• Elastomers and Composites
• /
• v.49 no.3
• /
• pp.245-252
• /
• 2014

FT-IR measurement and the physical properties of polyurethane adhesive prepared from the polyol, isocyanate, 2-HEMA and other acrylate monomers were examined. The softening point, viscosity, adhesion strength and mechanical properties of the PU adhesives were reviewed by Ring and Ball method, Brookfield viscometer and universal test machine, respectively. Results revealed that increment of both PPG amount and butyl acrylate content decreased softening point, adhesion strength, tensile strength and 100% modulus. However as 2-HEMA and MDI content increased the mechanical properties including tensile strength, 100% modulus increased, and also the viscosity and NCO content increased.

• KSTLE International Journal
• /
• v.8 no.1
• /
• pp.16-20
• /
• 2007

This study introduces a new approach to a falling ball viscometer by using a high speed motion camera to measure the viscosity of both Newtonian and non-Newtonian fluids from the velocity-time data. This method involves capturing continuous photographs of the entire falling motion of the ball as the ball accelerates from the rest to the terminal velocity state. The velocity of a falling ball was determined from the distance traversed by the ball by examining video tape frame by frame using the marked graduations on the surface of the cylinder. Each frame was pre-set at 0.01. Glycerin 74% was used for Newtonian solution, while aqueous solutions of Polyacrylamide and Carboxymethyl Cellulose were for non-Newtonian solutions. The experimental viscosity data were in good agreements with the results obtained from a rotating Brookfield viscometer.

• YAKHAK HOEJI
• /
• v.36 no.6
• /
• pp.538-547
• /
• 1992

Optimal synthetic condition of barium sulfate were investigated from the viewpoint of yield and bulkiness according to a randomized complete block design proposed by G.E.P. Box and K.B. Wilson. Barium chloride and magnesium sulfate were utilized as reactants in order to prepare barium sulfate in this study. It was found that optimum temperature range of reactant solutions was $60{\sim}100^{\circ}C$ and the optimum concentration range of the reactant solutions was $10{\sim}17.3%$ and $10{\sim}20%$ respectively, on the viewpoint of yield and bulkiness. The optimum mole ratio of $BaCI_2$ to $BaSO_4$ was in the range of $1.50{\sim}2.0$ and the optimum mole ratio of $BaCI_2$ to $BaSO_4$ was in the range of $1.50{\sim}2.0$ and the optimum reacting time range was $15{\sim}20$ minutes. The optimum drying temperature range was $110{\sim}130^{\circ}C$ from the viewpoint of yield, but it was $90{\sim}110^{\circ}C$ on the basis of bulkiness. Apparent viscosity of barium sulfate suspensions dispersed in various concentrations of Na. CMC was measured by using Brookfield synchrolectric viscometer model LVT, the relative equation, log ${\eta}_{sp}=A+B.{\phi}$ was examined and the equation was found to agree fairly well. 1 w/v% Na. CMC aqueous solution and 0.1 volume fraction of $BaSO_4$ powder were optimum in the preparation of $BaSO_4$ suspension showing highest viscosity at infinite shearing.

• Journal of Food Hygiene and Safety
• /
• v.16 no.1
• /
• pp.82-87
• /
• 2001

A study was performed to establish detection methods by viscometric and pulsed photostimulated luminescence (PPSL) methods for irradiated com powder. Viscosity was determined using a Brookfield DV-rotation viscometer at 3$0^{\circ}C$ and operated at 30, 60, 90, 120, 150, 180, and 210 rpm. All irradiated samples showed a decrease in Viscosity with increasing stirring speeds (rpm) and irradiation doses. Treatments at 1~3 kGy significantly decreased the viscosity. The photon counts of irradiated corn powder were measured by PPSL immediately after irradiation and exhibited an increase with increasing irradiation dose. The photon counts of irradiated com powder almost disappeared with lapse of time in room conditions, but detection of irradiation was still possible after one month at darkroom conditions. Consequently, these results suggest that the detection of irradiated com powder is possible by both viscometric and PPSL methods.

• Proceedings of the SOHE Conference
• /
• 1997.12a
• /
• pp.45-49
• /
• 1997

To study the effect of amylose on the mechanism of gel formation, swelling power, water solubility, the pattern of alkali gelatinization and gel properties were investigated. The swelling power of waxy maize starch(Amioca) was the highest and followed by those of PFP ＞Amaizo ＞ Amylomaize Ⅶ. Amioca showed higher iodine affinity of soluble amylose than other maize starches. The apparent viscosity of alkali gelatinization measured by Brookfield viscometer for Amaizo was $70{\pm}10^3cp$ which was higher than Amylomaize VII. The apparent viscosity of PFP was increased to $70{\pm}10^3cp$ and then decreased. As maize starches were autoclaved at $121^{\circ}C$ with starch : water ratio (1:9) and autoclaving-cooling cycle were up to 4 times, gel properties were measured by rheometer. Amaizo showed the highest value for hardness, adhesiveness, springiness, cohesiveness, and hardness of gel after two times of autoclaving-cooling cycles was the highest. Gel properties was thus affected by the chain length of amylose rather than amylose content.

• Korean Journal of Human Ecology
• /
• v.3 no.1
• /
• pp.88-99
• /
• 2000

This study was perfomed to search for how properties of the starch viscosity appear in different qualities, when acetic acid is added. For this study, corn starch which belongs to A-type. Potato starch to B-type. and sweet potato starch to C-type were chosen as an experimental material. which was added to acetic acid controlled as pH 4.0, 4.5, and 5.0 at the time of before and after heating. After that, the viscosity properties of each starch was analyzed using Amylogram and Brookfield viscometer. As a result. the viscosity was shown high in an order of potato. sweet potato, and corn starch. According to addition of acetic acid. tile viscosity appeared to be low. The viscosity differences of before and after heating when the acid is added were shown as follows : Amylogram shows that the lower the pH is. the lower the viscosity is when the acid is added before-heating. In case the acid is added before-heating, gelatinization temperature, consistency and setback was increased. but breakdown decreased. In case the acid is added after-heating, the viscosity goes down at soon as it is added meanwhile consistency and setback was decreased. but breakdown increased. Such properties of the viscosity show a conspicuous variation in an order of potato. sweet Potato. and corn starch. Brookrield viscometer shows that the lower the apparent viscosity is. the lower pH is at the time of before-heating when the acid is added. In case of after-heating, when the acid is added. the apparent viscosity shows a higher inclination than that of before-heating in corn starch and sweet potato starch.

• Journal of the Korean Society of Marine Environment & Safety
• /
• v.22 no.2
• /
• pp.240-245
• /
• 2016

This paper describes the rheological behavior study such as viscosity and change of shear stress regarding marine lubricating oil according to the amount of Marine Gas Oil (MGO) dilution. The viscosity reduction due to fuel dilution is crucially important characteristic to decreasing engine durability because of the abrasion of piston ring or liner. The lubricating oil used in this paper was blended with magnetic stirrer diluted High Sulfur Diesel (HSD, 0.05 wt%) ratio of 3 %, 6 %, 10 %, 15 % and 20 %. The viscosity and shear stress of diluted lubricating oil were measured with the temperature range from $-10^{\circ}C$ to $80^{\circ}C$ using a rotary viscometer (Brookfield Viscometer). As the amount of MGO dilution increasing in lubricating oil, the viscosity and stress of those decreased, because the lubricating oil diluted MGO with low viscosity show the trends to decreased viscosity and shear stress. Especially, the viscosity and shear stress of lubricating oil radically decreased at low temperature ($0{\sim}-10^{\circ}C$) and doesn't effect in MGO dilution at over $40^{\circ}C$. As temperature risen, the reduction of the viscosity and shear stress in lubricating oil shows the Newtonian behavior. The lubricating oil was required to check up periodically to improve engine durability since the viscosity reduction by MGO dilution accelerating the engine abrasion.

• Proceedings of the Korea Concrete Institute Conference
• /
• 2004.05a
• /
• pp.616-619
• /
• 2004

This study has focused on the possibility for recycling of tailings from the Sangdong tungsten mine as powder. The experimental tests for entrapped water ratio were carried out in accordance with the specificed method by Okamura. The rheological measurements of cement paste were conducted by using a commerically digital Brookfield viscometer (Model LVDV-II+) equipped with cylindrical spindles. The results of this study, in case of cement paste mixed with tailings, entrapped water ratio was decreased with increasement of mixing ratio. Thickness of pseudo water film was increased, and mean plastic viscosity was decreased with increasing replacement.

• Proceedings of the Korean Society for Applied Microbiology Conference
• /
• 1986.12a
• /
• pp.532.1-532
• /
• 1986

유산균이 생성하는 polysaccharide 에 관한 연구의 일환으로서 L. casei YIT 9018 SKD-0007, L. bulgaricus SKD-0003, sir. faecalis SKD-1007, str. thermophilus SKD- 1005, str. thermophilus 510 SKD-1006등을 탈지유에 배양하면서 polysaccharide 생성에 의한 배양액의 점도 변화를 검토하였다. 이러한 다당류가 Antitumor로서의 활성과 제암효과를 가지며 인체내의 생리효과를 고양시킨다고 보고되어 있는바 다당류가 최대로 생성되는 조건을 찾는 것을 본 실험의 목적으로 하였다. 다당류의 생성을 측정하는 방법으로서 배지로는 10% 환원탈지유와 12% 환원전지유를 선택하였으며 Brookfield Viscometer를 사용하여 배양액의 점도를 경시적으로 측정하였다. 시험균 중에서 str. thermophilus 510 SKD-1006이 가장 높은 점도를 나타내었는데 41$^{\circ}C$ 배양 5일째에 5000 cps였고 다른균에 비해서 1000cps이상 높았다. 접종량이 증가할수록 점도도 증가하였으며 14%이상의 탈지유 농도에서는 7000cps를 나타냈다. 탈지유와 전지유 배양액 모두 의가소성 유체의 유동 양식을 나타내었는데 12% 환원전지유 배양액은 최대점도값이 2500 cps에 불과하였으며 배양 2일째에 최대점도 값에 도달하여 그 이후로 급격한 감소현상을 보였다.

• Journal of the Korean Chemical Society
• /
• v.16 no.1
• /
• pp.25-32
• /
• 1972

The effect on the apparent viscosity of 2 wt. % Veegum suspensions of different types of electrolytes and of different electrolyte concentrations was studied. Measurements were made with a Brookfield Synchro-Lectric Viscometer, using no.3 spindle at 30 R.P.M. at $24^{\circ}C$. As electriolyte concentration increased, the apparant viscosity was observed to increase to a maximum and then to decrease. Changes in viscosity were in general agreement with predicted results based on the Hofmeister sequence and the Schulze-Hardy rule. The observed electrolyte effect on the apparent viscosity was discussed in terms of the Verwey-Overbeek theory.