• Title/Summary/Keyword: bonding glass

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Electrical and optical properties of FTO transparent conducting oxide film by spray pyrolysis and its XPS analysis based on F/Sn ratio (분무열분해법에 의하여 제조한 FTO 투명전도막의 F/Sn 비율에 따른 전기, 광학적 특성과 XPS 분석)

  • Song, Chul-Kyu;Kim, Chang-Yeoul;Huh, Seung-Hun;Riut, Doh-Hyung;Choa, Yong-Ho
    • Korean Journal of Materials Research
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    • v.17 no.7
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    • pp.376-381
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    • 2007
  • Fluorine-doped tin oxide (FTO) thin film was coated on aluminosilicate glass at $450^{\circ}C$ by spray pyrolysis method. In the range of 0-2.7 molar ratio of F/Sn, the variations of electrical conductivity and visible light transmission were investigated. At the F/Sn ratio of 1.765, the film showed the lowest electrical resistivity value of $3.0{\times}10^{-4}{\Omega}\;cm$, the highest carrier concentration of $2.404{\times}10^{21}/cm^3$, and about $8\;cm^2/V{\cdot}sec$ of electronic mobility. The FTO film showed a preferred orientation of (200) plane parallel to the substrate. X-ray photoelectron spectroscopy analysis results indicated that the contents of $Sn^{4+}-O$ bonding are the highest at 1.765 of F/Sn molar ratio.

Preparation of Zeolite Membranes on Papers or Fibers (종이나 섬유를 지지체로 이용한 제올라이트 박막의 제조)

  • Song, Kyeong-Keun;Ha, Kwang
    • Korean Chemical Engineering Research
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    • v.43 no.6
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    • pp.691-695
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    • 2005
  • Zeolite membranes on various supports such as filter paper, cotton fiber, and glass fiber filter were prepared by secondary growth hydrothermal synthesis. First, zeolite NaA (${\approx}0.5{\mu}m$) and silicalite-1 (${\approx}0.2{\mu}m$) crystals were synthesized as zeolite seed crystals, and they were attached to the surfaces of the supports via chemical bonding. Zeolite NaA or silicalite-1 membranes could be synthesized on the supports coated with the seed crystals. The prepared zeolite membranes were observed by scanning electron microscope and analyzed by X-ray diffraction.

Morphology and Tensile Properties of Polyimide/Polyamideimide Composites from Different Polyimide Precursors (Polyimide 전구체에 따른 Polyimide/Ppolyamideimide 복합체의 형태학 및 인장 특성)

  • 김진봉;최윤희;임병탁;박준상
    • Polymer(Korea)
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    • v.25 no.2
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    • pp.160-167
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    • 2001
  • The various compositions of polyimide (PI)/polyamideimide (PAI) composites were prepared by heat treatment of the solvent cast PI precursors/PAI blends. The optical micrographs showed that a good compatibility was observed between poly(amic acid) (PAA) and PAI, but in the case of PAME/PAI mixtures, a phase separation apparently occurred due to the absence of ionic and/or H-bonding forces. Regardless of PI precursors, the similar tensile properties were observed. The tensile modulus of the composites were higher than that of the neat polyimide. The X-ray diffraction patterns of the composites showed that the chain rearrangement of PI was increased due to the plasticizing effect of PAI, which has lower glass transition temperature than that of PI, during thermal imidization process.

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Co-Fe-B 자왜변환기를 이용한 간섭계형 광섬유 자계센서의 동작특성

  • 이경식
    • Korean Journal of Optics and Photonics
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    • v.4 no.4
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    • pp.474-479
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    • 1993
  • An interferometric fiber-optic magnetic field sensor is constructed by bonding a Co-Fe-B metallic glass transducer developed here by the melt-spun method to a single mode fiber arm in the fiber Mach-Zehnder interferometer and is tested. The bias field for the peak ac-sensitivity was observed near 0.97 Oe and the minimum detectable magnetic field was 3.9${\times}10^{-5}$ Oe(rms)/${\sqrt{Hz}}$ a 3 kHz. The output of the ac field sensor becomes saturated near the input signal level of 1 Oe(rms). The Co- Fe-B transducer exhibits peak response near 500 Hz.

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Experimental Method for Evaluating Debonding Strength of FRPs Used for Retrofitting Concrete Structures (콘크리트 휨부재 보강용 FRP의 부착성능 평가를 위한 실험방법 연구)

  • Utui, Nadia;Kim, Hee-Sun
    • Journal of the Korean Society for Advanced Composite Structures
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    • v.2 no.3
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    • pp.36-41
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    • 2011
  • This study proposes a experimental method to evaluate bonding strength of FRPs used for retrofitting concrete structures. Specimens are designed so that debonding failure of FRPs can be induced from reinforced concrete beams retrofitted with two layers of carbon and glass FRPs. And three-point loading tests are performed to see if debonding failure with proper debonding strength is observed from the specimens. The test results show that the tested beams are failed due to debonding of FRPs, therefore, the proposed test method is capable of evaluating debonding strength of FRPs using relatively small normal strength concrete beams.

Mixing Efficiency Evaluation in Y-channel Micromixer Using LIF Confocal Microscope (LIF 공초점 현미경을 이용한 Y-채널 마이크로믹서의 혼합 효율 평가)

  • Kim, Kyoung-Mok;Shin, Yong-Su;Ahn, Yoo-Min;Lee, Do-Hyung
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.31 no.2 s.257
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    • pp.159-166
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    • 2007
  • Mixing between two or more reagents is one of important processes in biochemical microfluidics. In efficient micromixer design, it is essential to analyze flow pattern and evaluate mixing efficiency with good precision. In this work, mixing efficiency for Y-channel micromixer is measured by fluorescence intensity using LIF(Laser Induced Fluorescence) Confocal Microscope. The Y-channel micromixers are fabricated with polydimethylsiloxane(PDMS) and those are bonded to glass plate through Plasma bonding. Nile Blue A is injected into the micromixer as a fluorescence dye for measuring of fluorescence intensity by He/Ne laser. For visualization of the flow pattern, dynamic image capturing is carried out using CAM scope. For the comparison with computer simulation, modified SIMPLE algorithm for incompressible flow equation is solved for the same geometry as in the experiment. Throughout the experiments and computer simulation, accurate mixing efficiency evaluation process for a PDMS Y-channel micromixer is established.

Fluoride penetration from three orthodontic adhesives: an experimental study

  • Wagner, Leopold;Szepietowska, Magdalena
    • The korean journal of orthodontics
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    • v.43 no.1
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    • pp.29-34
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    • 2013
  • Objective: To examine the prophylactic potential of 3 orthodontic bonding adhesives: Fuji Ortho SC, Illuminate, and Resilience. Methods: Thirty-six Wistar Wag rats were randomly divided into 4 groups consisting of 9 rats each. One of the groups received no treatment and was used as a control. In the other groups, individual bands coated with one of the 3 adhesives were cemented to the lower incisors. Enamel samples were obtained after 6 and 12 weeks and analyzed using scanning electron microscopy in combination with energy dispersive spectrometry. Results: Six weeks after band cementation, no fluoride was found in the enamel of the lower incisors. After 12 weeks, there was no fluoride in the enamel of teeth coated with the Resilience composite. However, in the case of the Illuminate composite and the resin-modified glass ionomer Fuji Ortho SC cement, the depth of fluoride penetration reached $2{\mu}m$ and $4.8-5.7{\mu}m$, respectively. Conclusions: Fluoride ions from orthodontic adhesives can be incorporated into the surface layer of the enamel. Orthodontists may apply orthodontic adhesives, such as the Fuji Ortho SC, to reduce the occurrence of caries during orthodontic treatment with fixed appliances.

Study on Fluorine Penetration of Capping Layers using FTIR analysis (FTIR을 이용한 캐핑레이어의 플루오르 침투 특성 연구)

  • Lee, Do-Won;Kim, Nam-Hoon;Kim, Sang-Yong;Kim, Tae-Hyoung;Chang, Eui-Goo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.07a
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    • pp.300-303
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    • 2004
  • To fill the gap of films for metal-to-metal space High density plasma fluorinated silicate glass (HDP FSG) is used due to various advantages. However, FSG films can have critical drawbacks such as bonding issue of top metal at package, metal contamination, metal peel-off, and so on. These problems are generally caused by fluorine penetration out of FSG film. Hence, FSG capping layers such like SRO(Silicon Rich Oxide) are required to prevent flourine penetration. In this study, their characteristics and a capability to block fluorine penetration for various FSG capping layers are investigated through FTIR analysis. FTIR graphs of both SRO using ARC chamber and SiN show that clear Si-H bonds at $2175{\sim}2300cm^{-1}$. Thus, Si-H bond at $2175{\sim}2300cm^{-1}$ of FSG capping layers lays a key role to block fluorine penetration as well as dangling bond.

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Manufacture and Characterization of Microfibrillated Cellulose (MFC)/Propolis-Incorporated PLA Films (마이크로피브릴화 셀룰로오스(MFC)/프로폴리스 첨가 PLA 필름 제조 및 특성 분석)

  • Yeon Ju Lee;Hye Jee Kang;Min Su Kim;Young Hoon Jung
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.29 no.2
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    • pp.103-110
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    • 2023
  • The study aimed to enhance the properties of polylactic acid (PLA), a biodegradable and biocompatible substitute for fossil-based plastics. Since the applicability of PLA has been limited because of its toughness and brittleness, microfibrillated cellulose (MFC) and propolis were introduced into PLA. As a result, the PLA film with MFC/propolis showed significant improvements in mechanical strength, elongation, and storage modulus, while also experiencing a decrease in the glass transition temperature. Additionally, the presence of polyphenols in propolis led to a reduction in light transmittance in the UV wavelength range. These enhancements are attributed to MFC tightly bonding with PLA polymers, and propolis acting as a plasticizer and mediator between MFC and PLA, preventing agglomeration. These reinforced PLA films have the potential to be used in flexible packaging for light-sensitive products.

Thermal Distribution Analysis in Nano Cell OLED (나노 셀 OLED의 열 분포 해석)

  • Kyung-Uk Jang
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.37 no.3
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    • pp.309-313
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    • 2024
  • The key to determining the lifetime of OLED device is how much brightness can be maintained. It can be said that there are internal and external causes for the degradation of OLED devices. The most important cause of internal degradation is bonding and degradation in the excited state due to the electrochemical instability of organic materials. The structure of OLED modeled in this paper consists of a cathode layer, electron injection layer (EIL), electron transport layer (ETL), light emission layer, hole transport layer (HTL), hole injection layer (HIL), and anode layer on a glass substrate from top to bottom. It was confirmed that the temperature generated in OLED was distributed around the maximum of 343.15 K centered on the emission layer. It can be seen that the heat distribution generated in the presented OLED structure has an asymmetrically high temperature distribution toward the cathode, which is believed to be because the sizes of the cathode and positive electrode are asymmetric. Therefore, when designing OLED, it is believed that designing the structures of the cathode and anode electrodes as symmetrically as possible can ensure uniform heat distribution, maintain uniform luminance of OLED, and extend the lifetime. The thermal distribution of OLED was analyzed using the finite element method according to Comsol 5.2.