• Title/Summary/Keyword: carbide analysis

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The Cutting Characteristics of Rotary Tools Using Regression Analysis (회귀분석법을 이용한 로타리 공구의 절삭 특성)

  • Maeng, Min-Jae;Jang, Sung-Min
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.4 no.4
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    • pp.14-20
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    • 2005
  • This paper deals with the study of feasibility of rotary carbide tools in the machining of aluminium alloy. A rotary tool holder was designed and manufactured for this work. Experiments were performed using Taguchi methods and regression analysis to analyse the influence of various factors and their interactions on the cutting characteristics of rotary carbide tools during machining. The cutting force is influenced the most greatly at the inclination angle. The surface roughness is influenced distinctly at depth of cut. It deduced an equation to predict cutting force and surface roughness. Hence, it could be concluded here that the proposed model agrees with the experimental data satisfactorily.

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Effect of Specific Surface Area on the Reaction of Silicon Monoxide with Porous Carbon Fiber Composites

  • Park, Min-Jin;Lee, Jae-Chun
    • The Korean Journal of Ceramics
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    • v.4 no.3
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    • pp.245-248
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    • 1998
  • Porous carbon fiber composites (CFCs) having variable specific surface area ranging 35~1150 $\m^2$/g were reacted to produce silicon carbide fiber composites with SiO vapor generated from a mixture of Si and $SiO_2$ at 1673 K for 2 h under vacuum. Part of SiO vapor generated during conversion process condensed on to the converted fiber surface as amorphous silica. Chemical analysis of the converted CFCs resulting from reaction showed that the products contained 27~90% silicon carbide, 7~18% amorphous silica and 3~63% unreacted carbon, and the composition depended on the specific carbide, 7~18% amorphous silica and 3~63% unreacted carbon, and the composition depended on the specific surface area of CFCs. CFC of higher specific surface area yielded higher degree of conversion of carbon to silicon and conversion products of lower mechanical strength due to occurrence of cracks in the converted caron fiber. As the conversion of carbon to silicon carbide proceeded, pore size of converted CFCs increased as a result of growth of silicon carbide crystallites, which is also linked to the crack formation in the converted fiber.

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As-Cast and Solidification Structures of Fe-3%C-x%Cr-y%V-w%Mo-z%W Multi- Component White Cast Irons (Fe-3%C-x%Cr-y%V-w%Mo-z%W 다합금계백주철의 주방상태 및 급냉조직)

  • Yu, sung-Kon;Shin, Sang-Woo
    • Korean Journal of Materials Research
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    • v.12 no.5
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    • pp.414-422
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    • 2002
  • Three different multi-component white cast irons alloyed with Cr, V, Mo and W were prepared in order to study their as-cast and solidification structures. Three combinations of the alloying elements were selected so as to obtain the different types of carbides and matrix structures : 3%C-10%Cr-5%Mo-5%W(alloy No.1), 3%C-10%V-5% Mo-5%W(alloy No. 2) and 3%C-17%Cr-3% V(alloy No.3). The as-cast microstructures were investigated with optical and scanning electron microscopes. There existed two different types of carbides, $M_7C_3$ carbide with rod-like morphology and $M_6C$ carbide with fishbone-like one, and matrix in the alloy No. 1. The alloy No. 2 consisted of MC carbide with chunky and flaky type and needle-like $M_2C$ carbide, and matrix. The chunky type referred to primary MC carbide and the flaky one to eutectic MC carbide. The morphology of the alloy No. 3 represented a typical hypo-eutectic high chromium white cast iron composed of rod-like $M_7C_3$ carbide which is very sensitive to heat flow direction and matrix. To clarify the solidification sequence, each iron(50g) was remelted at 1723K in an alumina crucible using a silicon carbide resistance furnace under argon atmosphere. The molten iron was cooled at the rate of 10K/min and quenched into water at several temperatures during thermal analysis. The solidification structures of the specimen were found to consist of austenite dendrite(${\gamma}$), $ ({\gamma}+ M_7C_3)$ eutectic and $({\gamma}+ M_6C)$ eutectic in the alloy No. 1, proeutectic MC, austenite dendrite(${\gamma}$), (${\gamma}$+MC) eutectic and $({\gamma}+ M_2C)$ eutectic in the alloy No. 2, and proeutectic $M_7C_3$ and $ ({\gamma}+ M_7C_3)$ eutectic in the alloy No 3. respectively.

Machining Characteristics and Cutting Force Analysis of Hardfacing Overlay Welding in High Chromium Carbide (고크롬탄화물 하드페이싱 육성용접물의 가공특성과 절삭력 분석)

  • Kim, Min-Ho;Kim, Tae-Young
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.18 no.5
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    • pp.469-476
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    • 2009
  • Hard facing overlay welding in high chromium carbide is a representative way of extending the fatigue life or recompensing damage, because workpiece surface is uniformly overlay-welded by alloy material. In general, grinding process is currently used for finish due to hardness of weld material. The development of tool material, such as PCBN, has made it possible to use turning instead of grinding. There are many advantages of hard Owning, as lower equipment costs, shorter setup time, fewer process steps, higher material removal rate, better surface integrity and the elimination of cutting fluid. In this paper, machining characteristics and cutting performance are examined to investigate turning possibility of overly welding in high chromium carbide.

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Research of the Composite Spun Yarn Manufacturing Process using Silicon Carbide and Para Aramid Fiber (SiC/p-Aramid 복합방적사 제조기술 연구)

  • Kim, Booksung;Ryu, Huijun
    • Textile Coloration and Finishing
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    • v.33 no.4
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    • pp.309-316
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    • 2021
  • Due to the rigid nature of the silicon carbide fiber(SiC), fiber damage occurs from the friction during the carding process. This damage not only lowers the spun yarn yield, but also lowers the heat resistance of the spun yarn, so that ultra-high heat resistant yarn cannot be manufactured. Therefore, in the carding process where the most friction between fiber and machine(wire, etc.) occurs, some factors were modified and tested, and as a result of measuring the change in physical properties, fiber damage decreased due to the wire angle or wire density, resulting in improved yield. The test method used to measure the yield of SiC fiber was the carbonization method, and the content of SiC fibers was calculated using the remaining amount after carbonization. Carbonization test was performed at air condition, 700℃, and for 2 hours. Analysis by SEM-EDX showed that the carbide was consistent with the composition of the SiC fiber.

A Study on Flammability and Mechanical Properties of HDPE/EPDM/Boron Carbide/Triphenyl Phosphate Blends with Compatibilizer (HDPE/EPDM/Boron Carbide/Triphenyl Phosphate 블렌드의 상용화제 첨가에 따른 난연성 및 기계적 물성 연구)

  • Shin, Bum-Sik;Jung, Seung-Tae;Jeun, Joon-Pyo;Kim, Hyun-Bin;Oh, Seung-Hwan;Kang, Phil-Hyun
    • Polymer(Korea)
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    • v.36 no.5
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    • pp.549-554
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    • 2012
  • It was known that triphenyl phosphate wasn't homogeneously dispersed in HDPE/EPDM/boron carbide blends, which caused the decrease in mechanical properties. HDPE, EPDM, boron carbide, and triphenyl phosphate were blended with PE-g-MAH(polyethylene-graft-maleic anhydride) as a compatiblizer for improving the miscibility of triphenyl phosphate. Tensile strength of HDPE/EPDM/boron carbide blends decreased with increasing the contents of triphenyl phosphate for flammability. However, the mechanical properties of HDPE/EPDM/boron carbide/triphenyl phosphate blends increased by the addition of compatiblizer because triphenyl phosphate was homogeneously mixed in the blend system. The homogeneous dispersibility of triphenyl phosphate was confirmed by using scanning electron microscopy (SEM). Increased thermal stability and flammability derived from high miscibility of triphenyl phosphate were confirmed by the results of thermogravimetric analysis (TGA) and limiting oxygen index (LOI). A self-extinguishing HDPE/EPDM/boron carbide/triphenyl phosphate blend was successfully fabricated with more than 21% LOI.

A Study on the Flank Wear of Carbide Tool in Machining SUS304 (SUS304 절삭시 Carbide 공구의 Crater 마모에 관한 연구)

  • Jeong, Jin-Yong;O, Seok-Hyeong;Kim, Jong-Taek;Seo, Nam-Seop
    • Journal of the Korean Society for Precision Engineering
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    • v.8 no.3
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    • pp.44-54
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    • 1991
  • A Study was made on falnk wear in carbide tools in turning SUS304 steel. When an austenitic stainless steel (SUS304 steel) is cut with the tool, saw-toothed chip are produced. It is found that machining SUS304 steel would make a tool worn fast. For increasing productivity, tool wear has to be predicted and controlled. An amended cutting geometry consisting of a negative rake angle ($-6^{\circ}$ ) and a high clearance angle ($-17^{\circ}$ ) is proposed for decreasing carbide tool wear (flank) in the machining of SUS304 steel. The amended cutting geometry is found to make the flank wear lower than a general cutting geometry (rake angle $6^{\circ}$ , clearance angle $5^{\circ}$). The effects of the three cutting variables (cutting speed, feed, tool radius) on the flank wear analyzed by fiting a simple first-order model containing interaction terms to each flank wear parameter by means of regression analysis and the predicted from first-order regression analysis model equation of flank wear.

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Evaluation of Thermal Degradation of 2.25Cr-1Mo Steel Using Ultrasonic Nonlinear Effect and X-ray Diffraction Method (초음파 비선형 음향 효과 및 X-선 회절법을 이용한 2.25Cr-1Mo 강의 열화 손상 평가)

  • Kim, Duk-Hee;Park, Un-Su;Park, Ik-Keun;Byeon, Jai-Won;Kwun, Sook-In
    • Journal of the Korean Society of Safety
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    • v.17 no.4
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    • pp.71-79
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    • 2002
  • It was attempted to evaluate the degree of degradation of thermally aged 2.25-1Mo steek by ultrasonic monlinear parameter(UNP) measurement and X-ray diffraction analysis of extracted carbide. Artificial aging was performed to simulate the microstructural degradation in 2.25Cr-1Mo steel arising from long time exposure at $540{\circ}C$. Microstructural analysis (number of carbides per unit area) and measurements of mechanical properties(Vickers hardness, DBTT) and degradation evaluation parameters(UNP and intensity ration of X-ray diffraction peak of electrolytically extracted carbide) were performed. Both of UNP and intensity ratio of X-ray diffraction peak for M6C carbide to that of M23C6 carbide(IR) increased abruptly in the initial 1000 hour of aging and then changed little. UNP and IR were proposed as potential parameters to evaluate the degree of aging degradation of 2.25Cr-1Mo steel.

Carbide Precipitation Behavior During Normalizing Heat Treatment in Low-alloyed Cr-Mo-V-Ti Steel (Cr-Mo-V-Ti 저합금강에서 노멀라이징 열처리조건에 따른 석출물의 거동)

  • Kim, Hong-Ki;Na, Hye-Sung;Lee, Sang-Hoon;Kang, Chung-Yun
    • Journal of the Korean Society for Heat Treatment
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    • v.30 no.2
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    • pp.43-52
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    • 2017
  • Heat treatment condition for dissolution of the M23C6 carbides in 2.25Cr-1Mo-V-Ti material for thermal power plant tube was investigated using a dilatometer method. 2.25Cr-1Mo-V-Ti material was heat-treated at $900{\sim}1,100^{\circ}C$ for 0, 10, 30 min to find the proper dissolution condition of M23C6 carbides. The phase identification and volume fraction of the carbide were measured by using OM, SEM, EBSD and TEM analysis. Optimal heat treatment condition of M23C6 carbide dissolution was selected by predicting dissolution temperature of carbide using Bs points appeared at dilatometer curve. Experimental results showed that the conditions of carbide dissolution was 900, 1,000, $1,100^{\circ}C$ for 30 min. Eventually, the optimal heat treatment condition for dissolution was 30 min at $1,000^{\circ}C$ considering the minimum coarsening of Austenite grain size.

A Brief Review of κ-Carbide in Fe-Mn-Al-C Model Alloys

  • Seol, Jae Bok
    • Applied Microscopy
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    • v.48 no.4
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    • pp.117-121
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    • 2018
  • The multiple length scale analysis of previously designed Fe-Mn-Al-C based low-density model alloys reveals the difference in ordered ${\kappa}-carbide$, $(Fe,Mn)_3AlC_x$, between Fe-25Mn-16Al-5.2C (at%) alloy and Fe-3Mn-10Al-1.2C (at%) alloy. For the former alloy composition consisting of fully austenite grains, ${\kappa}-carbide$ showed majorly cuboidal and minorly pancake morphology and its chemical composition was not changed through aging for 24 h and 168 h at $600^{\circ}C$. Meanwhile, for the isothermally annealed ferritic alloy system for 1 hr at 500 and $600^{\circ}C$, the dramatic change in the chemical composition of needle-shape ${\kappa}-carbide$, $(Fe,Mn)_3(Fe,Al)C_x$, was found. Here we address that the compositional fluctuations in the vicinity of the carbides are significantly controlled by abutting phase, either austenite or ferrite. Namely, the cooperative ordering of carbon and Al is an important factor contributing to carbide formation in the high-Mn and high-Al alloyed austenitic steel, while the carbon and Mn for the low-Mn and high Al alloyed ferritic steel.