• Resources Recycling
• /
• v.18 no.6
• /
• pp.18-23
• /
• 2009

An investigation on the synthesis of aluminum citrate, one of the aluminum organic compounds, has been performed using aluminum chloride solutions as a starting material. For the synthesis of aluminum citrate, citric acid was added to aluminum solutions with the mole ratio of citric acid to aluminum to be 2.5 and aluminum citrate synthesized was also characterized in terms of chemical analysis, X-ray diffraction, particle size measurement and SEM analysis. As a result, it was found that the ratio of ethanol/Al solution more than 4.0 was required for the synthesis of aluminum citrate from aluminum solutions. Furthermore, the pH should be controlled to be more than 7.0 in order to obtain the recovery of aluminum citrate higher than 97%. From the chemical analysis of aluminum citrate synthesized in this work, the content of $NH_4$, Al and C was found to be 17.0, 4.01 and 25.7%, respectively. Accordingly, the aluminum citrate synthesized from aluminum solutions was confirmed to be $(NH_4)_5Al(C_6H_4O_7)_2{\cdot}2H_2O$.

• Phonetics and Speech Sciences
• /
• v.8 no.4
• /
• pp.89-95
• /
• 2016

The purpose of this work is to analyze and synthesize the pseudo-periodicity of voice using a source model. A speech signal has periodic characteristics; however, it is not completely periodic. While periodicity contributes significantly to the production of prosody, emotional status, etc., pseudo-periodicity contributes to the distinctions between normal and abnormal status, the naturalness of normal speech, etc. Measurement of pseudo-periodicity is typically performed through parameters such as jitter and shimmer. For studying the pseudo-periodic nature of voice in a controlled environment, through collected natural voice, we can only observe the distributions of the parameters, which are limited by the size of collected data. If we can generate voice samples in a controlled manner, experiments that are more diverse can be conducted. In this study, the probability distributions of vowel pitch variation are obtained from the speech signal. Based on the probability distribution of vocal folds, pulses with a designated jitter value are synthesized. Then, the target and re-analyzed jitter values are compared to check the validity of the method. It was found that the jitter synthesis method is useful for normal voice synthesis.

• Journal of the Earthquake Engineering Society of Korea
• /
• v.24 no.4
• /
• pp.179-187
• /
• 2020

Seismic qualification of equipment including piping is performed by using floor response spectra (FRS) or in-structure response spectra (ISRS) as the earthquake input at the base of the equipment. The amplitude of the FRS may be noticeably reduced when obtained from coupling analysis because of interaction between the primary structure and the equipment. This paper introduces a method using a modal synthesis approach to generate the FRS in a coupled primary-secondary system that can avoid numerical instabilities or inaccuracies. The FRS were generated by considering the dynamic interaction that can occur at the interface between the supporting structure and the equipment. This study performed a numerical example analysis using a typical nuclear structure to investigate the coupling effect when generating the FRS. The study results show that the coupling analysis dominantly reduces the FRS and yields rational results. The modal synthesis approach is very practical to implement because it requires information on only a small number of dynamic characteristics of the primary and the secondary systems such as frequencies, modal participation factors, and mode shape ordinates at the locations where the FRS needs to be generated.

• Korean Journal of Veterinary Research
• /
• v.58 no.2
• /
• pp.65-72
• /
• 2018

The present study observed the effects of a green tea (Camellia sinensis) flower extract (GTFE) on melanin synthesis in B16-F10 melanoma cells. GTFE exhibited antioxidant activity on 2,2-diphenyl-1-picrylhydrazyl and inhibited mushroom tyrosinase activity in a dose-dependent manner. Furthermore, GTFE significantly diminished ${\alpha}-melanocyte$ stimulating hormone (${\alpha}-MSH$) stimulated cellular melanin content and tyrosinase activity throughout the concentration range evaluated. Based on RNA sequencing analysis, differential gene expression patterns observed in ${\alpha}-MSH$ stimulated B16-F10 melanoma cells were normalized by the addition of GTFE. In particular, the expression levels of melanoregulin and tyrosinase genes which are key regulating genes in melanin synthesis were up-regulated by 3.5 and 3 fold respectively by ${\alpha}-MSH$, and were normalized to control levels by the addition of GTFE. The results suggest that GTFE inhibits melanin synthesis in ${\alpha}-MSH$ stimulated B16-F10 melanoma cells by normalizing expression of genes that are essential for melanin synthesis. Overall, the results suggest that GTFE could be applied in the development of a whitening agent for the treatment of dermal hyperpigmentation.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.24 no.9 s.180
• /
• pp.2201-2210
• /
• 2000

Vibration of a rotating disk-spindle system is analyzed by using Hamilton's principle, FEM and substructure synthesis. A rotating disk undergoes the rigid body motion and the elastic deformation. It s equation of motion is derived by Kirchhoff plate theory and von Karman nonlinear strain. A rotating shaft is described by Rayleigh beam theory considering the axial rigid body motion. The stationay shaft supporting the rotating disk-spindle-bearing system is modeled by Euler beam theory, and the stiffness of ball bearing is determined by A.B.Jones' theory. FEM is used to solve the derived governing equations, and substructure synthesis is introduced to assemble each structure of the rotating disk-spindle system. The developed theory is applied to the spindle system of a 35' computer hard disk drive with 3 disks to verify the simulation results. The simulation results agree very well with the experimental ones. The proposed theory may be effectively expanded to the complex structure of a disk-spindle system.

• Transactions of the Korean Society for Noise and Vibration Engineering
• /
• v.16 no.8 s.113
• /
• pp.814-821
• /
• 2006

A structural coupling method is developed for the dynamic analysis of a nonlinear structure with concentrated nonlinear hinge joints or sliding lines. The component mode synthesis method is extended to couple substructures and the nonlinear models. In order to verify the improved coupling method, a numerical plate model consisting of two substructures and torsional springs, is synthesized by using the proposed method and its modal parameters are compare with analysis data. Then the coupling method is applied to a three-substructure-model with the nonlinearity of sliding lines between the substructures. The coupled structural model is verified from its dynamic analysis. The analysis results show that the improved coupling method is adequate for the structural nonlinear analyses with the nonlinear hinge and sliding mode condition.

• Proceedings of the Society of Korea Industrial and System Engineering Conference
• /
• 2002.05a
• /
• pp.445-454
• /
• 2002

This article explains the theory of multiple mode/physical coordinate synthesis method in order to analyze the dynamic characteristics for an huge marine engine. The theory leads to make a simulation code. The natural frequencies obtained from the simulation code is compared to those from a commercial analysis software, ANSYS. The simulation code is well reviewed.

• Journal of KSNVE
• /
• v.3 no.1
• /
• pp.77-82
• /
• 1993

In general, the dynamic analysis with FEM(Finite Element Method) of large structures requires large computer memory space and long computational time. For the purpose of economical dynamic analysis of large structures, most of engineers want to use an efficient solution algorithm. This paper reports the modified CMS(Component Mode Synthesis) method which uses more efficient algorithm than the classical CMS method. In this paper, it is shown that Ritz vector sets can play the role of normal mode vector sets of substurctures in the CMS algorithm. The modified CMS method has good convergence performance compared with that of the classical CMS method.

• Advances in nano research
• /
• v.2 no.2
• /
• pp.89-98
• /
• 2014

A novel and simple method for the synthesis of nano-magnetite particles is disclosed. In the novel procedure, $Fe^{2+}$ is the only source of metal cation. Carboxymethylcellulose (CMC) is used as the structure directing agent. The phase analysis of the nano-particles was performed using XRD and electron diffraction techniques. Size and morphology analysis was performed using light scattering and TEM techniques. The effect of $NH_4OH$ solution (32 wt. %) at different CMC concentrations on the size distribution of the final magnetite powders is studied. An optimal base concentration exists for each CMC concentration leading to minimal agglomeration. There exists a minimum CMC concentration (0.0016 wt. %), lower than that no magnetite forms. It is shown that using the new method, it is possible to immobilize a lipase enzyme (Candida Rugosa) with immobilization efficiency larger than 98 % with a loading more than 3 times the reported value in the literature. The latter phenomenon is explained based on the agglomerate state of the nano-particles in the liquid phase.

• Journal of the Institute of Electronics Engineers of Korea SC
• /
• v.37 no.2
• /
• pp.8-15
• /
• 2000

This study presents an H$_{\infty}$ optimal controller synthesis by the frequency domain analysis of weighting function. The main purpose of our study is to visualize weighting function domains and open loop transfer function domains that satisfy robustness and performance. Also we aim to simplify the iterative algorithm for H$\infty$ optimal controller synthesis. We report that the designed regulator by the proposed method in this paper satisfies the desired specifications and performance in spite of the plant uncertainty variation at any operating point.