• Title/Summary/Keyword: bead formation

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The Effect of Coagulant and Molecular Weight on the Wet Spinnability of Regenerated Silk Fibroin solution

  • Yoo, Young-Jin;Kim, Ung-Jin;Um, In-Chul
    • International Journal of Industrial Entomology and Biomaterials
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    • v.21 no.1
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    • pp.145-150
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    • 2010
  • The regenerated silk fibroin with various molecular weights (MW) was prepared by different dissolution condition and the effect of coagulant on the wet spinnability of the various MW silk fibroin solutions dissolved in formic acid was investigated by the observation of wet spun filament in coagulant and the measurement of maximum draw ratio. The observation on the wet spun filament in coagulation bath revealed that good fibers without bead were formed in a high MW and a very high MW silk fibroin samples. In contrast, beads were observed in the silk fibroin sample with medium MW. The maximum draw ratio of wet spun silk fibroin filament decreased with MW reduction. The decrease of maximum draw ratio in isopropanol, acetone, DMF and THF was remarkably higher than that in methanol and ethanol, indicating that the coagulant type strongly influenced the wet spinnability. The two simple evaluation methods used in this study showed complementary information for wet spinnability: (a) The observation of filament in coagulant was effective to check a continuous fiber formation and a bead formation, and (b) the maximum draw ratio measurement was useful to examine the post drawing ability related to molecular orientation.

Laser Weldability of Sheet steels for Tailored Blank Manufacturing(1) (테일러드 블랭크용 박판 강재의 레이저 용접성 (1))

  • 김기철
    • Journal of Welding and Joining
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    • v.16 no.1
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    • pp.77-87
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    • 1998
  • This paper deals with the effect of laser welding parameters on the weld formation. Thin steels for automotive application were prepared so as to be welded with high power carbon dioxide laser system. Major process parameters were position of focus and travel speed. The effect of shielding gas was also discussed by employing the high speed photometry. Test results showed that the optimal position of focus varied in accordance with the joint configuration; bead-on-plate, butt or lap welding. It was recommended that the position of focus for the lap welding be located at slightly inner part of the material to be welded. In this case, however, it was noticeable that the weld penetration ratio, d/t$_{0}$ dropped drastically at the critical region. Results also demonstrated that both the bead width and penetration reduced as the travel speed increased. The penetration ratio showed two distinct regions; stabilized zone at the lower range of the travel spped and sudden drop zone at the higher range of travel speed. Lower limit of the penetration for acceptable weld was proved to be about 90% of the parent metal thickness based on the physical properties of the weld. Mixed gas application for both the shielding of molten metal and laser induced plasma control was recommended as far as the penetration was concerned.d.

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A Preliminary Study on the Lamination Characteristics of Inconel 718 Superalloy on S45C Structural Steel using LENS Process (LENS 공정을 이용한 Inconel 718 초합금의 S45C 구조용강 위 적층 특성 고찰에 관한 기초 연구)

  • Kim, Hyun-Sik;Lee, Hyub;Ahn, Dong-Gyu
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.20 no.1
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    • pp.16-24
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    • 2021
  • A laser-engineered net shaping (LENS) process is a representative directed energy deposition process. Deposition characteristics of the LENS process are greatly dependent on the process parameters. The present paper preliminarily investigates deposition characteristics of Inconel 718 superalloy on S45C structural steel using a LENS process. The influence of process parameters, including the laser power and powder feed rate, on the characteristics of the bead formation and the dilution in the vicinity of the deposited region is examined through repeated experiments. A processing map and feasible deposition conditions are estimated from viewpoints of the aspect ratio, defect formation, and the dilution rate of the deposited bead. Finally, an appropriate deposition condition considering side angle, deposition ratio, and buy-to-fly (BTF) is predicted.

Direct Conversion of Raw Starch to Maltose in an Agitated Bead Enzyme Reactor using Fungal $\alpha$-Amylase (분쇄마찰 효소반응계에서 Fungal $\alpha$-Amylase를 이용한 생전분의 직접전환에 의한 Maltose 생산)

  • 이용현;박진서
    • Microbiology and Biotechnology Letters
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    • v.19 no.3
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    • pp.290-295
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    • 1991
  • Direct conversion of raw starch without liquefaction to maltose using maltose-forming fungal a-amylase (Fungamyl) was carried out in an agitated bead enzyme reactor (bioattritor). The reaction rate in bioattritor was comparable with conventional method which utilized liquefied soluble starch. Moreover the extent of maltose formation increased substantially compared with conventional method; from 150 g / I of raw starch, around 95 g/l of maltose was formed and 72% of maltose content in sugar mixture was achieved. Especially, pH influenced greatly not only on total sugar formation from raw starch in bioattritor but also on maltose content in sugar mixture. The optimal pH for maltose formation from raw starch was shifted into the weak alkaline pH, the optimal pH of 8.0~9.0 in bioattritor contrast to pH of 5.0~5.5 for liquefied starch. The maltose formation and content were also affected by the amounts of Fungamyl added and raw starch concentration. Consumption of maltose-forming Fungamyl can be substantially reduced by supplementary addition of starch liquefying a-amylase (Termamyl).

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A study on the seam tracking in CO_2$ fillet welding by using an arc sensor (CO_2$ 용접에서 전기적인 아크신호를 이용한 수평 필릿 용접선 추적에 관한 연구)

  • 선채규;김재웅;나석주;조형석;최칠룡
    • Journal of Welding and Joining
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    • v.8 no.3
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    • pp.70-78
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    • 1990
  • The harsh nature of welding environments makes welding a prime candidate for process automation. Among the variety of welding processes available, gas metal arc welding is one of the most frequently used methods, primarily because it is highly suited to a wide range of applications, and also to automation. Automatic seam tracking method is one of the most demanded techniques for automatic control of arc welding. In this study a seam tracking system has been developed by using the welding arc itself as a sensor. This paper described the principle and experimental result of the arc sensor system, as well as the development and application of the automatic CO_2$ welding for the horizontal fillet welding. A basic problem in horizontal fillet welding is the prevention of hanging bead formation such as undercut at the vertical plate and overlap at the horizontal plate. To produce the symmetric bead shape, the relationship of bead shape to welding parameters(welding velocity, weaving width, weaving speed, tip to workpiece distance) was also investigated.

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Influence of Heat Input and Weld Bead Composition on Welding Property in the Laser Welding between Sintered Segment and Mild Steel Shank (소결체와 저탄소강의 레이저용접 특성에 미치는 입열량 및 용접부 성분변화의 영향)

  • Jung Woo-Gwang;Cho Nam-Joon;Kim Sung-Wook;Lee Chang-Hee;Kim Sung-Dea;Lee Joo-Hyung;Park Hwa-Soo
    • Korean Journal of Materials Research
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    • v.14 no.6
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    • pp.425-431
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    • 2004
  • A laser welding was applied between sintered tip of Fe-Co-W and low carbon steel shank for the diamond saw blade. The welding characteristics and formation of defects were investigated carefully for the weld fusion zone in different welding condition. Dendrite arm spacing in weld bead decreased with decrease of heat input. Co and W increased and Fe decreased in the weld fusion zone with increase of the heat input. The corresponding change of composition was observed with the change of beam position. The maximum and total length of crack decreased with increase of the heat input. The crack in weld bead was propagated along the dendrite boundary and was caused mainly by the segregation of constituent during the solidification.

Development of Laser-Rotating An Hybrid Welding Process (레이저-회전 아크 하이브리드 용접공정의 개발)

  • Kim, Cheol-Hee;Chae, Hyun-Byung;Lee, Chang-Woo;Kim, Jeong-Han;Rhee, Se-Hun
    • Journal of Welding and Joining
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    • v.24 no.1
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    • pp.88-92
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    • 2006
  • Laser-rotating arc hybrid welding was introduced by combining $CO_2$ laser and rotating gas metal arc welding. While the arc rotation enhances the weld pool motion, it reduces the undercut formation which is one of most critical weld defects in the conventional laser-arc hybrid welding. This research investigated the bead characteristics according to the welding parameters such as frequency of rotation, welding voltage, shielding gas composition and interspacing distance between laser and we. The welding parameters were selected to reduce spatter generation and ensure sound weld beads fur bead welding and butt welding with various joint gaps. Gap bridging ability was improved, such that the sound weld beads were achieved for butt joint with up to 2mm joint sap, with no adjustment of CTWD(Contact tip-to-workpiece distance) and electrode diameter.

Preparation of Alginate-fibroin Beads with Diverse Structures (다양한 구조를 가진 알긴산-피브로인 비드 제조)

  • Lee, Jin-Sil;Lee, Shin-Young;Hur, Won
    • KSBB Journal
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    • v.26 no.5
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    • pp.422-426
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    • 2011
  • Alginate bead has been supplemented with various polymers to control permeability and to enhance mechanical strength. In this report, fibroin-reinforced alginate hydrogel was prepared, in which spatial localization of fibroin molecules was investigated. Confocal laser scanning microscopy revealed that fibroin molecules formed a fibrous network in the alginate-fibroin beads, which was expected to enhance mechanical strength as same as in many composite materials. Uniaxial compression test showed that fibroin-reinforced alginate beads had increased mechanical strength only after methanol treatment that caused ${\beta}$-sheet formation among fibroin molecules. Simultaneous curing and dialysis of alginate beads were carried out to remove excesscalcium but to retain fibroin in the dialysis chamber, which fabricated beads without internal fibrous fluorescent stains. Fibroin molecules were only found beneath the surface of the beads. The fibroin-diffused shell was further processed to form a thick wall after drying or was mobilizedto the centre of the bead by methanol treatment. Accordingly, the structure analyses provide processing methods of fibroin to form a wall or center clumps, which could be applied to design controlled delivery device.

Laser Welding Characteristics of Aluminum and Copper Sheets for Lithium-ion Batteries (자동차 이차전지 제조를 위한 알루미늄과 무산소동의 레이저 용접특성)

  • Kang, Minjung;Park, Taesoon;Kim, Cheolhee;Kim, Jeonghan
    • Journal of Welding and Joining
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    • v.31 no.6
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    • pp.58-64
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    • 2013
  • Several joining methods involving resistance welding, laser welding, ultrasonic welding and mechanical joining are currently applied in manufacturing lithium-ion batteries. Cu and Al alloys are used for tab and bus bar materials, and laser welding characteristics for these alloys were investigated with similar and dissimilar material combinations in this study. The base materials used were Al 1050 and oxygen-free Cu 1020P alloys, and a disk laser was used with a continuous wave mode. In bead-on-plate welding of both alloys, the joint strength was higher than the strength of O tempered base material. In overlap welding, the effect of welding parameters on the tensile shear strength and bead shape was evaluated. Tensile shear strength of overlap welded joint was affected by interfacial bead width and weld defect formation. The tensile-shear specimen was fractured at the heat affected zone by selecting proper laser welding parameters.