• 제목/요약/키워드: bulk temperature

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하이브리드 Ti2AlC 세라믹 소결체의 재료특성 및 Micro-EDM 유용성 연구 (Micro-EDM Feasibility and Material Properties of Hybrid Ti2AlC Ceramic Bulk Materials)

  • 정국현;김광호;강명창
    • 한국분말재료학회지
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    • 제21권4호
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    • pp.301-306
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    • 2014
  • Titanium alloys are extensively used in high-temperature applications due to their excellent high strength and corrosion resistance properties. However, titanium alloys are problematic because they tend to be extremely difficult-to-cut material. In this paper, the powder synthesis, spark plasma sintering (SPS), bulk material characteristics and machinability test of hybrid $Ti_2AlC$ ceramic bulk materials were systematically examined. The bulk samples mainly consisted of $Ti_2AlC$ materials with density close to theoretical value were synthesized by a SPS method. Random orientation and good crystallization of the $Ti_2AlC$ was observed at $1100^{\circ}C$ for 10 min under SPS sintering conditions. Scanning electron microscopy results indicated a homogeneous distribution and nano-laminated structure of $Ti_2AlC$ MAX phase. The hardness and electrical conductivity of $Ti_2AlC$ were higher than that of Ti 6242 alloy at sintering temperature of $1000^{\circ}C{\sim}1100^{\circ}C$. Consequently, the machinability of the hybrid $Ti_2AlC$ bulk materials is better than that of the Ti 6242 alloy for micro-EDM process of micro-hole shape workpiece.

마산과 행암 지역으로 유입되는 다환방향족탄화수소(PAHs)의 대기 침적 플럭스 산정과 특성 (Estimation and Characteristics of Atmospheric Deposition Flux of Polycyclic Aromatic Hydrocarbons (PAHs) into the Masan and Haengam Areas of Korea)

  • 이수정;문효방;최민규
    • 한국환경과학회지
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    • 제15권2호
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    • pp.121-131
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    • 2006
  • Atmospheric bulk (wet and dry) samples were monthly collected in Masan and Heangam areas of Korea, to assess the deposition flux and seasonal variation of polycyclic aromatic hydrocarbons (PAHs). Deposition fluxes of PAHs in bulk samples were determined using gas chromatography coupled to mass spectrometer detector (GC/MSD). Particle deposition fluxes from Masan and Haengam areas varied from 13 to $87\;g/m^2/year$ and from 5 to $52\;g/m^2/year$, respectively. PAHs deposition fluxes in atmospheric bulk samples in Masan and Haengam areas ranged from 135 to $464\;{\mu}g/m^2/year$ and from 62.2 to $194\;{\mu}g/m^2/year$, respectively. Atmospheric deposition fluxes of particles and PAHs in this study were comparable to or slightly lower values than those from different locations in Korea and other countries. PAHs profiles of atmospheric deposition bulk samples showed slightly different from two sampling areas, however the predominant species of PAHs were similar. Indeno (1,2,3-c,d)pyrene, benzo(g,h,i)perylene, phenanthrene compounds were the most detected PAHs in deposition bulk samples. Carcinogenic PAHs occupied the contribution of approximately $30-40\%$ of the total PAHs deposition fluxes. The non-metric multi-dimensional scaling (MDS) was used, to assess the differentiation of PAHs source between two sampling areas. The result suggests that PAHs contamination sources were different according to the location and season surveyed. There was no an apparent relationship between the PAHs deposition flux against temperature and rainfall amount, even though summer season with the highest temperature and the largest amount of precipitation showed the lowest PAHs deposition flux. Benzo(e)pyrene/benzo(a)pyrene ratio indicated that the photo-degradation process was one of important factors to the seasonal variation of PAHs with the lower deposition fluxes.

Bulk and Surface Reactions of Atomic H with Crystalline Si(100)

  • 조삼근
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2000년도 제18회 학술발표회 논문개요집
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    • pp.175-175
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    • 2000
  • Si(100) surfaces were exposed to gas-phase thermal-energy hydrogen atoms, H(g). We find that thermal H(g) atoms etch, amorphize, or penetrate into the crystalline silicon substrate, depending on the employed Ts range during the H(g) exposure. We find that etching is enhanced as Ts is lowered in the 300-700K range, while amorphous silicon hydride (a-Si:H) formation dominates at a Ts below 300K. This result was well explained by the fact that formation of the etching precursor, SiHx(a), and amorphization are both facilitated by a lower Ts, whereas the final step for etching, SiH3(a) + H(g) longrightarrow SiH3(g), is suppressed at a lower Ts. we also find that direct absorption of H(g) by the crystalline bulk of Si(100) substrate occurs within a narrow Ts window of 420-530K. The bulk-absorbed hydrogen evolved out molecularly from Si(100) at a Ts 80-120K higher than that for surface monohydride phase ($\beta$1) in temperature-programmed desorption. This bulk-phase H uptake increased with increasing H(g) exposure without saturation within our experimental limits. Direct absorption of H(g) into the bulk lattice occurs only when the surface is atomically roughened by surface etching. While pre-adsorbed hydrogen atoms on the surface, H(a), were readily abstracted and replaced by D(g), the H atoms previously absorbed in the crystalline bulk were also nearly all depleted, albeit at a much lower rate, by a subsequent D(g) at the peak temperature in TPD from the substrate sequentially treated with H(g) and D(g), together with a gas phase-like H2 Raman frequency of 4160cm-1, will be presented.

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Prediction of Air Movement and Temperature Distribution at Different Store Methods Using 3-D CFD Simulation in Forced-Air Cooling Facility

  • Yang, G.M.;Koh, H.K.
    • Agricultural and Biosystems Engineering
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    • 제3권2호
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    • pp.65-72
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    • 2002
  • Temperature is the most influential environment parameter which affects the quality change of agricultural products in cold storage. Therefore, it is essential to keep the uniform temperature distribution in the storage room. This study was performed to analyze the air movement and temperature distribution in the forced recirculating cold storage facility and to simulate optimum storage method of green groceries using 3-D CFD(three dimensional computational fluid dynamics) computer simulation which applied the standard $textsc{k}$-$\varepsilon$ turbulence model and FVM(finite volume method). The simulation was validated by the experimental results for onion storage and the simulation model was used to simulate the temperature and velocity distribution in the storage room with reference to the change of storage method such as location of storage, no stores, bulk storage, and pallet storage. In case of no stores, internal airflow was circulated without stagnation and consequently air movement and temperature distribution were uniform. In case of bulk storage, air movement was stagnated so much and temperature distribution of onion was not uniform. Furthermore, the inner temperature of onion roses more than the initial temperature of storage. In case of pallet storage, air movement and temperature distribution of onion were so uniform that the danger of quality change was decreased.

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고온 확산공정에 따른 산화막의 전기적 특성 (Electrical Characteristics of Oxide Layer Due to High Temperature Diffusion Process)

  • 홍능표;홍진웅
    • 대한전기학회논문지:전기물성ㆍ응용부문C
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    • 제52권10호
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    • pp.451-457
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    • 2003
  • The silicon wafer is stable status at room temperature, but it is weak at high temperatures which is necessary for it to be fabricated into a power semiconductor device. During thermal diffusion processing, a high temperature produces a variety thermal stress to the wafer, resulting in device failure mode which can cause unwanted oxide charge or some defect. This disrupts the silicon crystal structure and permanently degrades the electrical and physical characteristics of the wafer. In this paper, the electrical characteristics of a single oxide layer due to high temperature diffusion process, wafer resistivity and thickness of polyback was researched. The oxide quality was examined through capacitance-voltage characteristics, defect density and BMD(Bulk Micro Defect) density. It will describe the capacitance-voltage characteristics of the single oxide layer by semiconductor process and device simulation.

BaTiO$_3$계 세라믹 박막의 제조와 PTC특성 (Preparation and PTC Properties of Thin Films BaTiO$_3$ System)

  • 박춘배;송민옹;김태완;강도열
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1994년도 춘계학술대회 논문집
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    • pp.17-20
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    • 1994
  • PTCRl(positive temperature coefficient of resistivity) thermistors in the thin file BaTiO$_3$ system were deposited by radio frequency (13.56 MHz) and dc radio frequency (13.56MHz) and dc magnerton sputter equipment. R-T(resistivity -temperature) properties was investigated as a function of substrate and the temperature variation. The specimens make a comperison between the thin films and the bulk in the resistivity variation. Substrate temperature. deposition time. and forward power are deposited at the 400$^{\circ}C$, 10 hours, and 210 watt. respectively. The aim of this work is to obtain lower than bulk specimen resistivity in thin films BaTiO$_3$ system thermistor by RF/DC magnetron sputter equipment.

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소결온도에 따른 $Ba_{5}Ta_{4}O_{15}$ 세라믹스의 구조 밀 마이크로파 유전특성 (Structural and Microwave Dielectric Properties of the $Ba_{5}Ta_{4}O_{15}$ Ceramics with Sintering Temperature)

  • 이승준;김재식;남송민;고중혁;이영희
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2006년도 제37회 하계학술대회 논문집 C
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    • pp.1355-1356
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    • 2006
  • The microwave dielectric properties of the $Ba_{5}Ta_{4}O_{15}$ ceramics with sintering temperature were investigated. All sample of the $Ba_{5}Ta_{4}O_{15}$ ceramics prepared by conventional mixed oxide method and sintered at $1450^{\circ}C{\sim}1575^{\circ}C$. Porosity of the $Ba_{5}Ta_{4}O_{15}$ ceramics was reduced with increasing sintering temperature. The bulk density, dielectric constant and Qualify factor increased with increasing sintering temperature. In the case of $Ba_{5}Ta_{4}O_{15}$ ceramics sintered at $1550^{\circ}C$, The bulk density, dielectric constant and quality factor were $7.31g/cm^2$ and 27.4, 30,635GHz, respectively.

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벌크 비정질 합금의 초저온 소성 (Enhanced Plasticity of Bulk Amorphous Alloys at Cryogenic Temperature)

  • 윤규상;이미림;이재철
    • 대한금속재료학회지
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    • 제48권8호
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    • pp.699-704
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    • 2010
  • We investigated the cryogenic temperature plasticity of a bulk amorphous alloy. Experiments showed that as temperature decreases, the plasticity of the alloy increases, such that the alloy exhibited ~20% of plastic strain when tested at $-196^{\circ}C$. This enhancement in the plasticity at cryogenic temperatures was associated with the formation of abundant shear bands distributed uniformly over the entire surface of the sample. Nonetheless, the serrations, the characteristic feature of the plastic deformation of amorphous alloys, were unclear at $-196^{\circ}C$. In this study, both the enhanced plasticity and the unclear serrations exhibited by the amorphous alloy at cryogenic temperatures were clarified by exploring shear banding behaviors in the context of the velocity and the viscosity of a propagating shear band.

인공위성관측 해수면온도와 현장관측 수온의 비교를 통해 본 해양 피층-표층 수온의 차이 (Oceanic Skin-Bulk Temperature Difference through the Comparison of Satellite-Observed Sea Surface Temperature and In-Situ Measurements)

  • 박경애
    • 대한원격탐사학회지
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    • 제24권4호
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    • pp.273-287
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    • 2008
  • 1994년부터 2003년까지 임의로 선택한 달들에 대하여 NOAA/AVHRR 인공위성 자료와 해양 현장수온 관측 자료사이에서 획득된 845개의 일치점 자료를 활용하여 북동아시아 해역에서 해양 피층-표층 해수면온도 차이의 특성을 분석하였다. 해양상층 수 m내에서의 해수면온도의 일간 변화를 이해하기 위하여 일치점 데이터베이스는 낮과 밤, 표층 뜰개-선박 관측에 따라서 모두 네 가지 부류로 분류하였다. 주간표층 뜰개에 의한 수온 자료는 인공위성 해수면온도와 $0.56^{\circ}C$의 가장 작은 제곱평균오차를 보여서 위성관측 수온과 가장 잘 일치하였다. 주간 선박관측에 의한 CTD 수온 자료는 $1.12^{\circ}C$의 큰 제곱평균오차를 보여서 네 부류 중에서 가장 좋지 않은 정확도를 보였다. 위성 해수면온도와 현장 관측 해수면온도의 차이는 그 외에도 대기의 수증기 함량 효과, 연안으로부터 거리의 영향 등 다양한 요인에 의해 발생하였다. 그 중에서 가장 주목할 만한 오차는 수 m 이내 수온의 수직적 구조의 일간 변화에서 발생하였으며, 이는 표층 부이는 20 cm 정도, 선박 관측기기는 수 m현장에서 서로 다른 깊이의 수온을 관측하기 때문에 발생한 것으로 판단된다. 본 연구는 그동안 광범위하게 사용되어온 위성 SST는 어떤 경우에는 ${\pm}3^{\circ}C$의 큰 오차를 만들 수 있으므로 국지적 해양에서 해양 피층-표층 해수면온도 차이와 수온의 수직적 구조에 대한 보다 깊은 이해가 뒷받침되어야 하며, 이를 바탕으로 위성 SST를 사용자의 목적에 맞추어 주의 깊게 사용되어야 함을 제시한다.

Estimation of the air temperature over the sea using the satellite data

  • Kwon B. H.;Hong G. M.;Kim Y. S.
    • 대한원격탐사학회:학술대회논문집
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    • 대한원격탐사학회 2005년도 Proceedings of ISRS 2005
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    • pp.392-393
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    • 2005
  • Due to the temporal and spatial simultaneity and the high-frequency repetition, the data set retrieved from the satellite observation is considered to be the most desirable ones for the study of air-sea interaction. With rapidly developing sensor technology, satellite-retrieved data has experienced improvement in the accuracy and the number of parameters. Nevertheless, since it is still impossible to directly measure the heat fluxes between air and sea, the bulk method is an exclusive way for the evaluation of the heat fluxes at the sea surface. It was noted that the large deviation of air temperature in the winter season by the linear regression despite good correlation coefficients. We propose a new algorithm based on the Fourier series with which the SST and the air temperature. We found that the mean of air temperature is a function of the mean of SST with the monthly gradient of SST inferred from the latitudinal variation of SST and the spectral energy of air temperature is related linearly to that of SST. An algorithm to obtain the air temperature over the sea was completed with a proper analysis on the relation between of air temperature and of SST. This algorithm was examined by buoy data and therefore the air temperature over the sea can be retrieved based on just satellite data.

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