• Textile Coloration and Finishing
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• v.21 no.5
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• pp.27-34
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• 2009

PET fabric was dyed in black shade with disperse dyes of three primary color. The effect of combination ratio of dye concentration and energy type of disperse dye on dyeing and color property of black dyed PET fabric was investigated. Dyeing compatibility of disperse dyes of three primary color on PET was evaluated by comparison of dyeing rates of them. From the results, color property was dependent upon the combination ratio of dye concentration. In order to obtain low lightness ($L^*$) and black color, blue dye should be added enough. S-type disperse dye and $130^{\circ}C$ dyeing was suitable rather than SE-type dyes or $120^{\circ}C$ dyeing. Disperse dyes of three primary color used showed good dyeing compatibility at high dye concentration. Washfastness was fair to moderate and lightfastness was moderate.

• Textile Coloration and Finishing
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• v.29 no.4
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• pp.276-283
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• 2017

The aim of this study is to develop an effective dyeing process for black color on the silk fabrics, using natural Indigo, Madder, Amur cork tree, Alder, Logwood, and Gallnut. All natural dye materials were water-extracted, concentrated, and freeze-dried. Seven different processes were carried out and the color differences(${\Delta}E$) of black color with each process from the chemical black dyed fabric were compared. The light, washing, and rubbing fastness were evaluated. The black dyeing of the silk fabrics was well carried and excellent black color was obtained in every methods. The profound black color could be obtained by the subtractive mixture of the three primary colors of red, yellow, and blue in the order of indigo(blue) - amur cork tree(yellow) - madder or lac(red). Black color was efficiently obtained by iron mordant when logwood or alder fruit was used. The color difference(${\Delta}E$) from the black color with chemical dyestuff was the lowest in the indigo - amur cork tree - lac - iron method. Light fastness and washing fastness were excellent in all dyeing processes, showing grade 5. The fastness to rubbing was excellent as shown grade 5 in the dry samples of logwood - iron process and alder fruit - iron process.

• Journal of the Korean Society of Clothing and Textiles
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• v.22 no.5
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• pp.557-564
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• 1998

Dyeing properties of silk fabric with black tea colorants were investigated in terms of dye uptakes at various dyeing conditions and the effect of mordants on color change and colorfastness. Black tea colorants showed high affinity to silk and produced brown color. Two types of adsorption isotherm were obtained; Langmuir and Freundlich equilibrium at 360 nm and 460 nm, respectively. Thus, it is considered that both of ionic and hydrogen bondings are involved in silk dyeing with black tea colorants. Dye uptake increased continuously as concentration of colorants increased. Brown color was not changed with mordant type except that Fe mordant produced dark brown color. Mordanting did not influence colorfastness of dyed silk significantly. Therefore, mordanting was not necessary in dyeing silk with black tea colorants.

• Journal of Fashion Business
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• v.21 no.1
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• pp.166-176
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• 2017

This study is fundamental research on how to be able to scientifically quantify and reproduce a natural dyeing procedure. By dyeing silk fabrics, the establishment of a reproducible dyeing method was sought. Juglans mandshurica has been known as one of the most widely used black vegetable dyes. Repetition conditions and combination dyeing were performed with Juglans mandshurica cortex, gallnut, clove, and Eclipta prostrata L. extracts to express a deep black color. Juglans mandshurica cortex, gallnut, clove, and Eclipta prostrata L. extracts were suitable for black coloration and showed a darker black color when combined with iron mordant. Specifically, Juglans mandshurica cortex and clove can be used for deep black coloring. Color fastness when washed or dry cleaned was found to be strong with a grade of 4-5 and fastness to light was rated at a 3-4. The grade of color change when exposed to rubbing and perspiration was good at a 4-5. In regards to functional property aspects, it showed excellent results with a 99% deodorization rate at 120 minutes of dyeing time, 97.1% UV protection rate, and 85.9% and 62.3% bacterial reduction against Staphylococcus aureus and Streptococcus pneumoniae, respectively. Therefore, it is considered that the extract from the Juglans mandshurica cortex is of great value as an eco-friendly, natural dyestuff.

• Proceedings of the Korean Society of Dyers and Finishers Conference
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• 2008.10a
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• pp.13-14
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• 2008

In black dyeing of PET fabric, high concentrations of disperse dyes of three primary color are generally used, which leads low exhaustion level of dye and discharge of a large amount of unfixed dye into dyehouse effluent. In this study, the effect of combination ratio of dye concentration, liquor ratio, and dyeing pH on dyeing and color property of black dyed PET fabric was investigated.

• Current Research on Agriculture and Life Sciences
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• v.27
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• pp.13-19
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• 2009

The purpose of this study was the efficient use of the black rice bran for dyeing textiles. For this purpose, we investigated proper extracting conditions of black rice bran, dyeability and dyeing fastness of dyed silk fabrics. To find proper extracting condition of black rice bran, we extracted black rice bran with water at different temperatures($40^{\circ}C$, $60^{\circ}C$, $80^{\circ}C$), different extracting pH(pH3, pH4, pH5, pH6) and extracting time(20, 40, 60, 80, 100, 120, 140, 160, 180min.). Also we investigated the effect of dyeing time(1, 2, 3, 4, 5, 6hr.), dyeing temperature($40^{\circ}C$, $60^{\circ}C$, $80^{\circ}C$) and mordanting method(non, pre, sim, post) to examine dyeability and dyeing fastness of dyed silk fabrics. As a result, when the extracting temperature and time were $80^{\circ}C$, 3hr., respectively, extracting was best. And the higher the extracting concentration, the more the extracting amount. As the dyeing temperature and time were higher and longer, the dyeability of silk fabrics was better. With mordant, the dyeability was improved and when using premordant method better, the K/S value was maximized. The laundering fastness of the silk fabrics dyed with black rice bran was estimated to have a good grade of 3~4, however, the light fastness was poor to have a grade of 1~2.

• Fashion & Textile Research Journal
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• v.9 no.1
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• pp.103-112
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• 2007

The purpose of this study was to investgate dyeing, moradnting properties and colorfastness activities of silk, polyamide, acetate treated black soybean extracts. The color of extract by buffer solution (pH=1) red, but the higher pH of extracted black soybean solution the paler of color strength. Black soybean extracts was approved anthocyanin of 3type(Delphinidin3-glucoside, Cyanidin 3-glucoside, Petunidin 3-glucoside) by chemiclal analysis. This anthocynin, in acid condition, is oxinium structure (red color, soluable) but, in alkali condition quinoid structure(dark brown, in soluable). The optimum dyeing condition of black soybean anthocynin was 10min at $30^{\circ}C$, pH -1. Colorfastness to washing and light showed generally low but crocking fastness was excellent.

• Textile Coloration and Finishing
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• v.17 no.5 s.84
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• pp.20-25
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• 2005

The colorants were extracted from black soybean using a buffer solution. Dyeing properties and the fastness of silk fabric dyed with black soybean extracts were investigated. K/S values of dyed fabric were increased with concentration of black soybean extracts. Magnesium sulfate, nickel sulfate and calcium chloride as mordants are used to obtain reddish purple color. Optimum dyeing temperature of black soybean extracts was $30^{\circ}C$. Fastness were generally good except for light fastness which was extremely poor.

• Journal of the Korean Society of Clothing and Textiles
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• v.24 no.1
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• pp.34-42
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• 2000

The colorante from black tea infusion were applied to cotton fabric. Dyeing properties were investigated in terms of dye uptakes at various dyeing conditions and the effect of mordants on color change and colorfastness. Cotton showed low affinity to black tea colorants. Effects of mordants on dye uptake was not significant except Sn. Irrespective of mordant type, color of cotton dyed with black tea colorants was brownish and colorfastness was generally good. In order to improve dye uptake, cotton was cationized by treating with Cationon UK(tertiary ammonium salt) and chitosan. Dye uptake of cotton was remarkably increased by cationizing. Cationon UK was more effective than chitosan.

• Journal of the Korean Wood Science and Technology
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• v.37 no.4
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• pp.406-413
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• 2009

This study was carried out to investigate the natural dyeing characteristics of Korean traditional hand-made paper (Hanji). The Hanji was dyed black with extractive of gallnut (Rbusjavanica L), leaves of Amur maple (Acer ginnala), nutshell of chestnut (Castania crenata), and persimmon juice and Chinese ink. And moreover, the Hanji was dyed not only using single and combination of dyestuff but also changing mordants and mordanting procedure. And we estimated the relationship between dyeing characteristics and dyestuff concentration (o.w.f.). The gallnut was the most principal material dyeing black. The procedure of mordanting from copper acetate to Iron (II) chloride and dyeing from gallnut to Amur maple dyestuffs were the best dyeing method for the Hanji to black. The K/S value of dyed Hanji increased with increasing concentration of dyestuff.