• 제목/요약/키워드: aging properties

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우레탄 도막 방수재의 열열화 특성 (Influence of Thermal Aging on the Properties of Polyurethane Coating of Waterproof.)

  • 김성래;신홍철;신주재;김영근
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2008년도 추계 학술발표회 제20권2호
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    • pp.931-934
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    • 2008
  • 폴리우레탄은 방수재로 널리 사용되며 구조물에 발생되는 균열 및 거동에 의해 항상 외력을 받고있을 뿐만 아니라 사용 환경에 따라 각종 환경열화 인자에 노출되어 있다. 환경 열화인자로서는 자외선, 오존, 열, 수분 등이 잘 알려져 있다. 그 중에서 모든 열화의 기본이 되는 열의 영향, 특히 고온에서의 영향이 중요하다. 따라서, 노출형인 우레탄 고무계 1류 도막 방수재의 경우는 80$^{\circ}C$에서, 비노출형의 경우는 70$^{\circ}$C에서 촉진 열열화 시험을 3주간 실시하였다. 결과는 방수재의 기본물성과 인장 강도 및 신장율 모두 저하되는 경향을 보였으며, 특히 온도 60$^{\circ}$C에서 측정할 경우 급격히 물성 저하가 발생되었다.

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메틸셀룰로오스에 의한 탈랍지의 강도보강처리 - 메틸셀룰오스 점도 및 도포율의 영향 - (Strengthening of De-waxed Paper by Methyl Cellulose (MC) and Its Preservability - Effect of Viscosity and Coating Ratio of MC -)

  • 최경화;정혜영;조병욱
    • 펄프종이기술
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    • 제47권6호
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    • pp.130-138
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    • 2015
  • This study was conducted to investigate the effect of the strengthening treatment of methyl cellulose (MC) on properties and aging characteristics of the dewaxed papers during humid heating aging. Beeswax-treated Hanji was dewaxed by the supercritical fluid extraction method, and subsequently the strengthening treatment was performed with MCs having three different viscosities. MC was first applied by dipping a dewaxed paper into a MC solution whose concentration was controlled from 0.5% to 1.5%. After the strengthened papers were artificially aged at $80^{\circ}C$ and 65% RH, the changes in optical and mechanical properties of the samples were evaluated. The results show that viscosity and especially pick-up of MC influenced the strengthening efficiency and aging characteristics of dewaxed paper. Strength was increased with the MC coating weight; in addition, strengthening with MC improved preservability of the dewaxed paper. The optimum conditions for the strengthening with MC was found to be the coating ratio of 4% with 1500 cP MC.

A356합금을 이용한 정밀주조 Turbo Charger Wheel의 기계적 특성에 미치는 열처리의 영향 (Effect of Heat Treatment on the Mechanical Properties of Investment Casting Turbo Charger Wheel using A356 Alloy)

  • 김상미;우기도;김지영;김상혁;박상훈;강황진;박찬성
    • 한국주조공학회지
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    • 제31권5호
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    • pp.262-266
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    • 2011
  • The aim of this study is to investigate aging behavior of A356 alloy for turbo charger part. The specimen was fabricated by investment casting. Solution heat treatment was performed at $525^{\circ}C$ for 8h and followed by aging treated at $160^{\circ}C$, $170^{\circ}C$ for 0.5~20h. And their microstructures and mechanical properties of the aged specimens were analyzed by scanning electron microscope and hardness tester, respectively. All the cast A356 alloy included eutectic Si particles. In the cast A356 alloy, eutectic Si phase mainly was formed along Chinese script phase. Vickers hardness of the cast was improved by aging treatment due to formation of ${\beta}$" phase and ${\beta}$' phase.

열 노화에 따른 NBR과 EPDM 가황물의 물성변화 및 노화수명 예측 (Effects of Thermal Aging on Properties and Life-time Prediction of NBR and EPDM Vulcanizates)

  • 우창수;최성신
    • Elastomers and Composites
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    • 제40권2호
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    • pp.119-127
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    • 2005
  • 고무부품의 신뢰성을 확보하기 위해서 고무재료의 물성파악과 수명평가는 매우 중요하다 하겠다. 본 연구에서는 냉장고 콤프레샤 모터에서 발생되는 소음 및 진동 제어 목적으로 고무마운트에 사용되는 고무재료인 NBR과 EPDM에 대해 상온과 $70^{\circ}C,\;85^{\circ}C,\;100^{\circ}C$에서 75일 동안 노화시킨 상태에서 단축 인장과 이축 인장으로 물성시험을 수행하여 가교밀도, 100% 모듈러스 변화와 응력-변형률 관계를 파악하였다. 또한, 고무소재의 노화수명을 예측하기 위해 가속열 노화시험을 수행하여 시간-온도 환산식인 아레니우스 관계식을 구하였다.

점액질에 따른 한지 sheet의 열화 거동 (Ageing behavior of Hanji sheet by mucilage)

  • 이민형;김강재;엄태진
    • 한국펄프종이공학회:학술대회논문집
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    • 한국펄프종이공학회 2011년도 춘계학술발표회 논문집
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    • pp.271-277
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    • 2011
  • Hanji(Korean traditional paper) is made from bark of paper mulberry(Broussonetia kazinoki). For a long time, Hanji has been used in various fields, such as paintings, printing paper, as specialty paper. The utilization of Hanji will become more and more diverse. One of the characteristic properties of Hanji is a long life time comparing to western paper. The mucilage which must be used in Hanji manufacturing should effect the conservation properties of Hanji. The effectiveness of the mucilage in aging of Hanji was evaluated in this paper. Strength properties of thermal aged Hanji made with synthetic mucilage decreased more slowly than those of Hanji made with natural mucilage. As prolonged aging time, all Hanji made mucilage increased oxidation index. But, Hanji made with PAM was most stable in oxidation of cellulose.

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Sn-Bi-Ag계 땜납과 Cu기판과의 젖음성, 계면 반응 및 기계적 성질에 관한 연구 (A Study on Wetting, Interfacial Reaction and Mechanical Properties between Sn-Bi-Ag System Solders and Cu Substrate)

  • 서윤종;이경구;이도재
    • 한국주조공학회지
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    • 제17권3호
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    • pp.245-251
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    • 1997
  • Solderability, interfacial reaction and mechanical properties of joint between Sn-Bi-Ag base solder and Cu-substrate were studied. Solders were subjected to aging treatments to see the change of mechanical properties for up to 30 days at $100^{\circ}C$, and then also examined the changes of microstructure and morphology of interfacial compound. Sn-Bi-Ag base solder showed about double tensile strength comparing to Pb-Sn eutectic solder. Addition of 0.7wt%Al in the Sn-Bi-Ag alloy increase spread area on Cu substrate under R-flux and helps to reduce the growth of intermetallic compound during heat-treatment. According to the aging experiments of Cu/solder joint, interfacial intermetallic compound layer was exhibited a parabolic growth to aging time. The result of EDS, it is supposed that the soldered interfacial zone was composed of $Cu_6Sn_5$.

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The Effect of Hygrothermal Aging on the Properties of Epoxy Resin

  • Wang, Youyuan;Liu, Yu;Xiao, Kun;Wang, Can;Zhang, Zhanxi
    • Journal of Electrical Engineering and Technology
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    • 제13권2호
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    • pp.892-901
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    • 2018
  • Because of excellent electrical properties, epoxy resin is widely used in packaging and casting power equipment. Moisture and temperature in the environment are inclined to seriously affect the insulation tolerance of epoxy resin. This work focuses on the aging characteristics of epoxy resin in hygrothermal environment. Scanning electron microscopy images show that there are micro-crack, micro-slit and holes inside aged samples. The moisture absorption process undergoes three equilibrium stages and it does not follow the Fick's second law. Observing the change of hydrogen bonds in the infrared spectra of the dried samples, it is found that chemically moisture absorption immerges when the physical moisture absorption entered the third equilibrium stage. By Debye equation to fit the imaginary part of the dielectric constant, it is concluded that the uniformity of water molecule has a great influence on the electrical conductivity loss. Furthermore, the polarization loss can be more easily affected by water molecules than small free molecules. After the aged samples being dried, their real and imaginary part of the dielectric constant descend, but their original electrical properties cannot completely restored. After chemical moisture absorption appears inside the material, the residual space charges increase significantly and the charge dissipation rate slow down obviously.

냉장고 압축기용 고무마운트 수명예측에 관한 연구 (A Study on the Lifetime Prediction of Rubber Mount for Refrigerator Component)

  • 우창수;박현성
    • 한국신뢰성학회지:신뢰성응용연구
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    • 제6권2호
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    • pp.135-150
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    • 2006
  • Rubber material properties and lifetime evaluation are very important in design procedure to assure the safety and reliability of the rubber components. This paper discusses the failure mechanism and material tests were carried out to predict the useful lifetime of NBR and EPDM for compression motor, which is used in refrigerator component. The heat-aging process leads not only to mechanical properties change but also to chemical structure change so called degradation. In order to investigate the aging effects on the material properties, the accelerated test were carried out. The stress-strain curves were plotted from the results of the tensile test for virgin and heat-aged rubber specimens. The rubber specimens were heat-aged in an oven at the temperature ranging from $70^{\circ}C\;to\;100^{\circ}C$ for a period ranging from 1 to 180 days. Compression set results changes as the threshold are used for assessment of the useful life and time to threshold value were plotted against reciprocal of absolute temperature to give the Arrhenius plot. By using the compression set test, several useful lifetime prediction equations for rubber material were proposed.

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Application of Electron-Beam Irradiation Combined with Aging for Improvement of Microbiological and Physicochemical Quality of Beef Loin

  • Yim, Dong-Gyun;Jo, Cheorun;Kim, Hyun Cheol;Seo, Kang Seok;Nam, Ki-Chang
    • 한국축산식품학회지
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    • 제36권2호
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    • pp.215-222
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    • 2016
  • The combined effects of irradiation and aging temperature on the microbial and chemical quality of beef loin were investigated. The samples were vacuum-packaged, irradiated at 0 or 2 kGy using electron-beam (EB), and stored for 10 d at different aging temperatures (2, 14, or 25℃). The microbial growth, shear values, meat color, and nucleotide-related flavor compounds of the samples were analyzed. The irradiation effect on inactivation of foodborne pathogens was also investigated. The population of Listeria monocytogenes and Escherhia coli O157:H7 inoculated in beef samples decreased in proportion to the irradiation dose. Irradiation reduced the total aerobic bacteria (TAB) over the storage, but higher aging temperature increased the TBA. Thus TAB increased sharply in non-irradiated and high temperature-aged (14, 25℃) beef samples after 5 d. With increasing aging temperature and aging time, shear force values decreased. Lipid oxidation could be reduced by short aging time at low aging temperature. The color a* values of the irradiated beef were lower than those of the non-irradiated throughout the aging period. As aging period and temperature increased, IMP decreased and hypoxanthine increased. Considering microbial and physicochemical properties, irradiation can be used for raw beef to be aged at relatively high temperature to shorten aging time and cost.

원료콩의 파종시기와 산지에 따른 재래식 간장의 품질 특성 비교 (Comparisons of the Physicochemical Characteristics of Korean Traditional Soy Sauce with Varying Soybean Seeding Periods and Regions of Production)

  • 강선희;이슬;고종민;황인경
    • 한국식품영양학회지
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    • 제24권4호
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    • pp.761-769
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    • 2011
  • The objective of this study was to investigate the physicochemical properties of Korean traditional soy sauces made with soybeans sown in different producing regions(Hadong, Paju) and in different seeding periods(late-May, mid-June, late-June). The total acidity, salt content, chromaticity, browning, amino nitrogen content and the reducing sugar content of the soy sauce samples were compared. It was found that the total acidity level and the amino nitrogen contents were significantly lower in the soy sauce made with mid-June soybeans, and that these properties increased as the sauce aged. Salt content increased with the aging period regardless of the region of production. The reducing sugar content of Paju soy sauce was the highest in late -June, and for the Hadong region, highest in late-May. The sauce made with Hadong soy beans showed an increase in reducing sugar content positively correlated with the aging period. Reducing sugar content in the samples of Paju soy sauce decreased up to 60 days of aging, but increased after this point. In Paju soy sauce, the brightness(L value) was significantly higher in mid-June, and the Hadong variant it was higher in late -May. The yellowness(b value) at the beginning of the aging process was high in late -June for Hadong soy sauce, but overall it was higher in the mid-June period. The more matured soy sauce samples were darker and showed both higher a and b values. The browning was the lowest in the mid -June regardless of the regions and it increased with the aging period regardless of the production regions. The salt, amino nitrogen contents, browning and yellowness showed significant correlations among the samples. In conclusion, the seeding period of soy beans may affect the characteristics of produced soy sauce alongside the aging conditions.