefficient of determination of 0.9996 and RMSE of 0.00523.

HPLC를 이용한 랫트 혈장중의 딜타아젬 및 데아세틸딜티아젬의 정량 (HPLC Determination of Diltiazem and Deacetyldiltiazem in Rat Plasma)

  • 이용희;심창구;이민화;김신근
    • Journal of Pharmaceutical Investigation
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    • 제22권4호
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    • pp.317-321
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    • 1992
  • A high-performance liquid chromatographic (HPLC) method was developed for the determination of diltiazem (DTZ) and its major metabolite, deacetyldiltiazem (DAD), in rat plasma. DTZ, DAD and imipramine, the internal standard, were selectively fractionated from plasma on a $C_{18}$ reversedphase column $({\mu}-Bondapak,\;10\;{\mu}m\;silica,\;300{\times}3.9\;mm\;ID)$. The composition of the mobile phase was methanol: acetonitrile: 0.04 M ammonium bromide: triethylamine (40:24:36:0.06 in volume). The pH of the mobile phase of their method was lowered to 6.4. The eluents from the column were detected for DTZ and DAD using a UV detector at 237 nm. The recovery was >85% for DTZ and DAD, and average intra-day and inter-day coefficients of variation were <6% for DTZ and DAD at the concentration ranges of 20-1000 ng/ml. Detection limit of DTZ and DAD in plasma was 20 ng/ml with signal-to-noise ratio of 3. This method would be applicable to practical pharmacokinetic studies without detriment to the HPLC column.

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An Analysis and Evaluation of the Effectiveness of Decision Making During the Review of Scientifically Constructed Project Proposals

  • Abdykerova, G.Zh;Bukayeva, A.D.
    • 벤처창업연구
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    • 제3권2호
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    • pp.31-44
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    • 2008
  • A selection technique for innovative projects on the beginning stage has been presented in this article. It can be applied in projects assessment in HEI, enterprises, development institutes, etc. It is rather difficult to assess the project quality on the beginning stage of R&D due to the uncertainty in the technical and economic indices but the new development analysis on this stage is of a great interest. By innovative project quality as a management object we will mean those characteristics relating to the results capacity of the projects and its realization process to satisfy the requirements to the innovative products competitiveness and their innovative attractiveness for investors. The most important question in the innovative projects management is the determination of its quality level under modern conditions. The aim of the research is to analyze and evaluate the decision making during the project management process. The objectives and hypotheses are assessment of an innovative project with the application of McKinsey's model is better to realizes by 3 stages: a) selection of optimal criteria; b) determination of weighing coefficients; c) projects positioning in a matrix.

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곡류 및 버섯류의 평형함수율 및 박층건조방정식에 관한 연구(I) -벼의 박층건조방정식 - (Equilibrium Moisture Contents and Thin Layer Drying Equations of Cereal Grains and Mushrooms (I) - Thin Layer Drying Equations of Short Grain Rough Rice -)

  • 금동혁;박춘우
    • Journal of Biosystems Engineering
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    • 제22권1호
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    • pp.11-20
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    • 1997
  • Thin layer drying tests of short gain rough rice were conducted in an experimental dryer equiped with air conditioning unit. The drying tests were performed in triplicate at three air temperatures of $35^circ$, $45^circ$, $55^circ$, and three relative humidities of 40%, 55%, 70%, respectively. Previously published thin layer equations were reviewed and four different models widely used as thin layer drying equations for cereal grains were selected. The selected four models were Pages, simplified diffusion, Lewis's and Thompson's models. Experimental data were fitted to these equations using stepwise multiple regression analysis. The experimental constants involved in tow equations were represented as a function of temperature and relative humidity of drying air. The results of comparing coefficients of determination and root mean square errors of miosture ratio for low equations showed that Page's and Thompsons models were found to fit adequately to all drying test data with coefficient of determination of 0.99 or better and root mean square error of moisture ratio of 0.025.

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