• Restorative Dentistry and Endodontics
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• v.39 no.4
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• pp.270-275
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• 2014

Objectives: This study compared the mechanical properties of various instruments for canal exploration and glide-path preparations. Materials and Methods: The buckling resistance, bending stiffness, ultimate torsional strength, and fracture angle under torsional load were compared for C+ file (CP, Dentsply Maillefer), M access K-file (MA, Dentsply Maillefer), Mani K-file (MN, Mani), and NiTiFlex K-file (NT, Dentsply Maillefer). The files of ISO size #15 and a shaft length of 25 mm were selected. For measuring buckling resistance (n = 10), the files were loaded in the axial direction of the shaft, and the maximum load was measured during the files' deflection. The files (n = 10) were fixed at 3 mm from the tip and then bent $45^{\circ}$ with respect to their long axis, while the bending force was recorded by a load cell. For measuring the torsional properties, the files (n = 10) were also fixed at 3 mm, and clockwise rotations (2 rpm) were applied to the files in a straight state. The torsional load and the distortion angle were recorded until the files succumbed to the torque. Results: The CP was shown to require the highest load to buckle and bend the files, and the NT showed the least. While MA and MN showed similar buckling resistances, MN showed higher bending stiffness than MA. The NT had the lowest bending stiffness and ultimate torsional strength (p < 0.05). Conclusions: The tested instruments showed different mechanical properties depending on the evaluated parameters. CP and NT files were revealed to be the stiffest and the most flexible instruments, respectively.

• Journal of Dental Anesthesia and Pain Medicine
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• v.21 no.2
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• pp.139-153
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• 2021

Background: In anesthetic techniques, touching bones can cause needle bending. Theoretically, a needle should support such deflection without fracturing. However, it is possible that a needle may fracture depending on the quality and type of needle used. This study evaluated the physical, chemical, and micromorphological characteristics of long and short dental anesthetic needles, as well as the mechanical properties of flexural load and bending resistance when needles are subjected to different bending angles. Methods: Long and short needles (30G, Jets, Misawa, Selekto, Terumo, Unoject and 27G, Dencojet, Injex, Jets, Misawa, Procare, Setoject XL, Terumo) were evaluated. Scanning electron microscopy was used to evaluate the needle bevels and energy-dispersive X-ray spectroscopy was used for the chemical analysis of needle compositions. Flexural loading and bending strength assessments were performed using a universal testing machine by bending the needles (n = 5) to angles of 30°, 60°, or 90°, or until fracture occurred. Results: The Injex 27G, Jets 27G, and Septoject XL 27G needles were all less than 30 mm in length. There were small percentage variations in the chemical compositions of the needles. Superior smoothness was observed for the Unoject 30G needle, which exhibited the highest fracture resistance at 60°. The Jets 30G needle exhibited greater resistance to fractures at 90°. The Procare 27G needle exhibited the highest load resistance to bending, followed by the Septoject XL 27G needle, and both needles were tied for the lowest fracture resistance. No needle fractured when bent to 30° or at less than three bends to 60° or 90°. Conclusions: Greater needle resistance to bending increases the probability of early fracturing. Thinner and shorter needles are more resistant than longer and thicker needles. Performing a single bend does not result in any significant risk of fracture or obliterate the lumen, allowing for the continued passage of anesthetic liquid.

• Journal of Advanced Marine Engineering and Technology
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• v.23 no.4
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• pp.488-503
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• 1999

The present paper considers the constraint effect on J-R curves under the two-parameter $J-A_2$ controlled crack growth within a certain amount of crack extension. Since the parameter $A_2$ in $J-A_2$ three-term solution is independent of applied loading under fully plasticity or large-scale defor-mation $A_2$ is a proper constraint parameter uring crack extension. Both J and $A_2$ are used to char-acterize the resistance curves of ductile crack growth using J as the loading level and $A_2$ are used to char-acterize the resistance curves of ductile crack growth using J as the loading level and A2 as a con-straint parameter. Approach of the constraint-corrected J-R curve is proposed and a procedure of transferring the J-R curves determined from standard ASTM procedure to non-standard speci-mens or real cracked structures is outlined. The test data(e.g. initiation toughness JIC and tearing modulus $T_R$) of Joyce and Link(Engineer-ing Fracture Mechanics 1997, 57(4) : 431-446) for single-edge notched bend[SENB] specimen with from shallow to deep cracks is employed to demonstrate the efficiency of the present approach. The variation of $J_{IC}$ and $T_R$ with the constraint parameter $A_2$ is obtained and a con-straint-corrected J-R curves is constructed for the test material of HY80 steel. Comparisons show that the predicted J-R curves can very well match with the experimental data for both deep and shallow cracked specimens over a reasonably large amount of crack extension. Finally the present constraint-corrected J-R curve is used to predict the crack growth resistance curves for different fracture specimens. over a reasonably large amount of crack extension. Finally the present constraint-corrected J-R curve is used to predict the crack growth resistance curves for different fracture specimens. The constraint effects of specimen types and specimen sizes on the J-R curves can be easily obtained from the constrain-corrected J-R curves.

• The Journal of the Korean dental association
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• v.57 no.11
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• pp.672-678
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• 2019

AIM: The purpose of this study was to evaluate and compare the torsional fracture resistances, cyclic fatigue resistance, and bending stiffness of two nickel-titanium (NiTi) rotary instruments made of different heat-treated alloy: Aurum Blue (heat-treated) and Aurum Pro (conventional). Methods: Forty-five Aurum Blue and Aurum Pro NiTi files were selected for the three mechanical tests (n=15). For the torsional resistance test, 3 mm file tip was fixed and the shaft was driven clockwise at 2 rpm until fracture occurred by using a customized device. Cyclic fatigue resistance was evaluated by rotating instruments in artificial canal with dynamic mode. Bending stiffness was tested by observation of the bending moment on attaining a 45° bend. The results were analyzed by student-t tests at a significance level of 95%. The fractured surface of each groups were examined under a scanning electron microscope (SEM). Results: Aurum Blue showed significantly higher toughness, ultimate strength, distortion angle, and number of cycles to failure than those of Aurum Pro (p < 0.05). However, Aurum Blue and Aurum Pro did not differ significantly in terms of bending stiffness. SEM showed typical topographic appearances of the cyclic fatigue and torsional fracture. Conclusions: Under the limitations of this study, heat-treated instruments showed higher flexibility and fracture resistances than conventional NiTi instruments.

• The Transactions of the Korean Institute of Electrical Engineers C
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• v.48 no.6
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• pp.436-441
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• 1999

Joule heating effect in EM(Electromigration) test were performed on a bend test structure. EM test is done under high current densities(1.0-2.5MA/cm2), which leads to joule heating. Since joule heating is added to the controlled oven(stress) temperature, themetal line temperature is higher than the stress temperature. The increase in the stress temperature due to joule heating is important because EM phenomena and metal line failure are related to the stress temperature. In this paper, metal line was stressed with a current density of 1.0 MA/$cm^2$, 1.5MA/$cm^2$, 2.0MA/$cm^2$, 2.5MA/$cm^2$, for 1200 sec and temperature increase due to joule heating was less than $10^{\circ}C$. Also it took 30 minutes for the metal line to equalized with oven temperature. Recommendations are given for the EM test to determine the initial resistance of EM test structure under stress temperature and current density.

• Proceedings of the Korean Nuclear Society Conference
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• 1998.05b
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• pp.336-343
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• 1998

An iteration method has been developed for determining crack growth and fracture resistance cure (J-R curve) from the load versus load-line displacement record only. In this method, the hardening curve, the load versus displacement curve at a given crack length, is assumed to be a power-law function, where the exponent varies with the crack length. The exponent is determined by an iterative calculation method with the assumption that the exponent varies linearly with the load-line displacement. The proposed method was applied to the static J-R tests using compact tension(CT) specimens, a three-point bend (TPB) specimen, and a cracked round bar (CRB) specimen as well as it was applied to the quasi-dynamic J-R tests using CT specimens. The J-R curves determined by the proposed method were compared with those obtained by the conventional testing methodologies. The results showed that the J-R curves could be determined directly by the proposed iteration method with sufficient accuracy in the specimens from SA508, SA533, and SA516 pressure vessel steels and SA312 Type 347 stainless steel.

• Corrosion Science and Technology
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• v.22 no.6
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• pp.447-456
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• 2023

In this work, we performed a comparative study examining two coatings on Ti Gr.1 for use in fuel cell bipolar plates. The coatings consisted of carbon black as the conductor along with acrylic polymer and Ti Sol-Gel binder as the binder. Ti Sol-Gel that had precipitated as TiO₂ in areas impregnated between carbon black gaps, thereby acting as a binder for carbon black and serving as a polymer coating. Neither of the coatings peeled off during the 90° bend test to check formability. The contact resistance of the TiO₂ coating was found to be lower than that of the polymer binder coating. Moreover, due to coating shrinkage (denser) that occurred during the heat treatment process, the TiO₂ binder coating showed almost the same level of corrosion resistance, as measured by potentiostatic and EIS tests, despite being thinner than the polymer coating. However, both the polymer binder coating and the TiO₂ binder coating had many pores and irregularities internally (around 10 ~ 100 nm) and on the surface (0.1 ~ 2 ㎛). We considered that these pores and irregularities contributed to the lower corrosion resistance.

• Journal of Environmental Science International
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• v.12 no.4
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• pp.481-485
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• 2003

Two types of polyimide/silica composite films were prepared using sol-gel method through hydrolysis and polycondensation of tetraethoxysilane (TEOS) with the polyamic acid (PAA) and end-capped PAA solution. Samples were characterized by the means of differential thermogravimetry, X-ray diffractometry, scanning electron microscopy, universal test, impedance analyzer, chemical resistance test, etc. All of the PAA/silanol solutions heat-treated at 300$^{\circ}C$ for 6h were transformed to polyimide/silica composites. It has been demonstrated that the properties of polyimide/silica composites were affected by the amount of silica addition and the bend type existed between polyimide and silica.

• The Transactions of The Korean Institute of Electrical Engineers
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• v.60 no.9
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• pp.1727-1732
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• 2011

In order to realize a high performance(low loss, high isolation) microwave power divider/combiner, we have designed the power combiner/divider precisely in accordance with the different hight of central part. In the case of the high central part of the hight of $h_r$=10.2, a compensating part of the conical line is inserted in the conical conversion transmission line, and in the case of low central part of the hight of $h_r$=5.0, the conical conversion transmission line is remodeled into the 2-stage bend structure. In both case, the reflection characteristics are improved to 30dB over the operating frequency range of 5GHz bandwidth. A resistance is inserted between the peripheral ports so as to try to improve the isolation characteristics of the device. For the 16-divider/combiner, the isolation characteristics are improved to 10dB over the operating frequency range of 5GHz bandwidth.

• Computers and Concrete
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• v.17 no.4
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• pp.541-551
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• 2016

Asphalt pavements are exposed to complex weather conditions and vehicle traffic loads leading to crack initiation and crack propagation in asphalt pavements. This paper presents the impact of weather conditions on fracture toughness of an asphalt concrete, prevalently employed in Ardabil road networks, under tensile (mode I) and shear (mode II) loading. An improved semi-circular bend (SCB) specimen was employed to carry out the fracture experiments. These experiments were performed in two different weather conditions namely fixed and cyclic temperatures. The results showed that consideration of the impact of temperature cycling resulted in decreasing the fracture toughness of asphalt concrete significantly. Furthermore, the fracture toughness was highly affected by loading mode for the both fixed and cyclic temperature conditions studied in this paper. In addition, it was found that the MTS criterion correctly predicts the onset of fracture initiation although this prediction was slightly conservative.