• Title/Summary/Keyword: calcium extraction

Search Result 157, Processing Time 0.031 seconds

대두 NUTRAGEN III로부터 Isoflavones 추출을 위한 최적 조건

  • Kim, Gi-Uk;Jeon, Byeong-Su
    • 한국생물공학회:학술대회논문집
    • /
    • 2000.11a
    • /
    • pp.640-643
    • /
    • 2000
  • Soybeans contain the phytoestrogens genistein and daidzein, their glucosides genistin and daidziin and coumesterol. These isflavonoid compounds are capable of producing an estrogenic response in a number of diverse species. This study determined optimum conditions for extraction of isoflavones in defatted soybean meal. Extraction of isoflavones was conducted at various conditions such as difference concentrations of extraction solvent, temperature, time and pH to extact. The most optimum extraction conditions was achieved at 75% ethanol, $80^{\circ}C$, pH4 and extract for three hours. In addition. isoflavones with high purity were separated by adding up to 4%(w/v) of calcium chloride dihydrate.

  • PDF

Effect of oxygen containing compounds in uranium tetrafluoride on its non-adiabatic calciothermic reduction characteristics

  • Gupta, Sonal;Kumar, Raj;Satpati, Santosh K.;Sahu, Manharan L.
    • Nuclear Engineering and Technology
    • /
    • v.53 no.6
    • /
    • pp.1931-1938
    • /
    • 2021
  • Uranium ingot is produced by metallothermic reduction of uranium tetrafluoride using magnesium or calcium as reductant. Presence of oxygen containing compounds viz. uranyl fluoride and uranium oxide in the starting uranium fluoride has a significant effect on the firing time, final temperature of the charge, slag-metal separation and hence the metal recovery. As reported in the literature, the maximum tolerable limit for uranyl fluoride in the UF4 is 2.5 wt% and limit for uranium oxide content is in the range 2-3 wt%. No theoretical or experimental basis is available till date for these limits. Analyses have been carried out in this study to understand the effect of UO2F2 concentration in the starting fluoride on the final temperature of the products and thus the reduction characteristics. UF4 having uranyl fluoride concentration, less than as well as more than 2.5 wt%, have been investigated. Thermodynamic calculations have been carried out to arrive at a general expression for the final temperature attained by the products during calciothermic reduction of UF4. Finally, an upper limit for the oxygen containing impurities has been estimated using the CaO-CaF2 phase diagram.

Studies on Xanthine Oxidase from Bovine Thyroid Glands -[Part 1] Purification and Substrate Specificity- (소의 갑상선에 있는 크산친 옥시다아제에 관한 연구 -[제1보] 효소의 정제와 기질특이성-)

  • Lee, Hyo-Sa
    • Applied Biological Chemistry
    • /
    • v.21 no.2
    • /
    • pp.112-118
    • /
    • 1978
  • Xanthine oxidase from bovine thyroid glands was purified to apparent homogeneity when judged by analytical disc gel electrophoresis. The purification procedures include pancreatin digestion, butanol extraction, ammonium sulfate precipitation, calcium phosphate gel adsorption, ultrafiltration, calcium phosphate gel-cellulose column chromatography, gel filtration, preparative Sephadex G-25 column electrophoresis, and preparative polyacrylamide gel electrophoresis. The enzyme was enriched 1,000-fold. However, its specific activity was markedly low as compared with highly purified milk enzyme. Thyroidal xanthine oxidase exhibited a low specificity for substrates and electron acceptors. The kinetic properties of thyroid xanthine oxidase were found to be similar to those of the milk enzyme on the basis of Michaelis constants for common substrates.

  • PDF

Extraction Method for Paraquat from Soil (토양중 Paraquat의 효과적인 추출방법)

  • Kwon, Jin-Wook;Kim, Yong-Se;Choi, Jong-Woo;Lee, Kyu-Seung
    • Korean Journal of Environmental Agriculture
    • /
    • v.16 no.3
    • /
    • pp.239-244
    • /
    • 1997
  • To develope more effective extraction methods for paraquat in soil, some modification methods were accomplished in two different types of soil. For extraction of tightly bound-paraquat, conc. HCl 70ml were added with different shaking times, and then $H_2SO_4$ reflux were performed for an hour. In this case, 60 minutes shaking were optimum and recovery were increased more $1.09{\sim}1.50$ folds(84.0% in high clay contents soil, but 96.7% in low clay contents soil) and the long-time consuming step, filtration were easily done, with decreasing filtration time were shorter 4.6 folds(ca. $11{\sim}14min.$). than general paraquat analytical method(ca. $55{\sim}65min.$). And only $H_2O_2$ digestion with different volume and refluxing time resulted in recovery increasing. Nevertheless, considering analyst's safety, 30ml of $H_2O_2$ addition and 30 minutes reflux were regarded as optimum condition. Although, Kjeldahl digestion with $H_2O_2$ showed relatively high recovery, it is not significant statistically. For extraction of loosely bound-paraquat, 0.01, 0.1, 1.0, 10.0M of $NH_4Cl$ and of $CaCl_2$ compared with $1.5{\sim}24hr$ of different shaking time. There were no loosely bound residues of paraquat.

  • PDF

Development Status and Research Direction in the Mineral Carbonation Technology Using Steel Slag (제철 슬래그를 이용한 광물 탄산화 기술의 개발 현황과 연구 방향)

  • Son, Minah;Kim, Gookhee;Han, Kunwoo;Lee, Min Woo;Lim, Jun Taek
    • Korean Chemical Engineering Research
    • /
    • v.55 no.2
    • /
    • pp.141-155
    • /
    • 2017
  • In the present paper, we investigated the development status of precipitated calcium carbonate (PCC) production using steel slag, which is one of mineral carbonation (MC) technologies, from the standpoint of $CO_2$ utilization. Principle, feature, and global and domestic development status of the mineral carbonation technology were discussed together with the overview of the production method and market of PCC. Mineral carbonation is known as stable and environmentally-friendly technology enabling economical treatment of industrials wastes. Typically, PCC is produced by the reaction of $CO_2$ with supernatant solution after Ca extraction from steel slag followed by the separation of solid and liquid. The development status of MC using steel slag is at the pilot stage (Slag2PCC at Aalto University), and there remains the process economics improvement for commercialization. Key technologies for the further development are efficient extraction of Ca ions from steel slag including impurities removal, valorization of PCC via shape and size control, usage development and value-addition of residual slag, and optimization of reaction conditions for continuous process setup, etc.

Histologic Study on the Effect of Two Types of Bovine Bone Powder in Extraction Socket of Beagle Dogs (성견 발치와에 매식한 2종의 Bovine Bone Powder가 치유에 미치는 영향에 관한 조직학적 연구)

  • Park, Tae-Seong;Lim, Sung-Bin;Chung, Chin-Hyung;Kim, Jong-Yeo
    • Journal of Periodontal and Implant Science
    • /
    • v.30 no.3
    • /
    • pp.527-538
    • /
    • 2000
  • Several extraction cases with advanced bone loss as a result of periodontal disease, root or labial bone fracture, extensive caries, and periapical lesions occur esthetic, functional problems and severe bone loss. Therefore, to treat these cases used several surgical methods and socket preservation among this therapies have been evaluated simple, effective and good prognosis in the implant placement. Socket preservation therapy have been used with barrier membranes or/and graft materials. Deproteinized bovine bone mineral have been evaluated ideal grafting materials. Recently, calcium-phosphate thin film coated bovine bone powders were developed in our country, but the study for these material wasn't reported. When two types of xenograft materials were implanted in extraction sockets of Beagle dogs, the effects of these were analyzed after 4 weeks and 8 weeks histological views. The results of this study were as follows. 1. In control groups, 4 weeks after implantation, the extraction sockets were filled with connective tissue which has dilated vessels and epithelial growth. And after 8 weeks, irregular connective bundles were observed. But new bone formation was not seen. 2. In Bio-Oss groups, epithelial growth was not seen and bone powder was covered with connective tissue fiber. New bone formation was found around the interproximal bone. There was no special change seen after 8 weeks, connective tissue fibers became more regular, and bone growth near bone powder was not made well. 3. In Ca-P BBP groups, epithelial cells didn't grow in the extraction sockets, there was a lot of new bone made around the bone powder after 8 weeks, new bone around bone powder was replaced with mature bone. It is thought that bone powder grafting into the extraction sockets is very useful for conservation of ridge, and Ca-P BBP is more effective in bone formation than Bio-Oss.

  • PDF

Lime Treatment of Waterworks Sludges for Soil Cover in Municipal Landfilling Site (석회처리에 의한 정수 슬러지의 복토재 활용에 관한 연구)

  • Lim, Sung-Jin;Lee, Jae-Bok
    • Journal of Korean Society of Water and Wastewater
    • /
    • v.14 no.3
    • /
    • pp.231-239
    • /
    • 2000
  • Water treatment processes produce sludges resulting from water clarification. Sludge production amount increases each year and its treatment and disposal is growing to social problems according to water demand increase. Water treatment plant sludges can be modified to soil cover in sanitary landfill site through the lime treatment. Compression strength of $1.0kg/cm^2$ or more is recommended for soil cover material in municipal landfilling site. Compression and shear strength properties of modified sludges showed material property improvement applicable for soil cover alternatives. Solidification effect of the modified sludge was observed through the scanning electron microscope. Extraction tests for hazardous components in sludges revealed that extraction levels of cadmium, copper, and lead were below the regulated criteria. When adding 10% calcium hydroxide to water treatment plant sludges, the modified sludges can reach material properties for cover soil after 28 days solidification reaction.

  • PDF

A Study on the Extraction Time and Component Analysis of Goat Meat with Bone Extract (흑염소 육골액의 적정 추출시간 및 성분 분석에 관한 연구)

  • 조길석
    • Food Science and Preservation
    • /
    • v.9 no.4
    • /
    • pp.396-399
    • /
    • 2002
  • An attempt was made in this study to investigate the optimum extracting time from meat with bone of goat and the nutritional component of its extract. for the trials, the mixtures of meat with bone and water were adjusted to the ratios of five to four by weight and extracted for 6, 9 and 12 hours at 120$\^{C}$ under autoclave. Judging from the content of mineral and amino acid, nonenzymatic browning and yield, the optimum extracting time was 9 hours. The major components of mineral were composed of 47.7mg% potassium, 12.7mg% calcium, 150.0mg% sodium, 105.3mg% phosphorus and 0.5mg% iron, and of amino acids composed of 1,308.0mg% glutamic acid, 1,464.2mg% glycine, 750.2mg% alanine and 828.lmg% proline in extract. The yield of extract was 32.1 percentage by dry basis.

Effect of Calcium Carbonate on Properties of Paper in Alkali Paper Masking (중성초지에서 탄산칼슘의 성질이 종이의 물성에 미치는 영향)

  • 신종순
    • Journal of the Korean Graphic Arts Communication Society
    • /
    • v.8 no.1
    • /
    • pp.71-87
    • /
    • 1990
  • This paper presents a simple algorithm to obtain three dimensional information of an object. In the preprocessing of the stereo matching,feature point informations of stero image must be less sensitive to noise and well liked the correspondance problem. This paper described a simple technique of struture feature extraction of 3-D object and used edge-end point expanding method for unconnected line instade of Hough transform. The feature such as corner point and their angles are used for matching problem. The experimental results show that the described algorithm is a useful method for stereo correspondence problem.

  • PDF

CARE OF ANXIETY DISORDER AND HYPERVENTILATION DURING REFRACTORY TOOTH EXTRACTION IN A PSYCHOLOGIC DISABLED PATIENT (정신장애 환자에서 난발치 중의 불안장애와 과환기 관리 : 증례보고)

  • Oh, Ji-Hyeon;Yoo, Jae-Ha;Kim, Jong-Bae
    • The Journal of Korea Assosiation for Disability and Oral Health
    • /
    • v.10 no.2
    • /
    • pp.106-113
    • /
    • 2014
  • Hyperventilation is produced by several distinct causes: anxiety, respiratory alkalosis, increased blood catecholamine levels, and a decrease in the level of the ionized calcium in the blood. The dental fears about acute pain, bleeding, needle, drill and dental surgery lead to the severe anxiety and increased blood catecholamine level. Therefore, the most dental patient should be cared gently as the stress reduction protocol. In spite of the gentle care, a hyperventilation were occurred during the surgical extraction of impacted third molar with pericoronitis. We suggest that the dental patients with anxiety disorder must be attention for the manifestation of hyperventilation, especially in the psychologic disabled patient.