• Title/Summary/Keyword: aging treatment

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Aging Effect of Magnetic Properties in Amorphous $Fe_{78}B_{13}Si_9$ Alloy (비정질 $Fe_{78}B_{13}Si_9$ 합금의 자기적 특성의 경년 열화)

  • Kim, Ki-Uk;Min, Bog-Ki;Song, Jae-Sung;Hong, Jin-Wan;Cho, Hyun-Jin;Lee, Dong-Hee
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1988.05a
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    • pp.49-51
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    • 1988
  • The heat treatment condition and aging behavior of melt spun amorphous $Fe_{78}B_{13}Si_9$(Metglas 26058-2) were studied with investigating its magnetic properties, i.e., Br, $B_l$, Hc. The optimum heat treatment condition was $400^{\circ}C$, 1 hour under the external field of 200e, and aging was due to the surface oxidation and the appearance of local CSRO (chemical short lange order) with time and temperature. In addition. we investigated the effects of the thickness of the amorphous ribbons on the magnetic properties and aging effect of them.

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Strengthening Treatment of Aged Hanji with Solvent Soluble Polymers (용제 용해형 고분자를 이용한 열화한지의 보강처리)

  • Kim, Kang-Jae;Lee, Min-Hyung;Eom, Tae-Jin
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.44 no.1
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    • pp.1-9
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    • 2012
  • In this study, 5 solvent soluble polymers were treated on Hanji. Mechanical properties, morphology and oxidation index with thermal aging were measured on the aged Hanji, dewaxed Hanji and polymer treated Hanji. Synthetic polymers(such as polylactic acid, polybutylene succinate, polystyrene) treated Hanji had higher strength and thermal stability than cellulose derivatives(such as cellulose nitrate and cellulose acetate) treated Hanji. Polymer treated Hanji showed a little bit of color change. The oxidation index of PS treated Hanji did not increase with thermal aging because it did not have a carboxyl group in chemical structure. Finally, polystyrene was found to be the most efficient method for strengthening the dewaxed Hanji. The best aging safety and thermal stability were obtained at the polystyrene 3% solution.

Strengthening of De-waxed Paper by Methyl Cellulose (MC) and Its Preservability - Effect of Viscosity and Coating Ratio of MC - (메틸셀룰로오스에 의한 탈랍지의 강도보강처리 - 메틸셀룰오스 점도 및 도포율의 영향 -)

  • Choi, Kyoung-Hwa;Jeong, Hye Young;Cho, Byoung-Uk
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.47 no.6
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    • pp.130-138
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    • 2015
  • This study was conducted to investigate the effect of the strengthening treatment of methyl cellulose (MC) on properties and aging characteristics of the dewaxed papers during humid heating aging. Beeswax-treated Hanji was dewaxed by the supercritical fluid extraction method, and subsequently the strengthening treatment was performed with MCs having three different viscosities. MC was first applied by dipping a dewaxed paper into a MC solution whose concentration was controlled from 0.5% to 1.5%. After the strengthened papers were artificially aged at $80^{\circ}C$ and 65% RH, the changes in optical and mechanical properties of the samples were evaluated. The results show that viscosity and especially pick-up of MC influenced the strengthening efficiency and aging characteristics of dewaxed paper. Strength was increased with the MC coating weight; in addition, strengthening with MC improved preservability of the dewaxed paper. The optimum conditions for the strengthening with MC was found to be the coating ratio of 4% with 1500 cP MC.

Effects of Al Content on Microstructure and Hardness of Discontinuous Precipitates Formed by Isothermal Aging in Mg-Al Alloys (Mg-Al 합금에서 등온 시효로 생성된 불연속 석출물의 미세조직과 경도에 미치는 Al 함량의 영향)

  • Jun, Joong-Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.34 no.6
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    • pp.287-293
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    • 2021
  • This study was intended to investigate the influence of Al content on hardness and microstructural characteristics of discontinuous precipitates (DPs) formed by isothermal aging in Mg-8.7%Al and Mg-10%Al alloys. In order to obtain large amount of DPs in the microstructure, the alloy specimens were solution-treated at 688K for 24 h followed by water quenching, and then aged at 418K for 48h. The Mg-Al alloy with higher Al content was characterized by higher volume fraction of DPs at the same aging condition, lower interlamellar spacing of the DPs, thinner β phase layer and higher β phase content in the DPs. This is closely related to the higher velocity of discontinuous precipitation process resulting from the higher Al supersaturation in the α-(Mg) matrix. The Mg-10%Al alloy showed higher hardness of the DPs and greater difference in hardness between as-cast state and DPs than the Mg-8.7%Al alloy.

Effects of Submersion Aging in Chilled Water on Tenderness and Microbial Growth of Vacuum-Packed Hanwoo Meat (냉수침지 숙성법이 진공포장 한우육의 연도 및 미생물 증식에 미치는 효과)

  • 주선태;이한기;강근호;신철우;양한술;문성실;이정일;김영환;박구부
    • Food Science of Animal Resources
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    • v.22 no.3
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    • pp.228-233
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    • 2002
  • To investigate the effects of submersion aging in chilled water on tenderness and microbial growth of vacuum-packed beef, the semimembranosus muscles of Hanwoo (Korean cattle) was sampled at a commercial meat plant at 24 hrs postmortem. The samples were cut to 2.5 cm thick steaks and randomly assigned to following two treatments. The samples were stored in conventional refrigerator at 4$^{\circ}C$ after vacuum packaging for control whereas the other vacuum-packed samples were submersed in chilled water at 1$^{\circ}C$ for treatment, and both samples were stored for 14 days to measure total plate counts (TPC), sarcomere length, free calcium concentration, shear farce value and myofibrillar fragmentation index (MFI). The sarcomere length of treatment was significantly (p<0.05) longer than that of control at 3 days aging. Result suggested that submersion in chilled water of vacuum-packed beef might be effective to improve tenderness of meat compared to storage in conventional refrigerator. There were no significant differences in the shear force and MFI between control and treatment during storage. However, the free calcium concentration of samples from treatment was significantly (p<0.05) higher than that of control at 7 days of ageing. This result indicated that the lower shear force value and the longer sarcomere length of samples from treatment might be due to increasing the free calcium ion concentration in sarcoplasm during storage. On the other hands, samples from control showed significantly (p<0.05) higher number of microbial (TPC) compared to treatment during storage. from results obtained, submersion in chilled water of vacuum-packed beef could be recommended as a desirable aging method to improve tenderness of Hanwoo compared to aging in conventional refrigerator.

Ultrasonic Nonlinearity of AISI316 Austenitic Steel Subjected to Long-Term Isothermal Aging (장시간 등온열화된 AISI316 오스테나이트강의 초음파 비선형성)

  • Gong, Won-Sik;Kim, ChungSeok
    • Journal of the Korean Society for Nondestructive Testing
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    • v.34 no.3
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    • pp.241-247
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    • 2014
  • This study presents the ultrasonic nonlinearity of AISI316 austenitic stainless steels subjected to longterm isothermal aging. These steels are attractive materials for use in industrial mechanical structures because of their strength at high-temperatures and their chemical stability. The test materials were subjected to accelerated heat-treatment in an electrical furnace for a predetermined aging duration. The variations in the ultrasonic nonlinearity and microstructural damage were carefully evaluated through observation of the microstructure. The ultrasonic nonlinearity stiffly dropped after aging for up to 1000 h and, then, monotonously decreased. The polygonal shape of the initial grain structures changed to circular, especially as the annealing twins in the grains dissolved and disappeared. The delta ferrite on the grain boundaries could not be observed at 1000 h of aging, and these continuously transformed into their sigma phases. Consequently, in the intial aging period, the rapid decrease in the ultrasonic nonlinearity was caused by voids, dislocations, and twin annihilation. The continuous monotonic decrease in the ultrasonic nonlinearity after the first drop resulted from the generation of $Cr_{23}C_6$ precipitates and ${\sigma}$ phases.

Improving Effect of Silk Peptides on the Cognitive Function of Rats with Aging Brain Facilitated by D-Galactose

  • Park, Dong-Sun;Lee, Sun-Hee;Choi, Young-Jin;Bae, Dae-Kwon;Yang, Yun-Hui;Yang, Go-Eun;Kim, Tae-Kyun;Yeon, Sung-Ho;Hwang, Seock-Yeon;Joo, Seong-Soo;Kim, Yun-Bae
    • Biomolecules & Therapeutics
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    • v.19 no.2
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    • pp.224-230
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    • 2011
  • In order to develop silk peptide (SP) preparations possessing cognition-enhancing effect, several candidates were screened through in vitro assays, and their effectiveness was investigated in facilitated brain aging model rats. Incubation of brain acetyl-cholinesterase with SP-PN (1-1,000 ${\mu}g/ml$) led to inhibition of the enzyme activity up to 35%, in contrast to a negligible effect of SP-NN. The expression of choline acetyltransferase (ChAT) mRNA of neural stem cells expressing ChAT gene (F3.ChAT) was increased by 24-hour treatment with 10 and 100 ${\mu}g/ml$ SP-NN (1.35 and 2.20 folds) and SP-PN (2.40 and 1.34 folds). Four-week subcutaneous injections with D-galactose (150 mg/kg) increased activated hippocampal astrocytes to 1.7 folds (a marker of brain injury and aging), decreased acetylcholine concentration in cerebrospinal fluid by 45-50%, and thereby impaired learning and memory function in passive avoidance and water-maze performances. Oral treatment with SP preparations (50 or 300 mg/kg) for 5 weeks from 1 week prior to D-galactose injection exerted recovering activities on acetylcholine depletion and brain injury/aging as well as cognitive deficit induced by D-galactose. The results indicate that SP preparations restore cognitive functions of facilitated brain aging model rats by increasing the release of acetylcholine, in addition to neuroprotective activity.

A Study on the Precipitation Behavior of $Al_2Ti$ Phase in $L1_0$-TiAl and $L1_2-(Al,Cr)_3Ti$ ($L1_0$-TiAl 및 $L1_2-(Al,Cr)_3Ti$ 중에 $Al_2Ti$상의 석출거동에 관한 연구)

  • Han, Chang-Suk
    • Journal of the Korean Society for Heat Treatment
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    • v.21 no.1
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    • pp.20-25
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    • 2008
  • Structural studies have been performed on precipitation hardening and microstructural variations found in Ti-Al-Cr ternary $L1_0$- and $L1_2$-phase alloys using transmission electron microscopy. Both the $L1_0$ and $L1_2$ phase alloys harden by aging at 973 K after solution annealing at higher temperatures. The amount of age hardening of the $L1_2$ phase alloy is larger than that of the $L1_0$ phase alloy. The phase separation between $L1_0$ and $L1_2$ phase have not been observed by aging at 973 K. But $Al_2Ti$ was formed in each matrix alloy during aging. The crystal structure of the $Al_2Ti$ phase is a $Ga_2Zr$ type in the $L1_0$ and a $Ga_2Hf$ type in the $L1_2$ phase, respectively. At the beginning of aging the fine coherent cuboidal $Al_2Ti$-phase are formed in the $L1_0$ phase. By further aging, two variants of $Al_2Ti$ precipitates grow along the two {110} habit planes. On the other hand, in the $L1_2$ phase, the $Al_2Ti$ phase forms on the {100} planes of the $L1_2$ matrix lattice. After prolonged aging the precipitates are rearranged along a preferential direction of the matrix lattice and form a domain consisting of only one variant. It is suggested that the precipitation of $Al_2Ti$ in each matrix alloy occurs to form a morphology which efficiently relaxes the elastic strain between precipitate and matrix lattices.

A Study on the Strain Rate and Temperature Dependence of Yield Stress of Al-Li Alloy (Al-Li합금의 항복응력에 대한 변형속도 및 온도의존성에 관한 연구)

  • Oh, Chang-Sup;Han, Chang-Suk
    • Journal of the Korean Society for Heat Treatment
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    • v.24 no.6
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    • pp.311-317
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    • 2011
  • The effect of strain rate on the yield stress of an Al-Li alloy has been investigated at temperatures between 77 and 523 K and over the strain rate range from $1.77{\times}10^{-4}s^{-1}$ to $1.77{\times}10^{-2}s^{-1}$. At testing temperatures below 373 K, the yield stress is almost independent of strain rate at any aging stage. At testing temperatures above 373 K, the yield stress increases linearly with the logarithm of strain rate, and the strain rate dependence increases with increasing testing temperature. The yield stresses of under-aged alloy at temperatures between 373 and 473 K at high strain rates are greater than the yield stress at 77 K. For the alloy under-aged or aged nearly to its peak strength, the temperature range within which the positive temperature dependence of yield stress appears expands to the higher temperature side with increasing strain rate. The strain rate dependence of the yield stress is slightly negative at this aging stage. The yield stress of the over-aged alloy decreases monotonically with decreasing strain rate and with increasing testing temperature above 373 K. The modulus normalized yield stress is nearly constant at testing temperatures below 373 K at any strain rate investigated. And, strength depends largely both on the aging conditions and on the testing temperature. The peak positions in strength vs. aging time curves shift to the side of shorter aging time with increasing testing temperature. For the specimens aged nearly to the peak strength, the positive temperature dependence of yield stress is observed in the temperature range. The shift of peak positions in the aging curves are explained in terms of the positive temperature dependence of cutting stress and the negative temperature dependence of by-passing stress.

Microstructure Evolution of Ti-6Al-4Fe-0.25Si through Aging Heat Treatment (시효처리에 따른 Ti-6Al-4Fe-0.25Si 합금의 미세조직 변화)

  • Song, Yong Hwan;Kang, Joo-Hee;Park, Chan Hee;Kim, Seong-Woong;Hyun, Yong-Taek;Kang, Nam Hyun;Yeom, Jong-Taek
    • Korean Journal of Metals and Materials
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    • v.50 no.7
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    • pp.477-485
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    • 2012
  • The effect of aging heat treatment on microstructure evolution of the Ti-6Al-4Fe-0.25Si alloy with an initial microstructure of an elongated alpha was investigated. Aging treatments of the samples were carried out at $550^{\circ}C$ for up to 100 hours. The microstructure of the 5 hours heat-treated sample consisted of alpha grains, beta matrix and some TiFe intermetallic compounds that were precipitated from the beta matrix. Increasing the aging time to 10 hours, most of the beta matrix was decomposed to very fine alpha grains (${\sim}0.5{\mu}m$) and TiFe, and thus the volume fraction of the beta matrix was significantly decreased. EBSD analysis revealed that newly formed tertiary-alpha-grains in the vicinity of TiFe had high angle boundaries with respect to the primary and secondary alpha grains. As a result of these phase transformations during aging, the fraction of the alpha/alpha grain boundary was increased while that of the alpha/beta phase boundary was decreased.