• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2002년도 추계학술대회 논문집 Vol.15
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• pp.276-279
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• 2002

$Bi_{2}Sr_{2}CaCu_{2}O_{x}$ was prepared by the conventional method of solid state reaction and SHS method. The samples were annealed in different atmosphere in order to examine the influence of atmospheres on the carbon contents in the $Bi_{2}Sr_{2}CaCu_{2}O_{x}$ compound. The lowest carbon content in $Bi_{2}Sr_{2}CaCu_{2}O_{x}$ could be attended when the sample was annealed in $O_{2}$ at $800^{\circ}C$ for 100 hours. The $CO_{2}$ in air pollute the samples and increase the carbon content in the sintering process. The critical current density of the $Bi_{2}Sr_{2}CaCu_{2}O_{x}$ samples will decrease with the increasing carbon contents in the samples. The impurity carbon will deposit in the grain boundary, which makes critical current density lower.

• 한국응용과학기술학회지
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• 제23권3호
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• pp.199-206
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• 2006

Direct decomposition of methane over three types of carbon black (N330-p, N330-f, and HI-900L) was carried out in a fluidized bed quartz reactor. Properties of carbon black before and after reaction were measured and found to be related with surface structure and weight gain. For N330-p and N330-f, some carbon deposit on the surface was considered to be the reason for the increase of BET surface area and pore volume with weight gain. Carbon deposits on the surface and the conglutination of some aggregates may explain the slight increase of particle size. Properties of HI-900L changed much more significantly with weight gain. It is supposed that the increase of aggregate size of HI-900L were due to some unknown oily components. The corresponding agglomeration might be the reason for the decrease of BET surface area with weight gain, as compared with the increase of that for the case of N330 black.

• 한국가스학회지
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• 제16권3호
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• pp.48-53
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• 2012

이 논문의 목적은 LPG 자동차의 액상 분사시스템에 관련된 고장사례를 연구하는 것이다. LPi 분사시스템인 인젝터를 점검한 결과, 인젝터에 카본이 누적되어 운전 중에 간헐적으로 연료를 분사하는 인젝터의 미세한 홀을 막아 연비를 5% 정도 떨어뜨리는 것으로 확인되었다. 엔진의 공회전을 조절하는 시스템인 공회전 조절장치 부품과 엔진에 공기를 공급하는 시스템인 스로틀 보디에 카본이 퇴적되어 공기의 흐름을 간섭함으로써 연비가 7% 악화된 것을 확인되었다. 엔진의 흡기 매니폴드 개스킷의 일부가 찢어져, 실린더 헤드와 실린더 블록의 밀착성이 약화되어 흡기행정에서 외부의 공기가 이 틈새로 간헐적으로 유입되면서 증가된 공기량만큼 연료량의 증가를 가져와 엔진의 회전수가 증가하여 부조화 현상이 발생되어 정상적인 상태보다 연비가 3% 정도 악화된 것으로 확인되었다. 이러한 고장사례는 운전중에 엔진의 출력 성능을 떨어뜨리고, 자동차의 연비를 악화시키는 요인이 된다. 따라서 품질확보에 철저하게 대처하여 고장현상을 최소화 하여야 할 것으로 판단된다.

• 대한기계학회논문집A
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• 제31권1호
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• pp.139-144
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• 2007

This paper presents development of carbon nanotube (CNT) tip modified by focused ion beam (FIB) and experimental results in non-contact mode of atomic force microscopy (AFM) using fabricated tip. We used an electric field which causes dielectrophoresis, to align and deposit CNTs on a conventional silicon tip. The morphology of the fabricated CNT tip was then modified into a desired shape using focused ion beam. We measured anodic aluminum oxide sample and trench structure to estimate the performance of FIB-modified tip and compared with those of conventional Si tip. We demonstrate that FIB modified tip in non contact mode had superior characteristics than conventional tip in the respects of wear, image resolution and sidewall measurement.

• Journal of Welding and Joining
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• 제6권2호
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• pp.40-46
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• 1988

The effect of heat input on the content of residual .delta.-ferrite and the hot cracking susceptibility in the austenitic stainless steel overlaid on the carbon steel was studied in the range of heat input from 7.5 to 15.1 KJ/cm. Present study shows that residual .delta.-ferrite content in the overlay is mainly determined by the dilution of the base metal (carbon steel) which is in turn affected by heat input, i.e. the amount of dilution decreases as heat input increase. Accordingly, higher heat input results in a substantial increase in Cr equivalent but a little increase in Ni equivalent due to the less dilution of carbon from base metal. This fact can explain the result obtained in this study, i, e, the higher content of .delta.-ferrite in the weld deposit made with higher heat input. This in turn causes more resistant overlaying weld metal to hot cracking.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2006년도 춘계학술대회 논문집
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• pp.461-462
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• 2006

This paper reports on the development of a scanning probe microscopy(SPM) tip with caborn nanotubes. We used an electric field which causes dielectrophoresis(DEP), to align and deposit CNTs on a metal-coated SPM tip. Using the CNT attached SPM tip, we have obtained an enhanced resolution and wear property compared to that from the bare silicon tip through the scanning of the surface of the bio materials. The carbon nanotube tip align toward the source of the ion beam allowing their orientation to be changed at precise angles. By this technique, metal coated carbon nanotube tips that are several micrometer in length are prepared for scanning probe microscopy.

• 한국레이저가공학회지
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• 제2권2호
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• pp.34-41
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• 1999

A RS840 $CO_2$laser and a powder auto-feeding apparatus have been used to deposit single tracks of Ni-base superalloy on low carbon steel. In this paper, the effects of laser cladding parameters on clad geometry, dilution and microhardness are studied. As a results, the w/h ratio of the clad layer increases with decreasing powder feed rate and increasing laser scan speed. Increase of powder density and decrease of specific energy have little effect on dilution. It was found that the clad layer of the highest hardness has a structure in which fine and leaf like phases are dispersed in ${\gamma}$Ni matrix.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2001년도 추계학술발표회 초록집
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• pp.29-30
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• 2001

This paper presents some results of plasma nitriding on hard chromium deposit. The substrates were C45 steel and $30~50{\;}\mu\textrm{m}$ of chromium deposit by electroplating was formed. Plasma nitriding was carried out in a plasma nitriding system with $95NH_3{\;}+{\;}SCH_4$ atmosphere at the pressure about 600 Pa and different temperature from $450^{\circ}C{\;}to{\;}720^{\circ}C$ for various time. Optical microscopy and X-ray diffraction were used to evaluate the characteristics of surface nitride layer formed by nitrogen diffusion from plasma atmosphere inward iCr coating and interface carbide layer formed by carbon diffusion from substrate outward Cr coating. The microhardness was measured using microhareness tester at the load of 100 gf. Corrosion resistance was evaluated using the potentiodynamic measurement in 3.5% NaG solution. A saturated calomel electrode (SiCE) was used as the reference electrode. Fig.1 shows the typical microstructures of top surface and cross-section for nitrided and unnitrided samples. Aaer plasma nitriding a sandwich structure was formed consisting of surface nitride layer, center chromium layer and interface carbide layer. The thickness of nitride and carbide layers was increased with the increase of processing temperature and time. Hardness reached about 1000Hv after nitriding while 900Hv for unnitrided hard chromium deposit. X-ray diffraction indicated that surface nitrided layer was a mixture of $Cr_2N$ and CrN at low temperature and erN at high temperature (Fig.2). Anodic polarization curves showed that plasma nitriding can greatly improve the corrosion resistance of chromium e1ectrodeposit. After plasma nitriding, the corrosion potential moved to noble direction and passive current density was lower by 1 to 4 orders of magnitude compared with chromium deposit(Fig.3).

• 한국표면공학회지
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• 제50권6호
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• pp.531-535
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• 2017

Enormous amount of waste oyster-shell (OS) has a major disposal problem in coastal regions. OSs have attracted much attention for recycling, because these are mainly composed of calcium carbonate with rare impurities. In this study, we demonstrate the calcareous deposit films on steel plate by using OSs on the basic of cathodic protection technique. The composition of the OSs was analyzed by wavelength dispersive X-ray fluorescence spectrometer. Carbon dioxide gas was pumped into distilled water to make carbonic acid solution for dissolution of OS. The calcareous deposit was characterized by second electron microscope (SEM), energy dispersive X-ray analysis (EDX) and X-ray diffraction. Corrosion rates were estimated by measurements of anodic polarization and immersion test. It is confirmed that calcareous deposits on steel plate are formed under all condition of cathodic protection by using waste OS from the SEM and EDX results. Calcareous deposits on steel by OS provide good corrosion resistance by acting as a barrier to oxygen supply to the steel surface.

• 한국산학기술학회논문지
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• 제11권3호
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• pp.1016-1022
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• 2010

액상 중유 연료를 사용하는 고용량 증기 보일러에서 발생되어 연소기기 내부에 침적되는 슈트, 슬래그, 크랭커, 회분, 산화물의 on-line 세정을 위한 세정제 제조에 대한 연구를 수행하였다. 액상 중유 연료를 사용하는 보일러 및 가열로에 생성되는 슈트, 슬래그, 크랭커, 회분, 산화물을 제거하는 기존 기술은 보일러 및 가열로의 가동 중단 후 작업자들에 의한 기계적인 처리를 통하여 침적물을 제거하는 기술을 사용하고 있다. 기존 기술을 대치할 수 있고 보일러의 중단이 없는 상태에서 침적물을 세정할 수 있는 세정제의 최적 조성을 도출하였다. 질산암모늄과 질산마그네슘의 혼합물이 주 세정제로 도출되었으며, 각종 전이금속 화합물에 의한 영향을 영향을 연구하여, 세정에 의한 부식을 방지할 수 있으며, 연소효율의 증대를 얻을 수 있는 전이금속화합불 첨가제를 도출하였다.