• Title/Summary/Keyword: chemical composition analysis

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Dyeability with Silk Fabrics and Chemical Composition of Natural Dye PinuxTM Manufactured from Pinus Radiata Balk (라디아타 소나무 수피로부터 제조한 PinuxTM염료의 화학조성과 견섬유와의 염색성)

  • Song, Kyung-Hun;Mun, Sung-Phil;Kim, Dae-Sung;Hong, Young-Ki
    • Korean Journal of Human Ecology
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    • v.18 no.6
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    • pp.1315-1321
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    • 2009
  • The chemical composition of natural powder dye $Pinux^{TM}$ manufactured from Pinus radiata bark and dyeability of dyed silk fabrics with $Pinux^{TM}$ were examined. It is made up of the optimum dyeing condition of silk fabric according to the dyeing concentration, dyeing time, and dyeing temperature. Also, we examined the colorfastness and antibiosis of dyed silk fabrics to washing, rubbing, perspiration and light. For the analysis of the chemical composition of $Pinux^{TM}$, the total contents of phenolic compound, proanthocyanidin(PA) and anti-oxidative activities of the dye were analyzed. As a result, it was found that the main components of the $Pinux^{TM}$ manufactured from Pinus radiata bark is proanthocyanidin, mostly a flavonoid containing a procyanidin structure, and it consists of approximately 63% phenol. As a result of examining the dyeability of silk fabrics with $Pinux^{TM}$, it showed that the dyeability was best under the conditions of the concentration of dye $1{\sim}1.5%$(wt/v%), dyeing time of 90 minutes, and dyeing temperature at $90^{\circ}C$. It was found that the colorfastness of dyed silk fabrics, colorfastness to washing, perspiration for acidic and rubbing were as good as grade 4 or 4-5. However, the colorfastness to light was low at grade 1, the same as the results of other natural dyed fabrics. As a result of the antibiosis measurement for the $Pinux^{TM}$-dyed silk fabrics, it showed high antibacterial properties to Staphylococcus sureus at 99.6%.

Properties of the Chemical Composition of Safflower (Carthamus tinctorius L.) sprout (홍화(Carthamus tinctorius L.) 순의 이화학적 특성)

  • 김성규;차재영;정순재;정정한;최용락;조영수
    • Journal of Life Science
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    • v.10 no.1
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    • pp.68-73
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    • 2000
  • In order to develop new materials for the functional food, the components of safflower(Carthamus tinctorius L.) sprout was studied. Chemical composition, minerals, amino acids, and fatty acids of the leaf and the stem parts of 2 weeks grown safflower sprout were analyzed. The chemical composition of safflower spout was 12.7% (w/w) moisture, 28.5% crude protein, 10.1% crude fat, and 5.3% crude ash. Mineral contents of the leaf part were P 49%, K 22%, Mg 15%, Ca 10% whereas these of the stem part were K 51%, P 27%, S 10%, Ca 7%, Mg 4%. Other mineral contents were less than 2% in both parts. Especially, Pt was 0.18 ppb and 0.17 ppb in the leaf and the stem parts, respectively. The composition of the amino acid were approximately as follow, the major amino acid in the leaf and the stem were aspartic acid and glutamic acid, the contents of these were 10.7mg/g, 10mg/g in the leaf, 11.3 mg/g, 8.4 mg/g in the stem, respectively. The major fatty acids in the leaf and the stem parts were linoleic acid and $\alpha$-linolenic acid. The linoleic acid (C18:2) in the leaf and the stem parts were 67% (w/w) and 47% whereas the $\alpha$-linolenic acid. The linoleic acid (C18:2) in those parts were 14% (w/w) and 11%, respectively. On the basis of chemical analysis, the safflower sprout showed to have relatively high contents of crude protein and crude fat, minerals including small amount of Pt, polyunsaturated fatty acid as linoleic acid and $\alpha$ -linolenic acid. These results suggested that safflower sprout was found to be a useful material of natural health food for the functional food development.

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Biomineralization Strategy of Biocomposites on Regenerated Shell: Chitin Synthesis and Regenerated Shell Formtation by Deformed Oyster Shell (생체복합체의 재생패각 합성전략: 참굴 패각의 변형에 따른 키틴 합성 및 패각재생)

  • Lee, Seungwoo;Park, Seungbin;Yeong, Donghee;Choi, Cheongsong
    • Korean Chemical Engineering Research
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    • v.46 no.3
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    • pp.529-534
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    • 2008
  • The normal shell and the regenerated oyster shell, Crassostrea gigas, are separated according to the characteristics of inner shell morphology. To study characteristics of chitin obtained from the regenerated shell, chitin prepared by acid and alkali process is analyzed by FT-IR (Fourier transform infrared spectrometer) and XRD (X-ray Diffractometer). The content of insoluble protein in the normal shell was more than doubled as compared with that in the regenerated shell. A comparison of secondary structure of the normal shell and the regenerated shell revealed that the content of random of the regenerated shell was above 47%, indicating an amount in the structural unordered state. Through amino acid composition analysis and secondary protein structure of soluble protein isolated from the normal shell and the regenerated shell, it was found that there are differences in biomineralization strategy of the regenerated shell as compared to the normal shell. The relatively low hardness of the regenerated shell is caused by the change of amino acid composition and ordered secondary protein structure as compared to hardness of the normal shell.

A Study on the Granulometry and Chemical Composition of Psudo-Gleized Soil in Jeongdongjin Area (정동진 의사글레이층의 입도와 화학 조성에 대한 연구)

  • Kim, Jong Yeon
    • Journal of The Geomorphological Association of Korea
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    • v.24 no.3
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    • pp.27-45
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    • 2017
  • At the upper part of terrace deposits at Jeongdongjin area, there is a structure in which reddish brown and grayish white layers laying horizontally. Previous studies have reported the existence of these structures within the deposits and suggested the theoretical background related to the formation process. However, the analysis of physical properties and chemical composition such as particle size, classification, etc. of the materials constituting the reddish brown and grayish white layers is scarcely done. In this study, the physico - chemical properties of gray - white and reddish brown beds are investigated. The mean grain size of the particles was less than $4{\varphi}$ in both layers and the reddish brown layer was more coarse. The results shows that the sorting of the grayish white layer is better. The chemical composition of both layers shows that the average concentration of $SiO_2$, $Al_2O_3$ and $K_2O$ of the grayish white layer was higher than those of the reddish brown layer. The concentration of $Fe_2O_3$ of reddish brown lyaer was 3 times higher than those of the grayish white layer. The degree of chemical weathering (CIA) is 90 or so in both the reddish brown and grayish white layers, indicating a significant level of chemical weathering. In conclusion, reddish brown layers had been formed by the processes related to the migration of iron and the migration of water that induced aggregation after the formation of sediments (psudo-gleization). In this study area, a vertical layer of grayish white which cuts off horizontal reddish brown and grayish white color was found. The vertical layer or wedge similar to a ice-wedge or columnar structure that in a cold environment, and there is a difference in shape and size. The vertical layer appears to have occurred three or more cycles. The vertical layers begin to form at a certain height within the outcrop and descend downwards, which of course is difficult to see as directing certain times.

Characterization of the microbial communities along the gastrointestinal tract of sheep by 454 pyrosequencing analysis

  • Wang, Jin;Fan, Huan;Han, Ye;Zhao, Jinzhao;Zhou, Zhijiang
    • Asian-Australasian Journal of Animal Sciences
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    • v.30 no.1
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    • pp.100-110
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    • 2017
  • Objective: The gastrointestinal tract of sheep contain complex microbial communities that influence numerous aspects of the sheep's health and development. The objective of this study was to analyze the composition and diversity of the microbiota in the gastrointestinal tract sections (rumen, reticulum, omasum, abomasum, duodenum, jejunum, ileum, cecum, colon, and rectum) of sheep. Methods: This analysis was performed by 454 pyrosequencing using the V3-V6 region of the 16S rRNA genes. Samples were collected from five healthy, small tailed Han sheep aged 10 months, obtained at market. The bacterial composition of sheep gastrointestinal microbiota was investigated at the phylum, class, order, family, genus, and species levels. Results: The dominant bacterial phyla in the entire gastrointestinal sections were Firmicutes, Bacteroidetes, and Proteobacteria. In the stomach, the three most dominant genera in the sheep were Prevotella, unclassified Lachnospiraceae, and Butyrivibrio. In the small intestine, the three most dominant genera in the sheep were Escherichia, unclassified Lachnospiraceae, and Ruminococcus. In the large intestine, the three most dominant genera in the sheep were Ruminococcus, unclassified Ruminococcaceae, and Prevotella. R. flavefaciens, B. fibrisolvens, and S. ruminantium were three most dominant species in the sheep gastrointestinal tract. Principal Coordinates Analysis showed that the microbial communities from each gastrointestinal section could be separated into three groups according to similarity of community composition: stomach (rumen, reticulum, omasum, and abomasum), small intestine (duodenum, jejunum, and ileum), and large intestine (cecum, colon, and rectum). Conclusion: This is the first study to characterize the entire gastrointestinal microbiota in sheep by use of 16S rRNA gene amplicon pyrosequencing, expanding our knowledge of the gastrointestinal bacterial community of sheep.

Optimization for Scenedesmus obliquus Cultivation: the Effects of Temperature, Light Intensity and pH on Growth and Biochemical Composition

  • Zhang, Yonggang;Ren, Li;Chu, Huaqiang;Zhou, Xuefei;Yao, Tianming;Zhang, Yalei
    • Microbiology and Biotechnology Letters
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    • v.47 no.4
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    • pp.614-620
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    • 2019
  • Microalgae have been explored as potential host species for biofuel production. Environmental factors affect algal growth and cellular composition. The effects of several key environmental factors, such as temperature, light, and pH of the medium on the growth and biochemical composition of Scenedesmus obliquus were investigated in this study. The highest growth rate of microalgae was observed at an optimal temperature of 25℃, 150 μmol/(m2·s) light intensity, and pH 10.0. The biochemical composition analysis revealed that the carbohydrate content decreased at lower (20℃) or higher temperature (35℃), whereas the protein and lipid contents increase at these temperatures. The fluctuation of light intensity significantly affected the contents of protein, carbohydrate, and lipid. The protein levels varied greatly when the pH of the medium was below 7.0. The carbohydrate and lipid contents significantly increased at pH above 7.0.

Experimental Research of Piece-Mold Casting: Gilt-Bronze Pensive Bodhisattva

  • Yun, Yong-Hyun;Cho, Nam-Chul;Doh, Jung-Mann
    • Journal of Conservation Science
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    • v.37 no.4
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    • pp.340-356
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    • 2021
  • We have tried the experimental research of lost-wax casting to reconstruct Gilt-Bronze Pensive Bodhisattva; preliminary and reconstruction experiment based on ancient texts. Main object to reconstruct is Korean National Treasure No.83, Gilt-Bronze Pensive Bodhisattva (Maitreya), then we measure alloy ratio and casting method based on the scientific analysis. Other impurities were removed from the base metal components(copper : tin : lead) and their ratio was set to 95.5 : 6.5 : 3 where the ratios for tin and lead were increased by 2.5% each. The piece-mold casting method was used, and piece-mold casting experiments were carried out twice in this study but supplementary research on piece-mold casting was necessary. The microstructure was confirmed to be typical cast microstructure and the component analysis result was similar to that of the prior study. Analysis of the chemical composition is confirmed to copper, tin, lead, and zinc, and the chemical composition of the matrix was 87.8%Cu-7.5%Sn-2.7%Pb-2.1%Zn, and similar to previous experimental research. Also resulted in the detection of small impurity in Zn. Analysis of the mould revealed that the mould was fabricated by adding quartz and organic matter for structural stability, fire resistance, and air permeability. We expect that our research will contribute to provide base data for advanced researches in future.

Chemical Compositional Distribution of Ethylene-1-Butene Copolymer Prepared with Heterogeneous Ziegler-Natta Catalyst: TREF and Crystaf Analysis

  • Ko, Young-Soo;Jeon, Jong-Ki;Yim, Jin-Heong;Park, Young-Kwon
    • Macromolecular Research
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    • v.17 no.5
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    • pp.296-300
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    • 2009
  • Ethylene-1-butene copolymers were prepared with $SiO_2$-supported $TiCl_4$ catalyst by changing of 1-butene/ethylene molar ratio in feed, and the resulting copolymers were analyzed using temperature rising elution fractionation (TREF) and crystallization fractionation (Crystaf) methods to investigated the influence of $C_4/C_2$ molar ratio in feed on chemical compositional distribution and other parameters such as molecular weight and its distribution. TREF analysis showed that the copolymers had a broad and bimodal chemical compositional distribution (CCD) regardless of the content of 1-butene in the copolymer. The chemical composition was in the range of 5 to 55 branches per 1,000 carbons for all copolymers prepared in the study. Furthermore, the broader CCD was revealed for the copolymers having the higher content of 1-butene. Crystaf analysis did not showed a bimodal CCD for the copolymers having the 1-butene content of less than 5.1 wt%. The lower crytalline part having 1-butene content in Crystaf analysis was less than of TREF analysis.

음성지역 지하수의 수리화학적 특성에 대한 심도, 모암 및 광화대의 영향

  • 정찬호;이병대;성익환;조병욱
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2004.04a
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    • pp.492-494
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    • 2004
  • The purpose of this study is to investigate the hydrochemical characteristics of groundwater in the Umsung area, and to elucidate the effect of host rock type, well depth and mineralization zone on the groundwater chemistry, We carried out chemical analysis, isotopic analysis, statistical analysis of Box-Whisker and trigging analysis for this study. The chemical and isotopic compositions of the groundwater is distinguished into two areas according to host rocks(Cretaceous sedimentary rocks and Jurassic granite) and recharge altitude, and is not greatly influenced by mineralization zone of the mines.

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Mineralogical and Chemical Variation in Weathering Profile on Ultramafic Rocks During Vermiculitization (질석화가 진행된 풍화단면에서의 광물조성과 주원소의 변화)

  • Moon, Hi-Soo;Song, Yungoo;Sin, Sang Eun
    • Economic and Environmental Geology
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    • v.26 no.1
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    • pp.29-40
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    • 1993
  • Several vermiculite deposits occur as the alteration product from phlogopite in ultramafic rock, in the Hongseong and Cheongyang area, South Korea. Some quarries show well-defined weathering profile. Samples collected from those quarries were examined by XRD and chemistry to define a vertical variations in mineralogy and chemistry of the weathering profile developed on ultramafic rocks. The analysis by X-ray diffractometry showed that mineral compositions changed continuously as depth of profile increasing, the vermiculite-the phlogopite/vermiculite interstratified-the phlogopite. Chemical analysis of bulk samples in altered zone revealed that regardless of composition and kinds of mineral in the rock, there are significant increase of MgO, CaO and $H_2O$, and decrease of K as depth of profile decrease reflecting the characteristics in vermiculitization. Also, there was a tendency that weathering indicies of each sample horizon change gradually with increasing depth. This tendency can be explained as variations of degree of vermiculitization. The regular changes of mineralogical and chemical composition in vertical profile suggest that weathering is the most important process in vermiculitization in this area.

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