• Title/Summary/Keyword: bulk specific

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An HPLC-UV-based quantitative analytical method for Chrysanthemum morifolium: development, validation, and application

  • Jung, Dasom;Jin, Yan;Kang, Seulgi;Lee, Heesoo;Park, Keunbae;Li, Ke;Kim, Jin Hak;Geum, Jeong Ho;Lee, Jeongmi
    • Analytical Science and Technology
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    • v.32 no.4
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    • pp.139-146
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    • 2019
  • A simple and reliable analytical method based on high-performance liquid chromatography-ultraviolet detection was established for the analysis of the flowers of Chrysanthemum morifolium (CM). Luteolin-7-O-glucoside (LU7G) was chosen as a target analyte considering its content, availability, and ease of analysis. Chromatographic separation of LU7G was achieved using a Phenomenex Gemini $C_{18}$ column ($250{\times}4.6mm$, $5{\mu}m$) run with a mobile phase consisting of 0.5 % acetic acid in water and 0.5 % acetic acid in acetonitrile at a flow rate of $1.0mL\;min^{-1}$. The detection wavelength and column temperature were set at 350 nm and $40^{\circ}C$, respectively. Method validation was performed according to the AOAC guidelines and the method was specific, linear ($R^2=0.9991$ for $50-300{\mu}g\;mL^{-1}$), precise (${\leq}3.91%$RSD), and accurate (100.1-105.7 %). The limits of detection and quantification were 3.62 and $10.96{\mu}g\;mL^{-1}$, respectively. The established method was successfully applied to determine the contents of LU7G in various batches of bulk CM extracts and labscale CM extract. The developed method is a readily applicable method for the quality assessment of CM and its related products.

Allocation Techniques for NVM-Based Fast Storage Considering Application Characteristics (응용의 특성을 고려한 NVM 기반 고속 스토리지의 배치 방안)

  • Kim, Jisun;Bahn, Hyokyung
    • The Journal of the Institute of Internet, Broadcasting and Communication
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    • v.19 no.4
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    • pp.65-69
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    • 2019
  • This paper presents an optimized adoption of NVM for the storage system considering application characteristics. To do so, we first characterize the storage access patterns for different application types, and make two prominent observations that can be exploited in allocating NVM storage efficiently. The first observation is that a bulk of I/O does not happen on a single storage partition, but it is varied significantly for different application categories. Our second observation is that there exists a large proportion of single accessing in storage data. Based on these observations, we show that maximizing the storage performance with NVM is not obtained by fixing it as a specific storage partition but by allocating it adaptively for different applications. Specifically, for graph, database, and web applications, using NVM as a swap, a journal, and a file system partitions, respectively, performs well.

Investigation of the Light Reflection from Dielectric Thin Films Coated on Substrates (기판 위에 입혀진 유전체 박막의 빛 반사에 관한 연구)

  • Kim, Deok Woo;Kim, Jiung;Kim, Byoung Joo;Cha, Myoungsik
    • Korean Journal of Optics and Photonics
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    • v.31 no.6
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    • pp.321-327
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    • 2020
  • We investigated the light reflection from thin films coated on substrates. Using a prism with a high refractive index as the incident medium, the phenomena of the total internal reflection (TIR) of the prism/film/substrate system and the light coupling into the optical waveguide formed by the air/film/substrate system were comprehensively studied and compared. If the refractive index of the thin film is greater than that of the substrate, within the TIR region of the substrate, sharp reflection minima occur at specific angles where the waveguide modes are excited, that can be used to accurately measure the refractive index and thickness of a thin film. On the other hand, if the refractive index of the thin film is smaller than that of the substrate, such waveguide modes do not exist. In this case, although not so distinct as a bulk medium, the TIR effect of the thin film is still observable, accompanied by an interference pattern. In this study we analyzed the overall reflection phenomena occurring from prism/film/substrate structures, to investigate the possibility of measuring the refractive index of a thin film in both cases.

Synthesis of Cobalt Hydroxide Nanosheets based on Sonication-induced Exfoliation for Depolymerization of Polyethylene Terephthalate (폴리에틸렌 테레프탈레이트의 해중합을 위한 초음파 박리법 기반의 코발트 수산화물 나노시트의 제조)

  • Jin, Se Bin;Son, Seon Gyu;Jeong, Jae-Min;Choi, Bong Gill
    • Applied Chemistry for Engineering
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    • v.31 no.6
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    • pp.668-673
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    • 2020
  • In this work, ultrathin and two-dimensional (2D) cobalt hydroxide [Co(OH)2] nanosheets were synthesized by a sonication assisted liquid-phase exfoliation of bulk Co(OH)2. The resulting exfoliated Co(OH)2 is a hexagonal mono-layered nanosheet with a high specific surface area of 27.5 ㎡ g-1. The depolymerization of polyethylene terephthalate (PET) based on glycolysis reaction was also performed using an exfoliated Co(OH)2 catalyst. Excellent catalytic reaction performances were demonstrated; a high PET conversion and bis(2-hydroxyethyl) terephthalate (BHET) yield of both 100% using the nanosheet catalyst were achieved within a reaction time and temperature of 30 min and 200 ℃, respectively. The long-term stability of exfoliated Co(OH)2 catalysts was also demonstrated by recyclability tests of the catalyzed glycolysis reaction of PET over four cycles, showing both 100% of high PET conversion and BHET yield.

Effects of pulsed laser surface remelting on microstructure, hardness and lead-bismuth corrosion behavior of a ferrite/martensitic steel

  • Wang, Hao;Yuan, Qian;Chai, Linjiang;Zhao, Ke;Guo, Ning;Xiao, Jun;Yin, Xing;Tang, Bin;Li, Yuqiong;Qiu, Shaoyu
    • Nuclear Engineering and Technology
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    • v.54 no.6
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    • pp.1972-1981
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    • 2022
  • A typical ferritic/martensitic (F/M) steel sheet was subjected to pulsed laser surface remelting (LSR) and corrosion test in lead-bismuth eutectic (LBE) at 550 ℃. There present two modification zones with distinct microstructures in the LSRed specimen: (1) remelted zone (RZ) consisting of both bulk δ-ferrite grains and martensitic plates and (2) heat-affected zone (HAZ) below the RZ, mainly composed of martensitic plates and high-density precipitates. Martensitic transformation occurs in both the RZ and the HAZ with the Kurdjumov-Sachs and Nishiyama-Wassermann orientation relationships followed concurrently, resulting in scattered orientations and specific misorientation characteristics. Hardnesses of the RZ and the HAZ are 364 ± 7 HV and 451 ± 15 HV, respectively, considerably higher than that of the matrix (267 ± 3 HV). In oxygen-saturated and oxygen-depleted LBE, thicknesses of oxide layers developed on both the as-received and the LSRed specimens increase with prolonging corrosion time (oxide layers always thinner under the oxygen-depleted condition). The corrosion resistance of the LSRed F/M steel in oxygen-saturated LBE is improved, which can be attributed to the grain-refinement accelerated formation of dense Fe-Cr spinel. In oxygen-depleted LBE, the growth of oxide layers is very low with both types of specimens showing similar corrosion resistance.

Analysis of Factor Affecting for Improving Construction Engineering Market

  • Park, Junho;Yu, Jungho
    • International conference on construction engineering and project management
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    • 2015.10a
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    • pp.450-453
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    • 2015
  • The Construction Engineering Industry (CEI) is construction field based on professional knowledge, staff and information service, and is distinguished by construction activity. The contemporary CEI market has extended globally and diversified construction work classifications. International construction engineering companies now have an important economic and social effect. Over the last five years (2009 to 2013), the top-200 global engineering firms reported global revenue that grew from 54.4 billion to 71.5 billion, about 27% growth (ENR, 2014). Countries such as the U.S.A., Canada, those in Europe (Several developed countries, i.e., United Kingdom, Netherlands, France, Spain, France, Italy, and Spain), Australia, Japan, China, and Korea comprise the bulk of world construction engineering revenue. Although the construction engineering market continues to grow, much of the work is limited to Europe, mid-Asia, and Asia. Additionally, specific construction types are focused on building projects, industrial plants, and refining plants. As such, there are imbalances in the construction engineering market and some market saturation. Further, there is heavy competition and the construction engineering market may shrink in the future. This paper analyzed various factors affecting the construction engineering market, specifically looking at construction classifications and factors related to a global market. To accomplish this, we collected to data from Engineering News Record (ENR) and recast each variable. And we used nonparametric statistics because the number of cases were small, making it difficult to assume a case's population parameter. Then we tested with the Kruskal-Wallis test and drew results. The results indicate that concentration in particular construction types and extending global regional markets will be have a positive effect on the overall global construction engineering market..

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Positive Effects of Humic Substances on Plant Growth and Biological Soil Indicators when Spring barley is Green Manured on Reclaimed Soils (처리토에 녹비 식물 청보리 경작 시 휴믹 물질이 식물생장 및 생물학적 토양 인자에 주는 긍정적 영향)

  • Sua Kang;Hyesun Park;Younrho Lee;Bumhan Bae
    • Journal of Soil and Groundwater Environment
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    • v.29 no.1
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    • pp.51-62
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    • 2024
  • A study was performed to investigate the positive impacts of humic substances (HS) on the growth of green barley, a type of green manure plant. The study was conducted in a pot culture using two different types of reclaimed soils that had been treated by land farming (DDC) and thermal desorption (YJ) methods, respectively. The experimental conditions consisted of three treatments: plant only (P), plant plus 2% HS, and no plant (control). After 89 days of culture in a controlled growth chamber, the growth of spring barley and activity of seven soil enzymes were measured. The results indicated that the addition of HS had a substantial (p<0.10) positive effect on shoot biomass in both types of soil. Furthermore, the addition of HS notably (p<0.05) enhanced all seven soil enzyme activities in both soils. Both the aboveground and belowground parts of barley plants were returned to soil and aged for 10 weeks in the same growth chamber, which resulted in notable enhancement in soil health indicators. These improvements included an increase in organic matter, a drop in bulk density, and an increase in the activity of seven different soil enzymes. When lentil seeds were planted in the aged soils, the development of the seedlings was more vigorous than that in the control in both soils, although allelopathy of barley suppressed lentil germination in soil with pH 7.0 but not in soil with pH 8.5.

Single-cell RNA sequencing reveals the heterogeneity of adipose tissue-derived mesenchymal stem cells under chondrogenic induction

  • Jeewan Chun;Ji-Hoi Moon;Kyu Hwan Kwack;Eun-Young Jang;Saebyeol Lee;Hak Kyun Kim;Jae-Hyung Lee
    • BMB Reports
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    • v.57 no.5
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    • pp.232-237
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    • 2024
  • This study investigated how adipose tissue-derived mesenchymal stem cells (AT-MSCs) respond to chondrogenic induction using droplet-based single-cell RNA sequencing (scRNA-seq). We analyzed 37,219 high-quality transcripts from control cells and cells induced for 1 week (1W) and 2 weeks (2W). Four distinct cell clusters (0-3), undetectable by bulk analysis, exhibited varying proportions. Cluster 1 dominated in control and 1W cells, whereas clusters (3, 2, and 0) exclusively dominated in control, 1W, and 2W cells, respectively. Furthermore, heterogeneous chondrogenic markers expression within clusters emerged. Gene ontology (GO) enrichment analysis of differentially expressed genes unveiled cluster-specific variations in key biological processes (BP): (1) Cluster 1 exhibited up-regulation of GO-BP terms related to ribosome biogenesis and translational control, crucial for maintaining stem cell properties and homeostasis; (2) Additionally, cluster 1 showed up-regulation of GO-BP terms associated with mitochondrial oxidative metabolism; (3) Cluster 3 displayed up-regulation of GO-BP terms related to cell proliferation; (4) Clusters 0 and 2 demonstrated similar up-regulation of GO-BP terms linked to collagen fibril organization and supramolecular fiber organization. However, only cluster 0 showed a significant decrease in GO-BP terms related to ribosome production, implying a potential correlation between ribosome regulation and the differentiation stages of AT-MSCs. Overall, our findings highlight heterogeneous cell clusters with varying balances between proliferation and differentiation before, and after, chondrogenic stimulation. This provides enhanced insights into the single-cell dynamics of AT-MSCs during chondrogenic differentiation.

Physical, Mechanical and Durability Properties of the Quartzite Units of Central Nepal Lesser Himalaya

  • Dinesh Raj Sharma;Naresh Kazi Tamrakar;Upendra Baral
    • The Journal of Engineering Geology
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    • v.34 no.1
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    • pp.67-105
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    • 2024
  • This study compares the quartzites of four quartzite units: The Fagfog Quartzite, Dunga Quartzite (member of the Robang Formation), Pandrang Quartzite (member of the Kalitar Formation) and the Chisapani Quartzite. The analysis shows variations in flakiness and elongation, as the Fagfog Quartzite displays low flakiness whereas the Pandrang and the Chisapani have moderate and the Dunga Quartzite has shown variations. The density values of the four quartzite units remain consistent, indicating uniform physical properties and porosity levels. However, bulk density values differ among the quartzites, suggesting variations in particle arrangement, porosity, and density. Regarding strength measures, the Pandrang and the Chisapani Quartzite have higher strength characteristics as compared to the Fagfog and the Dunga Quartzites. The Pandrang Quartzite has the highest average point load strength index, classifying it as "Extremely Strong". The resistance to impact and crushing forces varies among the quartzites, with lower Aggregate Impact Value (AIV) and Aggregate Crushing Value (ACV) indicating higher strength and durability. Durability tests show that the Fagfog Quartzite has high durability against slaking, with a slight decrease observed after the fifth cycle. The Dunga Quartzite shows varying degrees of weathering, while the Pandrang and the Chisapani Quartzite have minimal weight changes, indicating strong resistance to weathering. Magnesium sulfate soundness tests indicate high durability and resistance to degradation for all four units. The Los Angeles abrasion value (LAAV) tests indicate favorable resistance to abrasion for the majority of the Fagfog, Dunga, and the Pandrang Quartzites samples, while Chisapani Quartzite shows more variability in LAAV values. The Pandrang Quartzite shows a higher proportion of elongated particles but lower flakiness index values as compared to Fagfog and Dunga Quartzites while Chisapani Quartzite stands out with a significantly higher presence of flaky particles and lower elongation index values. Mechanically, the Fagfog and Dunga Quartzite show higher strength and better resistance to abrasion and freeze and thaw. The Pandrang Quartzite shows moderate resistance to crushing and sudden effect, while the Chisapani Quartzite has variable resistance to effect. This comparative study emphasizes the diversity and complexity of quartzite rock types, showing the need for comprehensive characterization and assessment to determine their suitability for specific applications.

A method to obtain radioactivity of non-γ nuclides by 60Co based on Monte Carlo simulations

  • Yingbo Shi;Yulin Xiang;Rongbo Su;Bitao Hu;Shaohua Sun;Zuoye Liu
    • Nuclear Engineering and Technology
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    • v.56 no.10
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    • pp.4134-4140
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    • 2024
  • Source term investigation is a critically important aspect of reactor decommissioning, particularly as the range of nuclides under consideration expands beyond the capabilities of existing analysis methods. In this study, we try to propose a methodology to indirectly determine the radioactivity of long-lived nuclides which are non-γ or low energy in various nuclear waste materials by measuring the radioactivity of 60Co. The critical point of this method is to establish relationship between some easy to measure (ETM) key nuclides, such as certain γ emitters (like 60Co), and the difficult to measure (DTM) nuclides to derive information for the DTM nuclides of interest. To begin, we calculate nuclide bulk densities of 55Fe, 60Co, 63Ni and 152Eu in nuclear waste materials. By constructing inversion matrices and analyzing the intensity matrices of characteristic γ lines emitted by 60Co, we can extract the radioactivity of non-γ radionuclides (55Fe, 63Ni, and 152Eu) present in the nuclear waste materials that are contained within a specific container. Furthermore, our methodology accounts for the influence of voids within the container, thereby ensuring the reliability and validity of the obtained results. This innovative approach offers a promising avenue for efficiently sorting nuclear waste.