• Transactions of the Korean Society of Mechanical Engineers
• /
• v.16 no.9
• /
• pp.1643-1653
• /
• 1992

A method, which uses analytical or numerical modal analysis results, e.g. from finite element analysis, to select desirable response measurement and excitation points for an efficient modal testing is introduced. First, points of master degree of freedom(DOP) are determined so as to statistically minimize errors between responses of a full order model and those estimated from the reduced order model. Such master DOF's are selected as the response measurement points. Then a criterion named 'driving point model constant(DPMC)' related to the magnitudes of resonance peaks of the driving point freqency response functions used to select the point of excitation out of the master DOF's. In this work, the method is demonstrated through applications to modal testing on a one dimensional cantilever beam and an aluminum plate and the results are compared with those by another technique. also, the method is applied to a two dimensional structural component of a passenger car.

• Analytical Science and Technology
• /
• v.26 no.3
• /
• pp.165-173
• /
• 2013

To establishment of PT Program for Indoor air quality field that manufacture of confidential development PTMs (proficiency testing materials) and examined of proficiency testing evaluation included sampling process whether or not that is valid. Confirmation of homogeneity and stability of PTMs prepared. PTMs were confirmed to be homogeneous enough to be used as proficiency testing materials since withinbottle homogeneities of the RMs were lower than 0.3 times of targeted standard deviation of proficiency testing. The result of this study showed that the Robust RSD of proficiency testing for VOCs (volatile organic compounds) appeared 23~43% in concentration of 50~320 ${\mu}g/m^3$ for Method A(Distribution by adsorption in Tenax-tube of VOCs), but less 13~42% in concentration of 200~1200 ${\mu}g/m^3$, 16~31% in concentration of 100~450 ${\mu}g/m^3$ for Method B (distribution by VOCs of gas phase in 10L Tedalr bag), C (directly sampling of cylinder with high pressure) respectively. The result of this study showed that method C with sampling is most adequate to the proficiency testing for VOCs in indoor air.

• Analytical Science and Technology
• /
• v.21 no.4
• /
• pp.284-295
• /
• 2008

For plastics samples, a method using combustion ion chromatography was selected as a method for rapid low-cost analysis to test whether hazardous substances are contained or not. Using combustion ion chromatography, a verification test for F, Cl and Br compounds generated a linear calibration curve with a correlation coefficient of $r^2$ = 0.999~1.000 in the calibration range from 0.5 to 4.0 mg/kg. The detection limits were found to be 0.005~0.024 mg/kg and quantitative limits were found to be 0.014~0.073 mg/kg. The recoveries of combustion ion chromatography using certified reference material (CRM) were found to be 95.5~104.9%. Based on these results, a proficiency test was conducted together with several laboratories in and out of the country, to make comparative analysis of the results from each laboratory. As a result, the data supported the use of combustion ion chromatography as an effective analysis method to deal with regulations for halogen-free electronic products and for other hazardous substances in the electronic products.

• Analytical Science and Technology
• /
• v.25 no.3
• /
• pp.178-189
• /
• 2012

As phthalates classified as toxic to reproduction category 2 and endocrine disrupting chemicals were more strictly regulated as Substances of Very High Concern (SVHC) for authorization in under EU REACH and considered as priority substances in RoHS II, standardization of phthalate testing method is now being proposed in IEC 62321 of IEC TC 111 and the 2nd revision of KS M 1991 is also finished. In order to assist standardization activities related to phthalating testing, solvent extraction part of existing national standards were compared and verified. Recovery of DEHP (diethylhexyl phthalate) from PVC (polyvinyl chloride) by Soxhlet extraction increased in the order of methanol, toluene, dichloromethane and hexane from 46.9% to 95.3% as measured by GC-MS. Optimum extraction time was verified to be 6 hours using hexane. Recovery of DBP (dibutyl phthalate), BBP (butylbenzyl phthalate), and DEHP from different matrixes such as PVC, nitro cellulose, ABS (acrylonitrile butadiene styrene). and EPDM(ethylene propylene diene monomer) rubber were evaluated to be more than 90% up to 99%. The detection limits of phthalates in solvent extraction followed by GC-MS analysis were 0.08~0.3 ${\mu}g/mL$ in solution and 8~30 mg/Kg in polymeric samples. GC-MS analyses of phthalates were carried out using different solvent extraction based on the EN 14372, ASTM D 7083, Japanese test method (MHLW 0906-4) and KS M 1991, proving that equivalent recoveries ranging from 98%~99% were obtained. DBP and DEHP were detected in three consumer products such as a child toy, a power cable and manicure with the amount of 22~1,910 mg/kg.

• Steel and Composite Structures
• /
• v.34 no.3
• /
• pp.453-465
• /
• 2020

Influences of different variables that affect the effective flexural rigidity of reinforced concrete (RC) members are not considered in the most seismic codes. Furthermore, in the last decades, the application of steel fibers in concrete matrix designs has been increased, requiring development of an accurate analytical procedure to calculate the effective flexural rigidity of steel fiber reinforced concrete (SFRC) members. In this paper, first, a nonlinear analytical procedure is proposed to calculate the SFRC members' effective flexural rigidity. The proposed model's accuracy is confirmed by comparing the results obtained from nonlinear analysis with those recorded from the experimental testing. Then a parametric study is conducted to investigate the effects of different parameters such as varying axial load and steel fiber are then investigated through moment-curvature analysis of various SFRC (normal-strength concrete) sections. The obtained results show that increasing the steel fiber volume percentage increases the effective flexural rigidity. Also it's been indicated that the varying axial load affects the effective flexural rigidity. Lastly, proper equations are developed to estimate the effective flexural rigidity of SFRC members.

• Transactions of the Korean Society of Automotive Engineers
• /
• v.20 no.6
• /
• pp.100-106
• /
• 2012

Recently, the demand to acquire and improve durability performance has steadily risen in rubber components design. In design process of a rubber component, an analytical prediction is the most effective way to improve fatigue life. Existing methods of analytical estimation have mainly used an equation for fatigue life obtained from fatigue test data. However, such formula is rarely used due to costs and time required for fatigue testing, as well as randomness of rubber materials. In this paper, we describe fatigue life estimation of rubber component using only the results from a relatively simple tearing test. We estimated fatigue life of the Janggu type fatigue specimen and the automotive motor mount, and evaluated reliability of the proposed method by comparing the estimated values with actual test results.

• Analytical Science and Technology
• /
• v.9 no.1
• /
• pp.91-97
• /
• 1996

The extent of binding($K_B$) between chemical compound and humic acid was measured as an indicator of decrease in toxicity. From the experimental $K_B$ and estimated $K_B$ calculated from $K_{ow}$, no reduction of toxicity among test chemicals in aquatic systems were predicted except P,P'-DDT. The effect of humic acid on aquatic organisms is not expected to be significant for the compounds with $K_B{\leq}10^5$ or $K_{ow}{\leq}10^6$.

• Analytical Science and Technology
• /
• v.5 no.1
• /
• pp.91-96
• /
• 1992

A simple and cheap AC voltammeter was manufactured in our lab. This instrument consists of a DC function generator and a lock-in amplifier. We tested this instrument in some chemical systems. Our data, CV voltammogram and AC voltammogram, obtained form using a Pt working electrode in 1M $H_2SO_4$ and a reversible system of $1{\times}10^{-3}M$ ${Fe(CN)_6}^{3-}$ proved our system works well. The quantitative result of iodine is also obtained.

• Steel and Composite Structures
• /
• v.14 no.2
• /
• pp.105-120
• /
• 2013

Flexural behavior of thin walled steel-concrete composite sections as cross sections for beams is investigated by conducting an experimental study supported by applicable analytical predictions. The experimental study consists of testing up to failure, simply supported beams of effective span 1440 mm under two point loading. The test specimens consisted of composite box and channel (with lip placed on tension side and compression side) sections, the behavior of which was compared with companion empty sections. To understand the role of shear connectors in developing the composite action, some of the composite sections were provided with novel simple bar type and conventional bolt type shear connectors in the shear zone of beams. Two RCC beams having equivalent ultimate moment carrying capacities as that of composite channel and box sections were also considered in the study. The study showed that the strength to weight ratio of composite beams is much higher than RCC beams and ductility index is also more than RCC and empty beams. The analytical predictions were found to compare fairly well with the experimental results, thereby validating the applicability of rigid plastic theory to cold-formed steel concrete composite beams.

• Analytical Science and Technology
• /
• v.27 no.4
• /
• pp.196-200
• /
• 2014

Currently nonaqueous titration method for the assay method using the hazardous reagent, mercury acetate for difemerine hydrochloride has been used in Korean Pharmaceutical Codex. We developed an alternative titration assay method by substituting the use of the hazardous reagent, mercury acetate to the use of less toxic ones like ethyl alcohol. The linearity of the calibration curves in the desired concentration range was good (r>0.999). Precision was less than 0.64%. Accuracy was obtained with recoveries in range of 99.10% and 99.71%. The developed assay could be expected to become valuable tools for revising the Korean Pharmaceutical Codex.