• 제목/요약/키워드: central mixing composite design

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건조 찹쌀가루를 이용한 오븐구이 찰떡의 관능적.물리적 최적화 (반응 표면 분석법을 이용) (Optimization of the Sensory and Physical Properties of Oven-Roasted Glutinous Rice Cakes Prepared with Dry Glutinous Rice Flour (By Response Surface Methodology))

  • 김경미;김옥선;김종군
    • 동아시아식생활학회지
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    • 제17권6호
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    • pp.883-893
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    • 2007
  • To optimize the preparation process for oven-roasted glutinous rice cake, an experiment was derived using a central mixing composite design to determine the optimal conditions. The addition of flour by soaking time as well as sucrose and water, were the independent variables, with the moisture content, color, sensory, and texture properties of the ovenroasted glutinous rice cakes selected as response variables. For the moisture content, color, sensory, and textural properties, we found significant effects for moisture, lightness, redness, hardness, and cohesiveness in the oven-roasted glutinous rice cakes, and water was one of the most influential factors. The optimal mixing conditions for the highest quality oven-roasted glutinous rice cake, in terms of sensory and textural properties, were 266.0 g of water, 25.4 g of sucrose, and 61.5 minutes of soaking time for the glutinous rice flour. The soaking time was in close to the median, whereas the water and sucrose values were slightly above the median.

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실험계획법을 이용한 가스 혼합-순환식 플라즈마 공정의 최적화 (Optimization of Gas Mixing-circulation Plasma Process using Design of Experiments)

  • 김동석;박영식
    • 한국환경과학회지
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    • 제23권3호
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    • pp.359-368
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    • 2014
  • The aim of our research was to apply experimental design methodology in the optimization of N, N-Dimethyl-4-nitrosoaniline (RNO, which is indictor of OH radical formation) degradation using gas mixing-circulation plasma process. The reaction was mathematically described as a function of four independent variables [voltage ($X_1$), gas flow rate ($X_2$), liquid flow rate ($X_3$) and time ($X_4$)] being modeled by the use of the central composite design (CCD). RNO removal efficiency was evaluated using a second-order polynomial multiple regression model. Analysis of variance (ANOVA) showed a high coefficient of determination ($R^2$) value of 0.9111, thus ensuring a satisfactory adjustment of the second-order polynomial multiple regression model with the experimental data. The application of response surface methodology (RSM) yielded the following regression equation, which is an empirical relationship between the RNO removal efficiency and independent variables in a coded unit: RNO removal efficiency (%) = $77.71+10.04X_1+10.72X_2+1.78X_3+17.66X_4+5.91X_1X_2+3.64X_2X_3-8.72X_2X_4-7.80X{_1}^2-6.49X{_2}^2-5.67X{_4}^2$. Maximum RNO removal efficiency was predicted and experimentally validated. The optimum voltage, air flow rate, liquid flow rate and time were obtained for the highest desirability at 117.99 V, 4.88 L/min, 6.27 L/min and 24.65 min, respectively. Under optimal value of process parameters, high removal(> 97 %) was obtained for RNO.

반응표면 분석법을 이용한 바질 첨가한 홈메이드 파스타 제조의 최적화 (Optimization of Homemade Pasta with Addition of Basil using Response Surface Methodology)

  • 최은영;주나미
    • 한국식생활문화학회지
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    • 제20권1호
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    • pp.61-67
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    • 2005
  • The purpose of study was to determine the organoleptic characteristics of homemade basil-pasta made in various compounding ratio according to central composite design. The optimum mixing condition for basil-pasta was optimized by response surface methodology. The texture, including color, flavor, elasticity and overall quality, was measured as sensory evaluation. The optimum mixing rates of durum wheat semolina, basil and egg were 73.97g, 5.95g and 36.17g for color, 53.14g, 4.52g and 35.85g for flavor, 48.75g, 2.95g and 36.85g for elasticity. The organoleptic overall quality of basil-pasta showed the maximum score in the mixing condition of 55.52 g durum wheat semolina, 4.55g basil paste and 35.51g egg.

화학적 응집공정에서 요인배치 중심합성설계법을 이용한 축산폐수의 COD 제거특성 평가 및 최적화 연구 (Analysis of Removal Characteristics and Optimization of Livestock Wastewater using a Factorial Design in the Coagulation Process)

  • 조일형;이내현;장순웅;안상우;윤영한;조경덕
    • 한국물환경학회지
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    • 제23권1호
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    • pp.111-121
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    • 2007
  • The experimental design and response surface methodologies haven been applied to the investigation of the chemical coagulation of livestock wastewater. The chemical coagulation reactions were mathematically described as a function of parameters raping mixing (rpm) of chemical coagulation ($X_1$), slow mixing (rpm) of chemical coagulation ($X_2$), $FeCl_3 $ concentration (mg/L) ($X_3$) and pH ($X_4$) being modeled by use of the central composite design. Empirical models were developed to describe relationship between the experimental variables and response. Statistical analysis indicates that three factors ($X_1$: raping mixing (rpm), $X_2$: slow mixing (rpm), $X_3$: $FeCl_3 $ concentration (mg/L) on the linear term (main effect), slow mixing (rpm) (${X_2}^2$) on the non-linear term (quadratic), and two factors ($X_1-X_3$, $X_2-X_3$) on the non-linear term (cross-product) had significant effects, respectively. The estimated ridge of maximum responses and optimal conditions for CODcr using canonical analysis was 87.44% ($X_1$: 229 rpm, $X_2$: 51 rpm, $X_3$: 877 mg/L, $X_4$: 4.3). To confirm this optimum condition, three additional experiments were performed and the mean CODcr removal (%) and concentration (mg/L) with a standard deviation of $87{\pm}1.2%$ ($576{\pm}34ppm$) were obtained.

콜리플라워를 이용한 피클제조 최적화 (Optimization on Organoleptic Charateristics of Cauliflower Pickles)

  • 윤지영;황재선;주나미;정현아
    • 한국식생활문화학회지
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    • 제19권2호
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    • pp.193-199
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    • 2004
  • The purpose of this study was to determine the organoleptic charateristics of cauliflower pickles made in various compounding ratio according to central conposite design for optimum organoleptic characteristics of the cauliflower pickles. The optimum mixing condition of cauliflower pickles were optimized, using central composite design with 3 variables and 3 levels, by response surface methodology. The various kinds of cauliflower pickle were made in various compounding ratio of vinegar, salt and sucrose - critical ingredients of pickle recipe - and were presented to reliable panels, who graded the subjects in 7 degrees for 4 items : color, flavor, hardness and overall quality. The optimum mixing conditions of cauliflower pickle were 603.50g of vinegar, 80.13g of salt and 251.07g of sucrose in the maximum point of overall quality.

반응표면분석법을 이용한 노니젤리 제조의 최적화 (Optimization of Jelly with Addition of Morinda Citrifolia(Noni) by Response Surface Methodology)

  • 박상현;주나미
    • 한국식품조리과학회지
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    • 제22권1호
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    • pp.1-11
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    • 2006
  • To determine the optimal mixing conditions of Noni jelly, samples were prepared with various compounding ratios of Noni juice(120, 160, 200, 240 and 280 g), gelatin(12, 16, 20, 24 and 28 g) and sucrose(80, 100, 120, 140 and 160 g) using a central composite design. Physical and sensory evaluations were performed and the results analyzed using response surface methodology. The optimum mixing rate satisfying sensory items was Noni juice 192 g, gelatin 18.25 g and sucrose 135 g.

차이브를 첨가한 홈 메이드 파스타 제조의 최적화 (A Study on the Sensory Optimization of Home made Pasta with the addition of Chives)

  • 고영주;주나미
    • 한국식품조리과학회지
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    • 제20권3호
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    • pp.227-234
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    • 2004
  • To determine the optimum mixing conditions of home made pasta with chives, samples were prepared with various compounding ratios of Durum wheat semolina (99, 198 and 297g), chive paste (27, 45 and 63g) and egg (72, 81 and 90g) using a central composite design, and sensory evaluations were performed and considered using a response surface methodology. The optimum mixing rates of Durum wheat semolina, chive paste and egg were 191.10, 45.53 and 80.98g for color, 149.00, 47.00 and 73.24g for flavor, 185.06, 43.99 and 81.18g for elasticity, and 188.69, 42.32 and 82.36g for overall quality. These results show that Chive paste effect the color and flavor, and Durum wheat semolina and egg effect the elasticity and overall quality.

반응표면분석법을 이용한 백년초젤리 제조의 최적화 (Optimization of Jelly Preparation from Nopal by Response Surface Methodology)

  • 정현아;주나미
    • 한국식생활문화학회지
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    • 제20권6호
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    • pp.695-702
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    • 2005
  • To determine the optimum mixing conditions of nopal jelly, samples were prepared with various compounding ratios of gelatin(16, 18, 20, 22 and 24g), sucrose(100, 120, 140, 160 and 180g), Citric acid(2, 3, 4, 5 and 6) using a central composite design. Physical and sensory evaluations were performed and considered using a response surface methodology. The optimum mixing rates which meet sensory items is gelatin 20.19g, sucrose 141.52g and citric acid 4.04g.

플랜트 생산 재활용 상온 혼합물의 도로 표층 적용성에 관한 기초연구 (Fundamental Study on the Application of a Surface Layer using Cold Central-Plant Recycling)

  • 최준성
    • 한국도로학회논문집
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    • 제20권1호
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    • pp.69-76
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    • 2018
  • PURPOSES : This study determined the optimal usage rate of RAP (reclaimed asphalt pavement) using cold central-plant recycling (CCPR) on a road-surface layer. In addition, a mixture-aggregate gradation design and a curing method based on the proposed rate for the surface-layer mix design were proposed. METHODS : First, current research trends were investigated by analyzing the optimum moisture content, mix design, and quality standards for surface layers in Korea and abroad. To analyze the aggregate characteristics of the RAP, its aggregate-size characteristics were analyzed through the combustion asphalt content test and the aggregate sieve analysis test. Moreover, aggregate-segregation experiments were performed to examine the possibility of RAP aggregate segregation from field compaction and vehicle traffic. After confirming the RAP quality standards, coarse aggregate and fine aggregate, aggregate-gradation design and quality tests were conducted for mixtures with 40% and 50% RAP usage. The optimum moisture content of the surface-layer mixture containing RAP was tested, as was the evapotranspiration effect on the surface-layer mixture of the optimum moisture content. RESULTS : After analyzing the RAP recycled aggregate size and extraction aggregate size, 13-8mm aggregate was found to be mostly 8mm aggregate after combustion. After using surface-chipping and mixing methods to examine the possibility of RAP aggregate segregation, it was found that the mixing method contributed very little for 3.32%, and because the surface-chipping method applied compaction energy directly as the maximum assumption the separation ratio was 15.46%. However, the composite aggregate gradation did not change. Using a 40% RAP aggregate rate on the surface-layer mixture for cold central-plant recycling satisfied the Abroad quality standard. The optimum moisture content of the surface-layer mixture was found to be 7.9% using the modified Marshall compaction test. It was found that the mixture was over 90% cured after curing at $60^{\circ}C$ for two days. CONCLUSIONS : To use the cold central-plant recycling mixture on a road-surface layer, a mixture-aggregate gradation design was proposed as the RAP recycled aggregate size without considering aggregate segregation, and the RAP optimal usage rate was 40%. In addition, the modified Marshall compaction test was used to determine the optimum moisture content as a mix-design parameter, and the curing method was adapted using the method recommended by Asphalt Recycling & Reclaiming Association (ARRA).

천연 혼합유화제를 이용한 O/W 유화액의 제조 : 중심합성계획모델을 이용한 유화안정성 최적화 (Emulsification of O/W Emulsion Using Natural Mixed Emulsifiers : Optimization of Emulsion Stability Using Central Composite Design-Reponse Surface Methodology)

  • 홍세흠;천추이웨이;이승범
    • 공업화학
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    • 제34권3호
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    • pp.299-306
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    • 2023
  • 본 연구에서는 무환자와 알팔파로부터 추출한 천연계면활성제를 유화제로 사용하여 반응표면분석법 중 중심합성계획모델(CCD-RSM)을 이용한 O/W 유화 제조공정의 최적화를 수행하였다. 공정변수로는 혼합유화제 첨가량, 천연유화제 혼합비율(무환자 사포닌/알팔파 사포닌), 유화시간으로 설정하였고 반응치로는 유화액의 유화안정화지수, 평균입자크기, 항산화능(DPPH 라디칼 소거활성)으로 설정하였다. 기초실험을 통한 계량인자범위는 혼합유화제 첨가량(12~14 wt%), 천연유화제 혼합비율(30~70%), 유화시간(20~30 min)으로 설정하여 CCD-RSM을 이용하여 최적화한 결과, O/W 유화 제조공정의 최적조건으로 혼합유화제 첨가량은 13.2 wt%, 천연유화제 혼합비율은 44.2%, 유화시간은 25.8 min으로 나타났으며, 이 조건에서 예측된 반응치로서 유화액의 유화안정도지수(ESI)는 88.7%, 평균입자크기(MDS)는 815.5 nm, 항산화능은 38.7%으로 계산되었다. 이를 실험을 통해 확인한 결과 유화액의 ESI는 90.6%, MDS는 830.2 nm, 항산화능은 39.6%으로 나타났으며 평균오차율은 2.1%이었다. 따라서 CCD-RSM을 실제 유화 제조에 적용하여 만족스러운 O/W 유화제조 공정조건을 얻을 수 있었다.