• Title/Summary/Keyword: aluminium complex

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A Study on Preparation of Industrial Polyaluminium Sulfate (공업용 포리황산알미늄의 제조에 관한 연구)

  • 육창규;이내우
    • Journal of Environmental Science International
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    • v.5 no.2
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    • pp.203-210
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    • 1996
  • To improve coagulation characteristics and to reduce dossage of chemicals in watertreatment, polyaluminium sulfate was manufactured by reaction of polymerization between aluminium sulfate and sodium aluminate. As the results of affirmation and performance test, the yield of product was about 24% from molecular cut on levels by ultrafilteration method. The type of molecular is nearly affirmated as a kind of complex like AIm(OH)n(3m-n)+ from Scanning Electron Microscopy (S.E.M.) and X-ray diffraction test. Since the synthesized polymer was supposed to be quasi, further study for stabilization was required.

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A Study on Manufacturing Process of Cr6+-free Zinc/Aluminium Complex layer (6가 크롬을 대체한 친환경 Zn/Al 복합 화성피막 제조기술에 대한 연구)

  • Choe, Hye-Gang;Kim, Dong-Hyeon;Park, Jeong-Hwan;Jo, Dae-Hyeong
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2013.05a
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    • pp.55-55
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    • 2013
  • 중금속이 함유되지 않은 친환경 방청코팅제 개발을 위해 현재 국내 시장을 잠식하고 있는 외산 무기 아연말 피막기술의 국산화 상용기술 방안과 경쟁력 확보를 위해 다양한 연구방법을 시도하였으며, 외산 기술에 상응하는 SST 1,000시간이상의 고내식성 확보 기술을 제안하고자 한다.

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Development f head-neck complex dummy for experimental study (실험적 해석을 위한 머리-목 형태의 더미 개발)

  • Kim, Yeong-Eun;Nam, Dae-Hun;Koh, Chang-Hun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.21 no.7
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    • pp.1058-1072
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    • 1997
  • A head-neck complex dummy, for measuring brain pressure and reaction force in the cervical spine was developed for experimental study related in injury mechanism. Dummy comprised aluminium-casted head with water filled cavity for simulating brain and mechanical neck assembled with six motion segments. Several kinds of experiments (compression, bending, cyclic modulus, relaxation and constant velocity profile) for the developed mechanical neck showed that this neck model is biomechanically reliable compared with in-vitro test results. As an application of developed head-neck complex dummy, shock absorbing properties of protective helmet was chosen. The experiments showed that the maximum pressure increment of brain after impact was tolerable compared with the guide line for mild brain injury pressure (25psi). Constrast to this results, the reaction force in the neck was high enough to produce failure in the cervical spine.

X-ray/gamma radiation shielding properties of Aluminium-Bariume-Zinc Oxide nanoparticles synthesized via low temperature solution combustion method

  • K.V. Sathish;K.N. Sridhar;L. Seenappa;H.C. Manjunatha;Y.S. Vidya;B. Chinnappa Reddy;S. Manjunatha;A.N. Santhosh;R. Munirathnam;Alfred Cecil Raj;P.S. Damodara Gupta;B.M. Sankarshan
    • Nuclear Engineering and Technology
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    • v.55 no.5
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    • pp.1519-1526
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    • 2023
  • For the first time Aluminium-BariumeZinc oxide nanocomposite (ZABONC) was synthesized by solution combustion method where calcination was carried out at low temperatures (600℃) to study the electromagnetic (EM) (X/γ) radiation shielding properties. Further for characterization purpose standard techniques like PXRD, SEM, UV-VISIBLE, FTIR were used to find phase purity, functional groups, surface morphology, and to do structural analysis and energy band gap determination. The PXRD pattern shows (hkl) planes corresponding to spinel cubic phase of ZnAl2O4, cubic Ba(NO3)2, α and γ phase of Al2O3 which clearly confirms the formation of complex nano composite. From SEM histogram mean size of nano particles was calculated and is in the order of 17 nm. Wood and Tauc's relation direct energy band gap calculation gives energy gap of 2.9 eV. In addition, EM (X/γ) shielding properties were measured and compared with the theoretical ones using standard procedures (NaI (Tl) detector and multi channel analyzer MCA). For energy above 356 keV the measured shielding parameters agree well with the theory, while below this value slight deviation is observed, due to the influence of atomic/crystallite size of the ZABONC. Hence synthesized ZABONC can be used as a shielding material in EM (X/γ) radiation shielding.

The Effects of Material Attenuation on Acoustic Resonance Scattering from Cylindrical Tubes (초음파 감쇠가 원형관의 공명 산란에 미치는 영향)

  • Lee, J.P.;Choi, M.S.;Joo, Y.S.;Lim, H.T.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.14 no.1
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    • pp.23-31
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    • 1994
  • Sound scattering by cylindrical tubes submerged in water is numerically analyzed with material attenuation considered. Complex wave numbers is introduced to see the effects of material attenuation on resonance scattering Backscattering pressures from the shells immersed in water are calculated for air-filled aluminium and acryl tubes. In order to investigate the resonance characteristics in detail, numerical analysis program has been completed which enables us to evaluate the effects of material attenuation. The testing of the program by comparison with previous results is reported and calculation results are compared and discussed for both aluminium and acryl tubes with material attenuation considered. The resonance peak and width is strongly affected by attenuation and this becomes severe as the peak is sharp and narrow and $k_{1{\alpha}}$ is high.

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Preparation and Sintering Behavior of Monodispersed Alumina-Zirconia Fine Powders (단분산 $Al_2O_3-ZrO_2$ 복합분말의 합성과 소결특성)

  • 부재필;송용원;최상홀
    • Journal of the Korean Ceramic Society
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    • v.31 no.10
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    • pp.1209-1217
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    • 1994
  • Monodispersed alumina-zirconia fine powders were prepared by controlled hydrolysis of alkoxides. These powders and the sintered bodies were characterized. Aluminium alkoxide and zirconium alkoxide were dissolved into complex solvent with butanol and n-propanol, and by acetonitrile added hydrolytic solution, hydrolysis rate was controlled. The oil, as a dispersant, was added in hydrolytic solution, and then prepared powders were nano-sized and well-monodispersed. In the case of hydroxypropyl celluose (HPC) as a dispersant, it was added in complex solution with butanol and iso-propanol, sub-micrometer sized and well-monodispersed powders could be prepared. The value of relative density (R.D.) and tetragonal phase fraction of zirconia in the sintered body made by nano-meter sized powders were respectively higher than those in the case of sub-micrometer sized one.

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Spectrophotometric Determination of Aluminium Ion in Drinking Water by Flow Injection Analysis (흐름주입분석법에 의한 음용수 중 알루미늄 이온의 분광광도법 정량)

  • Choi, Yong-Wook;Jin, Jae-Young
    • Journal of the Korean Chemical Society
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    • v.44 no.5
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    • pp.422-428
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    • 2000
  • Optimum analytical conditions of the aluminium ion were established by flow injection analysis. Eriochrome Cyanine R(ECR) dye reacts with the aluminium ion at pH 6.0 to form a complex that exhibits maximum absorption at 535 nm. Reaction conditions including the mixing and the reaction coil length, the concentration and the pH of the buffer solutio, temperature, and injection loop volume were optimized to intro-duce this reaction into flow injection analysis. The results were as follows. A mixing coil length of 0.5 m and a reaction coil length of 4.0 m, the pH 6.0 and 1M of acetate buffer solution, the ECR concentration of 0.56 mM, the reaction temperature of 40$^{\circ}C$, the injection loop volume of 300${\mu}L$ were chosen as optimum conditions. Under these conditions the detection limit of the aluminiumion was less than 0.05 mg/L and the repeatability was better than 1%. A sampling frequency of 24 times for an hour was achieved. Interfering ions such as $F^-$, HP$O_4^{2-}$, $Fe^{2+}$, $Fe^{3+}$, $Mn^{2+}$, and other anions were tested, interference did not occur up to 1,000mg/L of ion concentration and up to 2,CO0mg/L of sulfate ion con-centration. This method was applied for the determination of aluminium ion in tap water and ground water of Jeonju and the Gochang area. The results showed that the aluminium residual in tap water of the Jeonju area was at a mean of 0.478mg/L and that in tap water of the Gochang area was at a mean of 0.278mg/L. Aluminium ion residual of the tap waters in the Jeonju area was higher level than that in the Gochang area. Aluminium residual in the ground water of the Jeonju area was 0.386 mg/L and was lower compared to 0.564 mg/L for the Gochang area.

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Analysis of Complex Heat Distribution in TIG Assisted Friction Stir Welding of Dissimilar Materials (STS304+Al6061) (이종재료(STS304+Al6061) TIG-FSW Hybrid 용접부의 열 특성 해석)

  • Bijoy, M.S.;Bang, Hee-Seon;Bang, Han-Sur
    • Proceedings of the KWS Conference
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    • 2010.05a
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    • pp.59-59
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    • 2010
  • Friction stir welding has become a viable and important manufacturing alternative or fabrication component, especially in aerospace and automobile applications involving aluminium alloys. In recent years, there is an increasing interest for FSW of dissimilar metals and alloys, particularly systems which are difficult to weld by conventional, thermal (or fusion) welding. In this study we tried to analyse the complex heat distribution occurring in TIG assisted FSW of dissimilar butt joint (STS304 and Al6061). For this, an analytical model for heat generation by FSW based on contact conditions has been developed. The heat input was calculated considering the coefficient of friction and slip factor between each work piece material with the tool material. The thermal model is used to generate the temperature characteristics curve, which successfully predicts the maximum welding temperature in each alloys. The analysis was carried out using the in-house solver.

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Characteristics of Surface Roughness Based on Wire Vibration and Wire-cut Electric Discharge Machining of Aluminum Alloy 6061 (I) (알루미늄 합금 6061에서 와이어 진동부가에 의한 와이어 컷 방전가공에 따른 표면 거칠기 특성 (I))

  • Ryu, Cheong-Won;Choi, Seong-Dae
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.14 no.2
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    • pp.59-66
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    • 2015
  • The production of high value-added products requires efficient processing and this constant demand for complex shape processing has led to the need for hybrid processing. In this study, the surface characteristics of hybrid machining, which combines wire-cut E.D.M and vibration, are examined. The selected experimental parameters are verticality, waveform, amplitude, peak current and frequency. The experimental results provide a guideline for selecting reasonable machining parameters. Surface roughness was improved by increasing the amplitude of the vibration.

Characteristics of Surface Roughness According to Wire Vibration and Wire-cut Electric Discharge Machining of Aluminum Alloy 6061 (III) (알루미늄 합금 6061에서 와이어 진동부가에 의한 와이어 컷 방전가공에 따른 표면 거칠기 특성 (III))

  • Ryu, Cheong-Won;Choi, Seong-Dae
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.15 no.1
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    • pp.81-88
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    • 2016
  • Recently, high-efficiency machining in the production of high-value products with complex shapes has constantly been required along with the need for hybrid machining. In this study, in addition to wire-cut Electric Discharge Machining (EDM) and vibration, we present the possibility of a hybrid process by carrying out an experiment with aluminum alloy, and the hybrid process determines the nature of the surface. The selected experimental parameters are waveform, amplitude, peak current, and two-dimensional (2D) vibration. The experimental results give the guideline for selecting reasonable machining parameters. The surface roughness was improved about 20% with increases in the amplitude of the vibration.