• 제목/요약/키워드: chemical testing

검색결과 824건 처리시간 0.025초

Analysis of the utilization of existing test data for phase-in substance registration under the Act on the Registration and Evaluation, etc. of Chemical Substances

  • Choi, Bong-In;Kwak, Yeong-Don;Jung, Yu-Mi;Ryu, Byung-Taek;Kim, Chang Gyun
    • Environmental Analysis Health and Toxicology
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    • 제30권sup호
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    • pp.4.1-4.7
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    • 2015
  • Objectives Approximately 2000 phase-in substances are subject to registration according to the Act on the Registration and Evaluation, etc. of Chemical Substances (K-REACH), and the expected testing cost is 2.06 trillion Korean won assuming all the test data required for registration are acquired. The extent to which these enormous test costs can be reduced depends on the availability of existing data that can be used to meet the requirements of the K-REACH we examined the current availability of test data that can be used for chemical substance registration. Methods We analyzed the possibility of utilizing the existing test data obtained from 16 reference databases for 369 of 518 kinds of phase-in substances subject to registration that were reported in last October 2014. Results The physical and chemical properties were available for 57.1% of substances, whereas data regarding human hazards and environmental hazards were available at considerably lower rates, 8.5% and 11.8%, respectively. Conclusions Physical and chemical properties were available for a fairly high proportion, whereas human hazards and environmental hazards were reported for considerably fewer substances.

Study on Properties and Accelerated Life-time Test of Rubber O-ring by Temperature Stress

  • Shin, Young-Ju;Kang, Bong-Sung;Chung, Yu-Kyung;Choi, Kil-Yeong;Shin, Sei-Moon
    • 한국신뢰성학회:학술대회논문집
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    • 한국신뢰성학회 2006년도 학술발표대회 논문집
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    • pp.48-54
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    • 2006
  • In this thesis, accelerated life test (ALT) method and procedure for rubber O-ring are applied to assure specified reliability of the products at guaranteeing the life of the products. Rubber O-ring is parts that keep intensity or make machine operation smoothly on attrition portion of machine and is used to prevent that oil is leaked. Usually. Rubber O-ring used NBR that is copolymer of acrylonitrile and butadiene. this are superior oil resistance, heat resistance, durability of abrasion, cold resistance, chemical resistance etc. The accelerated life test model for rubber O-ring are developed using the relationship between stresses and life characteristics of products. Using the accelerated life test method and the acceleration life test equipment which is developed, we performed life test, collected life data and analyzed the results of tests. The proposed accelerated life test method and procedure may be extended and applied to testing similar kinds of products to reduce test times and costs of the tests remarkably.

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LDPE 중 PFOS의 분석법 개발과 비교숙련도 결과 (Determination of PFOS in LDPE and the Result for Proficiency Testing)

  • 정재학;이영규;명승운;정남용
    • 대한화학회지
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    • 제57권1호
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    • pp.40-51
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    • 2013
  • 전기전자 부품 및 제품상에서 주로 사용되는 Plastic 중 함유된 Perfluorooctanesulfonic acid (PFOS)의 정량 분석법을 개발하기 위해 LDPE 시료를 대상으로 soxhlet 용매추출과 액체크로마토그래피/질량분석법(LC/MS)을 사용하여 시험방법 유효화를 진행하였다. 그 결과 검출한계(LOD)와 정량한계(LOQ)는 각각 $2.58{\mu}g/L$, $7.82{\mu}g/L$였으며, 회수율은 96-102%를 나타내었다. LC/MS의 검량선은 $7.82-100{\mu}g/L$ 농도범위에서 $r^2$값 0.9992의 직선성을 확인하였다. 또한 EU 환경규제 대응을 위한 전기전자 제품 중의 PFOS 분석법 표준화를 위해서 국내외 시험기관을 대상으로 비교숙련도 시험을 실시하였다. 그 결과 참여한 10개 시험기관 중 3개 시험기관이 이상값을 제출하였다. 이에 $^{19}F$ 핵자기공명분광분석법($^{19}F$ NMR)을 사용하여 이상값의 원인을 규명한 결과 그 주요 원인이 표준시약 및 시료 중에 존재하는 PFOS 이성질체들에 대한 결과처리의 오류였음을 확인하였다.

Ecotoxicological effects of ballast water effluent teated by an electrolytic method on marine environment

  • Kim, Tae Won;Kim, Keun-Yong;Shon, Myung-Baek;Kim, Young-Soo;Lee, Ji Hyun;Moon, Chang Ho;Son, Min Ho
    • Journal of Advanced Marine Engineering and Technology
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    • 제38권8호
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    • pp.1010-1020
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    • 2014
  • Ballast water effluent treated by an electrolytic method contains reactive chlorine species and disinfection by-products (DBPs). In this study, we conducted whole effluent toxicity (WET) testing and ecological risk assessment (ERA) to investigate its ecotoxicological effects on marine environment. WET testing was carried out for three marine pelagic organisms, i.e., diatom Skeletonema costatum, rotifer Brachionus plicatilis and fish Paralichthys olivaceus. The biological toxicity test revealed that S. costatum was the only organism that showed apparent toxicity to the effluent; it showed no observed effect concentration (NOEC), lowest observable effect concentration (LOEC) and effect concentration of 50% (EC50) values of 12.5%, 25.0% and 83.3%, respectively, at brackish water condition. In contrast, it showed insignificant toxicity at seawater condition. B. plicatilis and P. olivaceus also showed no toxicities to the effluent at the both salinity conditions. Meanwhile, chemical analysis revealed that the ballast water effluent contained total residual oxidants (TROs) below $0.03{\mu}g/L$ and a total of 20 DBPs including bromate, volatile halogenated organic compounds (VOCs), halogenated acetonitriles (HANs), halogenated acetic acids (HAAs) and chloropicrin. Based on ERA, the 20 DBPs were not considered to have persistency, bioaccumulation and toxicity (PBT) properties. Except monobromoacetic acid, the ratio of predicted environmental concentration (PEC) to predicted no effect concentration (PNEC) of the other 19 DBPs did not exceed 1. Thus, our results of WET testing and ERA indicated that the ballast water effluent treated by electrolysis and subsequently neutralization was considered to have no adverse impacts on marine environment.

다중채널 와전류탐상검사 장치 개발(II) (Development of a Multichannel Eddy Current Testing Instrument(II))

  • 이희종;남민우;조찬희;유현주;김인철
    • 비파괴검사학회지
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    • 제31권5호
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    • pp.552-559
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    • 2011
  • 전자기유도(electromagnetic induction) 현상을 이용한 비파괴진단기법으로서 최근까지 와전류탐상기법, 교류장측정기법, 자속누설검사기법, 그리고 원격장검사기법 등이 개발되어 활용되고 있다. 이 기법 중 와전류탐상기법은 오늘날 발전설비, 화학, 조선 및 군수설비 등의 열교환기 전열관 비파괴검사에 널리 적용되고 있다. 와전류탐상검사 시스템의 구성은 기능별로 와전류신호 합성 모듈, 아날로그 모듈, 디지털 신호처리를 위한 아날로그-디지털 변환 모듈, 전원공급장치 및 신호취득 평가 프로그램 등으로 구성되며, 선행 연구(I)에서는 다중채널방식의 와전류탐상검사 시스템의 구성 요소 중 1차로 와전류신호 합성 모듈, 아날로그 모듈을 설계 개발하였으며, 2차로 와전류 신호 취득 평가 프로그램을 개발하였다. 2차 연구에서 개발한 와전류 신호취득 평가 프로그램의 운영체제는 "Windows 7"로서 국내 사용자를 위해 최적화 하였으며, 주요 특징은 검사자가 "setup wizard"를 이용하여 검사에 필요한 검사 조건 및 변수를 용이하게 설정하고 이를 이용하여 신호취득 및 평가를 수행할 수 있다. 본 논문에서는 개발된 와전류신호 수집 및 평가 프로그램의 구성과 각 기능을 설명하고자 한다.

다중채널 와전류탐상검사 장치 개발(I) (Development of a Multichannel Eddy Current Testing Instrument(I))

  • 이희종;남민우;조찬희;윤병식;조현준
    • 비파괴검사학회지
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    • 제30권2호
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    • pp.155-161
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    • 2010
  • 전자기유도(electromagnetic induction) 현상을 이용한 비파괴진단기법으로 최근까지 와전류탐상기법, 교류장측정기법, 자속누설검사기법, 그리고 원격장검사기법 등이 개발되어 활용되고 있었다. 이 기법중 와전류탐상기법은 오늘날 발전설비, 화학, 조선 및 군수설비 등의 열교환기 전열관 비파괴검사에 널리 적용되고 있다. 와전류탐상검사 시스템의 구성은 기능별로 와전류신호 합성 모듈, 아날로그 모듈, 디지털 신호처리를 위한 아날로그-디지털 변환 모듈, 전원공급장치 및 신호취득 평가 프로그램 등으로 구성되며, 본 연구에서는 다중채널방식의 와전류탐상검사 장치(하드웨어) 개발에 필요한 구성 요소중 1차적으로 와전류신호 합성 모듈, 아날로그 모듈을 설계 개발하였다. 본 연구에서 개발한 와전류탐상검사 장치의 특정은 주파수영역 및 시간영역 다중화 방식에 의한 최대 4개 주파수의 동시 적용이 가능한 다중채널장치이다. 와전류신호 합성 모듈, 아날로그 모듈을 구성하는 각 회로에서 와전류신호 발생, 변조, 전처리, 변조 및 신호 디스플레이를 위한 신호가 적절하게 처리되어 최종적으로 와전류신호 평가에 필수적인 리사쥬신호가 임피던스 평면 내에 디스플레이 되는 것을 확인하였다.

공단지역에서 대기중 총 부유분진의 입자크기 분포와 화학적 성분에 관한 분석과 연구 (A Study on the Size Distribution and Chemical Composition of total Suspended Particulates at Industrial Region)

  • 박흥재;이성욱;박원우
    • 한국환경과학회지
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    • 제2권3호
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    • pp.201-206
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    • 1993
  • The concentration of Total Suspended Particulates(T.S.P), size distribution of suspended particulates, and soluble anions of T.S.P in atmosphere of industrial region in Busan were investigated. T.S.P was measured by High-Volume Air Sampler and particle size distribution was measured by Anderson Air Sampler. We analyzed the chemical component of the T.S.P by ion Chromatography and measure4 the shape and size of T.S.P by Scanning Electron Micrography The small size of T.S.P mainly exist in industrial region, but the large size of T.S.P mainly exist in residentail area.

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Alternative Finishing Process for Poly(ethylene terephthalate)(PET) Tire Cord using Atmospheric Plasma

  • Kim, Sam-Soo;Song, Eun-Young;Cho, Dong-Lyun;Park, Jun;Park, Sung-Ho;Lee, Jae-Woong
    • 한국염색가공학회지
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    • 제22권4호
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    • pp.300-305
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    • 2010
  • Poly(ethylene terephthalate)(PET) tire cord has relatively lower adhesion properties caused by limited reacting sites. In order to improve the adhesion force between PET tire cord and rubber, an additional process to activate surface of PET has been employed. Atmospheric plasma was used to substitute the chemical finishing process of PET tire cord as a green dipping process. Contact angle was measured to confirm surface change of PET after plasma treatment. The treated PET tire cords with/without resorcinol-formaldehyde-latex(RFL) and unvulcanized rubber were vulcanized in a testing mold at $160^{\circ}C$. After atmospheric plasma treatment of PET tire cord, adhesion force was somewhat increased under some conditions.

The Effect of Soil Physico-chemical Properties on Rhizome Rot and Wilt Disease Complex Incidence of Ginger Under Hill Agro-climatic Region of West Bengal

  • Sharma, B.R.;Dutta, S.;Roy, S.;Debnath, A.;Roy, M. De
    • The Plant Pathology Journal
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    • 제26권2호
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    • pp.198-202
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    • 2010
  • A study was conducted to find out the relationship of physico-chemical properties (viz. organic carbon(OC), pH, electrical conductivity, nitrogen, phosphorus and potassium content) of ginger growing soil with incidence percentage of rhizome rot and wilt disease complex of ginger. Organic carbon content and pH of the ginger soil contributed significantly (93%) in the prediction of ginger rhizome rot and wilt disease complex incidence with negative correlation. Soil having weak acidic reaction with OC percent greater than 2.25 was observed to have the lower average incidence of the disease.

Oxidation Stability of PAO Oils Determined by Differential Scanning Calorimetry

  • Shim, Joosup;Cho, Wonoh;Chung, Keunwo
    • Tribology and Lubricants
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    • 제12권1호
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    • pp.36-41
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    • 1996
  • The suitability of a pressure differential scanning calorimetry (PDSC) in monitoring the quality of synthetic base fluids has been investigated using polyalphaolefin (PAO) oils as an example. Induction period meassured at 170, 180 and 19$0^{\circ}C$, and 3.53 MPa oxygen pressure was applied to characterize their oxidation stability. The PDSC method has proven to be simple and repeatable and requires only small sample size for testing. More importantly, it can be applied in differentiating the oxidation performance quality of PAO oils and is versatile enough for use in studying kinetic aspects of PAO oil oxidation which include the effect of temperature and antioxidant concentration. Additionally, the method appears to correlate well with a rotary bomb oxidation test (RBOT).