• Title/Summary/Keyword: annealing conditions

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The fabrication of RTD via Lift-off process (Lift-off법에 의한 RTD의 제조)

  • 김종성;원종각
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.11a
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    • pp.299-302
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    • 2000
  • RTD temperature sensor is a thermoresistor which uses the liner dependence of the resistance of the sensing material on the temperature, and has good stability and sensibility, so it can be used in highly precise temperature measurement. In this study RTD sensor was fabricated using Pt thin film. The Pt thin film was deposited on alumina using DC-Sputter, and annealed with various temperature. Through the experiments of XRD, AFM, 4-point probe, the surface structure of the thin film with annealing conditions and their effects on the electrical resistance were investigated. RTD with serpentine pattern was fabricated using Lift-off and resistance-temperature characteristics were studied.

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Processing of Tin Oxide Nanoparticles by Inert Gas Condensation Method and Characterization

  • Simchi, Abdolreza;Kohi, Payam
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.122-123
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    • 2006
  • Tin oxide nanoparticles (n-SnO and $n-SnO_2$) were synthesized by the inert gas condensation (IGC) method under dynamic gas flow of oxygen and argon at various conditions. Transmission electron microscopy (TEM) and X-ray diffraction (XRD) method were used to analysis the size, shape and crystal structure of the produced powders. The synthesized particles were mostly amorphous and their size increased with increasing the partial pressure of oxygen in the processing chamber. The particles also became broader in size when higher oxygen pressures were applied. Low temperature annealing at $320^{\circ}C$ in air resulted to crystallization of the amorphous n-SnO particles to $SnO_2$.

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A Study on the Way to Increase Heat Resistance of Teflon Type Thin Film Electret Applied for Industrial Sensor (산업용 센서에 사용하는 Teflon계 박막 일렉트렛의 내열성 향상에 관한 연구)

  • 김병수;이덕출
    • Journal of the Korean Society of Safety
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    • v.18 no.3
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    • pp.60-63
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    • 2003
  • For the increase the charge stability of teflon electrets for used at uncomfortable industrial circumstances with high temperature or humidity, We made an investigation into double layer effect of teflon electrets. Teflon AF film was spincoated on FEP film and then the charge storage property of AF/FEP dual film was investigated to be compared with FEP film. It was found that the AF/FEP dual film has higher surface potential than FEP film on the repeated charging and annealing process. It seems that AF/FEP dual film has higher thermal stability than FEP film through TSC measurement. If the investigations of the double layer effect of Teflon film carried out more closely with it's molecular structures and surface conditions, it may be effectively improved the stability of charge storage.

Effects of microstructures on ferroelectric properties of PZT thin films prepared by PLD (PLD에 의해 제조된 PZT 박막의 미세구조가 강유전 특성에 미치는 영향)

  • 백동수;김민철;신현용;박용웅;윤석진
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.11a
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    • pp.224-227
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    • 1999
  • Ferroelectric Pb(Zr$\sub$0.52/Ti$\sub$0.48/)O$_3$ thin films were fabricated by pulsed laser deposition, mainly varying process conditions such as substrate temperature, oxygen pressure, and laser energy, PZT films annealed at more than 600$^{\circ}C$ were crystallized into pure perovskite phases regardless of deposition temperatures. Lower deposition temperature of 400$^{\circ}C$ accompanied with post-annealing at 650$^{\circ}C$ resulted in denser microstructures with extremely small grains compated to those of thin films annealed at higher deposition temperatures. Hysteresis curves of thin film with small grains exhibitied good squareness and low leakage characteristics.

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Electrical Characteristics of Ultra-thin $SiO_2$ Films experienced Hydrogen or Deuterium High-pressure Annealing (고압의 수소 및 중수소 분위기에서 열처리된 실리콘 산화막의 전기적 특성 관찰)

  • Lee, Jae-Sung;Baek, Jong-Mu;Do, Seung-Woo;Jang, Cheol-Yeong;Lee, Yong-Hyun
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.07a
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    • pp.29-30
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    • 2005
  • Experimental results are presented for the degradation of 3 nm-thick gate oxide ($SiO_2$) under both Negative-bias Temperature Instability(NBTI) and Hot-carrier-induced(HCI) stresses using P and NMOSFETs that are annealed with hydrogen or deuterium gas at high-pressure (1~5 atm.). Statistical parameter variations depend on the stress conditions. We suggest that deuterium bonds in $SiO_2$ film is effective in suppressing the generation of traps related to the energetic hot electrons.

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DEVELOPMENT OF THE ENIGMA FUEL PERFORMANCE CODE FOR WHOLE CORE ANALYSIS AND DRY STORAGE ASSESSMENTS

  • Rossiter, Glyn
    • Nuclear Engineering and Technology
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    • v.43 no.6
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    • pp.489-498
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    • 2011
  • UK National Nuclear Laboratory's (NNL's) version of the ENIGMA fuel performance code is described, including details of the development history, the system modelled, the key assumptions, the thermo-mechanical solution scheme, and the various incorporated models. The recent development of ENIGMA in the areas of whole core analysis and dry storage applications is then discussed. With respect to the former, the NEXUS code has been developed by NNL to automate whole core fuel performance modelling for an LWR core, using ENIGMA as the underlying fuel performance engine. NEXUS runs on NNL's GEMSTONE high performance computing cluster and utilises 3-D core power distribution data obtained from the output of Studsvik Scandpower's SIMULATE code. With respect to the latter, ENIGMA has been developed such that it can model the thermo-mechanical behaviour of a given LWR fuel rod during irradiation, pond cooling, drying, and dry storage - this involved: (a) incorporating an out-of-pile clad creep model for irradiated Zircaloy-4; (b) including the ability to simulate annealing out of the clad irradiation damage; (c) writing of additional post-irradiation output; (d) several other minor modifications to allow modelling of post-irradiation conditions.

MAGNETIC PROPERTIES OF NANOCRYSTALLIZED METALLIC GLASSES AT ELEVATED TEMPERATURES

  • Lachowicz, Henryk K.
    • Journal of the Korean Magnetics Society
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    • v.5 no.5
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    • pp.589-596
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    • 1995
  • In the present paper some of the magnetic properties of the nanocrystalline Fe-based magnets produced by an appropriate annealing of their metallic glass precursors are reviewed. These properties are discussed on the grounds of their characteristics measured at the elevated temperatures. It is shown that the effective magnetostriction these magnets display, results from the competition among two contributions of the opposite sign originating from the individual magnetic phases, crystalline phase and the residual glassy matrix in which the nanocrystallites are embedded. It is also shown that at certain conditions the magnets considered expose superparamagnetic behavior and that their isothermal magnetization characteristics can successfully be used to calculate the distribution of the particle volumes. Application of the recently invented new genetic algorithm method, a powerful tool to calculate these distributions is, finally, presented.

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Preparation of Magnesium Oxide Nanowires from a Magnesium Foil (마그네슘 금속으로부터의 산화마그네슘 나노와이어 제조)

  • Lee, Byung Gun;Choi, Jinsub
    • Applied Chemistry for Engineering
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    • v.22 no.5
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    • pp.514-517
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    • 2011
  • Herein, we fabricated magnesium oxalate nanostructures by chemical etching of a magnesium foil in alcoholic solvents containing acidic media. Interestingly, we could obtain magnesium oxalate nanowires in ethanolic oxalic acid. Growth mechanism for magnesium oxalate nanowires was investigated in terms of etching time. Annealing conditions were determined from TGA results. Magnesium oxalate nanowires were converted to magnesium oxide nanowires by thermal treatment and the magnesium oxide nanowires were examined by FE-SEM and FT-IR measurement.

A Study on the Fabrication and Structural Properties of Al-Co/AlN-Co Thin Films

  • Han, Chang-Suk;Han, Seung-Oh
    • Korean Journal of Metals and Materials
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    • v.49 no.3
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    • pp.256-263
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    • 2011
  • We have synthesized Al-Co/AlN-Co multilayer films with different layer thicknesses by using a Two-Facing Target Type dc Sputtering (TFTS) system. The deposited films were annealed isothermally at different temperatures and their microstructure, magnetic properties and resistivity were investigated. The magnetization of the as-deposited films was found to be very small, irrespective of layer thickness. It was found that the annealing conditions and layer thickness ratio of Al-Co to AlN-Co (LTR) were able to control the microstructure, as well as the physical properties of the prepared films. The resistivity and magnetization increased and the coercivity decreased with a decreasing LTR. A high resistivity of 2500 ${\mu}{\Omega}-cm$, a magnetization of 360 $emu/cm^3$, and a coercivity of 5 Oe were obtained for the films with LTR=0.175.

Fabrication and Characterization of AlN films Containing Various Amounts of Co Content

  • Bae, Chang-Hwan;Han, Seung-Oh;Han, Cahng-Suk
    • Korean Journal of Metals and Materials
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    • v.48 no.3
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    • pp.268-275
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    • 2010
  • A new approach is described for preparing AlN thin films containing various amounts of Co content by using a two-facing targets type sputtering (TFTS) system. The deposited films were annealed isothermally at different temperatures and their microstructure, magnetic properties and resistivity were investigated. A small saturation magnetization ($4{\pi}Ms=0.52{\sim}0.85kG$) was observed irrespective of Co content in the asdeposited films. It was found that annealing conditions can control physical properties as well as the microstructure of the films. A high saturation magnetization (3.7 kG) and resistivity of $2200{\mu}{\Omega}-cm$ was obtained for AlN films containing 25 at.% Co.