• Journal of Periodontal and Implant Science
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• 제24권2호
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• pp.433-440
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• 1994

The purpose of this investigation was to study the efficacy and safety of 6% hydrogen peroxide gel as a daily home tooth bleaching gel. The subjects consisted of 20 male dental students representing a variety of acquired stain and each subject participated for a 4-week period. Tooth color analysis(Shade determination), sulcus bleeding index, probing depth and probing attachment level were done and recorded at baseline and at the end of each week of study. The results indicated that home bleaching gel containing 6% hydrogen peroxide was effective and caused no gingival inflammation. Sulcus bleeding index, probing depth and probing attachment level showed no change. In conclusion, 6% hydrogen peroxide gel is an effective and safe agent for daily home tooth bleaching.

• Restorative Dentistry and Endodontics
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• 제23권1호
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• pp.183-196
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• 1998

The purpose of this study was to determine the effect of bleaching technique on the shear bond strength of esthetic restorative materials to bovine enamel. The bleaching agent was used 35% $H_2O_2$(Hi-Lite, Shofu, U.S.A.). Experimental groups were divided into two divisions as group A and B. Experimental A groups for the effect of number of bleaching were as follows ; Group Al : no bleaching Group A2 : bleaching 1 time ( for 5 minutes ) Group A3 : bleaching 3 times ( each for 5 minutes ) Group A4 : bleaching 6 times ( each for 5 minutes ) Group A5 : bleaching 9 times ( each for 5 minutes ) Experimental B groups for the effect of storage period in artificial saliva were as follows ; Group B1 : not stored in artificial saliva after bleaching Group B2 : stored in artificial saliva for 1 day after bleaching Group B3 : stored in artificial saliva for 1 week after bleaching Group B4 : stored in artificial saliva for 2 weeks after bleaching Group B5 : stored in artificial saliva for 4 weeks after bleaching Composite resin and glass ionomer cement were bonded to all specimens, and the shear bond strength between enamel and r~storative material were measured in Instron Universal Testing Machine(Instron, 4467, U.S.A,), Additionally, the bleached enamel specimens were examed after etching with 37.4% $H_3PO_4$ for 1 min under SEM(S-2300, Hitachi Co., Japan) to observe the effect of bleaching procedure on enamel surface morphology. The result were as follows ; 1. In SEM findings, bleached bovine enamel was found to be superficially rough. 2. In bleached bovine enamel, the effect of acid etching was reduced with the increase of number of bleaching. 3. The mean shear bond strength of composite resin and glass ionomer cement to bleached enamel surface tended to be lower than those to non-bleached enamel surface. 4. With the increase of number of bleaching, the shear bond strength of composite resin and glass ionomer cement to bleached enamel were progressively decreased. 5. Increasing the, storage period in artificial saliva after bleaching, the shear bond strength of composite resin and glass ionomer cement to bleached enamel were progressively increased. 6. The mean shear bond strength of glass ionomer cement to bleached bovine enamel tended to be clearly lower than that of composite resin.

• Restorative Dentistry and Endodontics
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• 제28권1호
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• pp.57-63
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• 2003

The purpose of the present study were to evaluate microleakage of a fourth generation dentin-bonding agent following a walking bleaching treatment, to determine the effect of temporary postbleaching dressing with calcium hydroxide on microleakage and to investigate the effect of delayed intracoronal restoration on microleakage. The results of this study were as follows : 1. Bleached groups showed more microleakage than unbleached group 2. Immediately restored group following bleaching procedure showed the highest microleakage score. 3. One-week delayed restorations showed less microleakage but there were no statistically significant difference between group II and III. 4. Provisional dressing with calcium hydroxide had no influence on microleakage. It is necessary to know the time that has elapsed from the bleaching treatment to the restoration procedure to achieve optimal seal, as well as to reduce the risk of microleakage in adhesive restoration.

• 대한가정학회지
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• 제37권2호
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• pp.113-126
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• 1999

In order to investigate the detergency effect of stained cotton and PET fabric, respectively, these fabrics stained with solid soils such as carbon black, liquid paraffin, and fat and examined the detergency effect in the optimum washing condition. The evaluation of washing efficiency of washed fabrics studied by using the surface reflectance measurement before and after washing treatment. The maximum detergency effect of stained cotton and PET fabric obtained in the mixed washing liquor-bleachig agen(ml)/concentrated washig agent(g/l). To obtain the excellent detergency effect, 2-step washing treatment, pre-washing by bleaching agent only and washing by concentrated detergent, is preferred. In comparing the detergency of polyester and cotton fabric, the detergency of stained polyester fabric superior than that of stained cotton fabric because of the difference of adhesive force between soil material and fabric in preparing soled stained fabric. In this study, we also studied the degree of fabric damage by the measurement of tensile strength change. From the results of the tensile strength measurement, the damage of washed fabric before and after washing treatment was nearly changed.

• 한국염색가공학회지
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• 제11권3호
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• pp.23-31
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• 1999

In order to investigate the detergency of the mixture of compact detergent and bleaching agent to fabric stained with a coffee and a red wine, respectively, and a japanese wet stained fabrics, to evaluation of detergency was studied under various washing conditions. In order to study the effect of alkaline agent addition on the detergency, the soda ash was added in the compact detergent system. The results are as follows : In a low temperature washing condition, the alkalinity of washing liquor effected more the removal of the composite stained fabrics than that of oilic stained fabrics. For the colored stained fabric such as red wine stained sample, the influence of the repeated washing treatment on the detergency was not significant factor. On the other hand, the influence of the repeated washing treatment for the coffee stained and japanese wet stained fabric on the detergency was gradually increased.

• Restorative Dentistry and Endodontics
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• 제38권4호
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• pp.241-247
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• 2013

Objectives: The aim of this study was to determine the effect of epigallocatechin gallate (EGCG) on the shear bond strength of composite resin to bleached enamel. Materials and Methods: Ninety enamel surfaces of maxillary incisors were randomly divided into 9 groups as follows: G1: control (no bleaching); G2: bleaching; G3: bleaching and storage for seven days; G4 - 6: bleaching and application of 600, 800 and 1,000 ${\mu}mol$ of EGCG-containing solution for 10 minutes, respectively; G7 - 9: bleaching and application of 600, 800 and 1,000 ${\mu}mol$ of EGCG-containing solution for 20 minutes, respectively. The specimens were bleached with 30% hydrogen peroxide gel and a composite resin cylinder was bonded on each specimen using a bonding agent. Shear bond strength of the samples were measured in MPa. Data was analyzed using the two-way ANOVA and Tukey HSD tests (${\alpha}$ = 0.05). Results: The maximum and minimum mean shear bond strength values were observed in G1 and G2, respectively. Time and concentration of EGCG showed no significant effects on bond strength of the groups (p > 0.05). Multiple comparison of groups did not reveal any significant differences between the groups except for G2 and all the other groups (p < 0.05). Conclusions: There is a significant decrease in bond strength of composite resin to enamel immediately after bleaching. A delay of one week before bonding and the use of EGCG increased bond strength of composite resin to bleached enamel.

• 디지털융복합연구
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• 제17권1호
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• pp.357-364
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• 2019

본 연구는 모발 탈색 시 사용되어지는 탈색제 입자에 따른 모발 손상도를 비교하였으며, 주사전자현미경을 사용하여 세 가지의 탈색제 입자크기를 관찰하였다. 탈색제의 주성분은 과황산암모늄과 과황산칼륨이 주성분인 분말형 탈색제로 각 제품 입자크기는 $131{\mu}m$, $72{\mu}m$, $48.8{\mu}m$로 나타났다. 손상도 실험에서 입자가 큰 탈색제보다는 입자가 작은 시술 제품에서 큐티클 층이 일어나거나 박리현상이 거의 일어나지 않았다. 모발의 색상 측정에서 입자 큰 탈색제의 모발시료는 가장 어둡게 나왔으며, 가장 작은 입자의 탈색 결과가 가장 밝게 나왔다. 연구 결과 모발의 손상도 완화에 더 효과적인 탈색제는 작은 입자를 가진 탈색제를 이용하여 시술하고, 탈색 정도에 따라 입자를 선택하는 것이 탈색력은 높이고 손상도를 낮출 수 있다고 사료된다. 이는 탈색제 선택에 대해서 우수한 결과를 만들기 위한 방안이며, 그 결과를 토대로 현장에서 탈색 시술시 모발 손상에 대처할 수 있을 것으로 기대 된다.

• 대한치과교정학회지
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• 제40권5호
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• pp.342-348
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• 2010

본 연구는 미백, 탈감작제 도포 후, 셀프 에칭 프라이머를 이용하여 브라켓 접착 시 법랑질에 대한 전단결합강도를 비교하기 위해 시행되었다. 48개의 소구치를 무작위로 12개씩 4개의 그룹으로 분류하였다. Group 1: 15% hydrogen-peroxide office bleaching agent (Illumine Office-IO), Group 2: IO + BisBlock Oxalate Dentin-Desensitizer, Group 3: Bis-Block Oxalate Dentin-Desensitizer, Group 4: 아무것도 하지 않음(대조군). 브라켓 접착 24시간 후 전단결합강도를 측정하였으며, 만능시험기의 속도를 5 mm/min로 하여 브라켓이 탈락할 때까지 시행하였다. Modified adhesive remnant index를 이용하여 탈락 양상을 분석하였다. 미백만 시행, 미백과 탈감작제 도포, 탈감작제만 도포한 경우 모두 브라켓의 전단결합강도를 현저히 감소시켰으며 ($p$ = 0.001), 이 세 실험군 간에는 통계적으로 유의성 있는 차이를 관찰할 수 없었다 (Group 1-Group 2, $p$ = 0.564; Group 1-Group 3, $p$ = 0.371; Group 2-Group 3, $p$ = 0.133). 세 실험군에서 브라켓의 탈락은 주로 법랑질-접착제 계면에서 발생하여 브라켓 베이스에 접착제의 100%가 남아있었다. 따라서 미백과 탈감작제 도포는 교정치료 후에 시행하는 것이 바람직하다.

• 한국콘텐츠학회논문지
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• 제12권1호
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• pp.353-360
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• 2012

본 연구에서는 현재 자가 미백용으로 많이 사용하고 있는 15% carbamide peroxide(CP)에 potassium nitrate와 fluoride(PF)가 함유된 제품과 미 함유된 제품을 사용하여 색과 표면미세경도를 측정하였다. 건전한 소구치 30개를 이용하여 30개의 시편을 제작하였고, 각 각 10개씩 3군으로 분류하였다. 1군은 대조군 (Distilled water), 2군은 15% CP, 3군은 15% CP(3% potassium nitrate and 0.11% fluoride 함유)이다. 치아미백은 14일 동안 하루에 6시간 미백하고 이후 시간은 증류수에 보관하였다. 색 측정은 미백 전과 14일에 측정하였고, 표면미세경도는 미백 전, 7일, 14일에 측정하여 다음과 같은 결과를 얻었다. 색변화를 본 결과 미백하지 않는 대조군 1군과 미백제가 함유된 2군과 3군에는 통계적으로 유의한 차이가 보였고(p<0.05), 2군과 3군 사이에는 통계적으로 유의한 차이를 나타내지 않았다(p>0.05). 표면미세경도 변화를 비교해보면 시간이 경과함에 따라 대조군을 제외하고 2군과 3군에서는 미백 전 경도 값에 비해서 미백 후 유의하게 경도의 감소를 보였고(p<0.05), 특히 미백 7일째 경도 값의 차이가 미백 후 14일보다 컸다. 미세경도 감소율을 보면 대조군인 1군은 7일과 14일에 각 각 1.7과 0.8로 차이가 거의 없으나 2군은 21.9,와 3.5이고, 3군은 16.7과 1.4로 미백 7일째에서 유의하게 감소했고(p<0.05), PF가 미 함유된 2군의 7일째 미세경도 감소율이 가장 컸다. 이상의 결과를 종합해 보면, PF는 치아미백에 부정적 영향을 주지 않으며, 미세경도 변화에서는 PF가 함유된 미백제에서 경도 감소율이 적었다. 따라서 PF가 함유된 치아미백제는 미백효과와 함께 치아법랑질의 경도 감소를 줄일 수 있다.

• 대한치과보철학회지
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• 제40권5호
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• pp.451-469
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• 2002

The purpose of this study was to estimate the effect of a bleaching agent on tooth surfaces and to evaluate the resin bond strength according to different surface treatments on bleached teeth. To prepare for the experimental samples, first, extracted human third molars were used and the body portions of the crowns were cut into four equal-sized specimens. Next, each specimen was mounted in an plastic bottle with self-cured resin and highly polished to have them reveal the enamel or dentin surfaces. Then, the enamel(E) and dentin(D) specimens were divided into four ; 1) non-bleached, laser-treated(NBLA) group 2) bleached, laser-treated(BLLA) group 3) non-bleached, acid-treated(NBAC) group and 4) bleached, acid-treated(BLAC) group. Here, $opalescence^{(R)}$ (10% carbamide peroxide) was used for bleaching agent. The treated specimens were observed by confocal laser scanning microscopy and bonded with composite resin for shear bond test. The following results were obtained from this experiment : 1. Compared with the ENB group, the EBL group was shown be dyed about $20{\mu}m$ deeper with rhodamine B. The DBL group appeared to be caved in at the entry part of the dentinal tubules, was dyed about $20{\mu}m$ deeper and $5{\mu}m$ wider in diameter, compared with the DNB group. 2. In comparison with the EBLAC group, the ENBAC group looked evenly bonded with the resin, while the DNBAC group, compared to DBLAC group, was observed to have its resin tags penetrated about $50{\mu}m$ deeper. Other than those, however, no observable differences between ENBLA and EBLLA group or between DNBLA and DBLLA group were found. 3, At the shear bond test, the ENBAC group was shown to have statistically significant higher shear bond strength than the EBLAC group(p<0.05). No statistically significant differences between the ENBLA and the EBLLA groups were observed(p>0.05). 4. At the shear bond test, the DNBAC group was shown to have statistically significant higher shear bond strength than the DBLAC group(p<0.05). No statistically significant differences between the DNBLA and the DBLLA groups were observed(p>0.05). The in vitro observations above suggest that tooth-bleaching procedure brings a certain change on enamel and dentin surfaces and it weakens the shear bond strength with composite resin when the bleached tooth was acid-treated.