• Proceedings of the Korean Society For Composite Materials Conference
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• 2004.04a
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• pp.232-236
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• 2004

The fracture characteristics of unidirectional composite single-lap bonded joints were investigated experimentally and numerically. The effects of bonding method, surface roughness, bondline thickness and the existence of fillet on the failure characteristics and strength of bonded single-lap joints were evaluated experimentally. The failure process, failure mode and the behavior of load-displacement curve was apparently different according to bonding method. The failure load of the specimen co-cured without adhesive was definitely superior to other types of specimens but the specimens co-cured with adhesive film had a less strength than secondary bonded specimens. In the secondary bonded specimens, the lower value of surface roughness and existence of fillet improved the strength of specimens. The strain energy release rates calculated by geometric nonlinear finite element analyses and Virtual Crack Closure Technique for the secondary bonded specimens considering the three types of initial cracks - comer crack, edge crack and delamination crack - were consistent with the test results.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2022.04a
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• pp.25-26
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• 2022

In this study, glued laminated timber were manufactured by different types of adhesives for larch and spruce. Adhesives used to manufacture glued laminated timber include resorcinol resin, phenol resorcinol resin, melamine resin, and polyurethane. The char thickness and char rate according to the type of adhesive forglued laminated timber were analyzed. Melamine, resorcinol, and polyurethane showed excellent fire resistance performance in that order.

• Steel and Composite Structures
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• v.49 no.3
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• pp.271-280
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• 2023

In this study, the three-dimensional finite element method is used to analyze the behavior of corner cracks in finite-thickness plates repaired with a composite patch. The normalized stress intensity factor at the crack front is used as fracture criterion. Comparison of stress intensity factor values at the internal and external positions of repaired quarter-elliptical corner crack was done, for three repair techniques. The influence of mechanical and geometrical properties of the adhesive layer and the composite patch on the variation of the stress intensity factor (SIF) at the crack-front was highlighted. The obtained results show that the application of double patch leads to a remarkable reduction of SIF at the crack front, compared to facial and lateral repairs.

• Journal of Dental Rehabilitation and Applied Science
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• v.18 no.3
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• pp.205-215
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• 2002

This study investigated the compressive fracture strength of Targis ceromer crown by the difference of occlusal thickness on a maxillary first premolar. Control group was a castable IPS-Empress all-ceramic crown with occlusal thickness of 1.5 mm constructed by layered technique. Experimental groups were Targis crowns having different occlusal thicknesses of 1.0 mm, 1.5 mm, 2.0 mm, 2.5 mm, respectively. The classification of Targis group is T10, T15, T20, T25 and T15N (for no-thermocycling and occlusal thickness of 1.5mm). Ten samples were tested per each group. Except occlusal thickness, all dimension of metal die is same with axial inclination of $10^{\circ}$and marginal width 0.8mm chamfer. All crowns were cemented with Panavia F and thermocycled 1,000 times between $5^{\circ}$ and $55^{\circ}$ water bath with 10 sec dwelling time and 10 sec resting time. The compressive fracture strength was measured by universal testing machine. The results were as follows : 1. Fracture strength was increased as the occlusal thickness increased : compressive fracture strength of Group T10, T15, T20, T25 was $66.65{\pm}4.88kgf$, $75.04{\pm}3.01kgf$, $87.07{\pm}7.06kgf$ and $105.03{\pm}10.56kgf$, respectively. 2. When comparing material, Targis crown had higher fracture strength than IPS-Empress crown : the mean compressive strength of group T15 was $75.04{\pm}3.01kgf$ and the value of group Control was $37.66{\pm}4.28kgf$. 3. Fracture strength was decreased by thermocycling : the compressive fracture strength of T15 was $75.04{\pm}3.01kgf$, which is lower than $90.69{\pm}6.88kgf$ of group T15N. 4. The fracture line of crowns began at the loading point and extended along long axis of tooth. IPS-Empress showed adhesive failure pattern whereas Targis had adhesive and cohesive failure. In the SEM view, stress was distributed radially from loading point and the crack line was more prominent on Targis crown.

• Proceedings of the Korea Concrete Institute Conference
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• 2004.05a
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• pp.794-797
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• 2004

In this study, tensile adhesive strength(TAS) test was carreid out for evaluated the effects of temperature conditions (-20, -10, 0, 5, 10, 20, 30, $40^{\circ}C$) on the tensile adhesive characteristics about 4 type waterproofing membranes which were commercially used in bridge decks. And, failure appeariences of waterproofing systems in each temperature after TAS test were observed the sawing surfaces of waterproofing systems for whether or not damaged of waterproofing membranes. Also, correction coefficient of TAS with temperature were calculated using 4 type waterproofing membrane. It could be shown that the higher TAS and shear adhesive strength, the lower temperature, regardless of the type of waterproofing membrane. Temperature sensibility of TAS was especially remarkable in epoxy membrane. Failure type was occurred the ductile failure in $30^{\circ}C\;and\;40^{\circ}C$. From these results, it was shown that if ambient temperature above $30^{\circ}C$ maintains for a long time, waterproofing membrane will be deformed by softening. Otherwise, waterproofing membrane in temperature below $20^{\circ}C$ shown that occurred the brittle failure. From the results of visual observation of cutting surface for specimen, the thin waterproofing membranes shown indented by hot aggregate of the asphalt mixtures. Therefore, it could be known that the specification of waterproofing membrane thickness is necessary by waterproofing membrane type. As temperature change varied with pavement depth, the interface temperature was more important than ambient temperature in TAS test. Now, TAS test results were limited only in $-10^{\circ}C\;and\;20^{\circ}C$ temperature, but correction coefficient of TAS by ambient temperature could be used as a solution to deal with this problem.

• Journal of the Korean Society for Nondestructive Testing
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• v.22 no.5
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• pp.508-515
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• 2002

The characterization of adhesive property in multi-layer materials has been hot issue for a long time. In order to evaluate adhesive properties, we constructed fully automated system for the backward radiation of leaky Lamb wave. The backward radiation profiles were obtained for the bare steel plate and plates with rubber-loading. The rf waveforms and frequency spectra of backward radiation show the characteristics of involved leaky Lamb wave modes. As the thickness of rubber-loading increased, the amplitude of profile at the incident angle of $13.4^{\circ}$ exponentially decreased. Scanning the incident position over the partially rubber-loaded specimen shows good agreement with the actual rubber-loading. The backward radiation of leaky Lamb wave has great potential to evaluate the adhesive condition as well as material properties of plates.

• Composites Research
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• v.33 no.2
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• pp.55-60
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• 2020

A study on the heating behavior and adhesion property of structural epoxy adhesive through induction heating have been conducted. An adhesive for induction heating was manufactured through mixing with nano and micro sized Fe₃O₄. From the results, it was observed that induction heating is less affected by adherend (GFRP) thickness than oven heating. The heating rate of Fe₃O₄ embedded epoxy adhesive using induction heating much higher than that of oven curing process and it is more appreciable when the contents of Fe₃O₄ increased. Furthermore, adhesion strength increased with increase of Fe₃O₄ particle contents.

• Resources Recycling
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• v.32 no.6
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• pp.3-9
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• 2023

Separation of LED packages from PCBs and analysis of the adhesive components was conducted to enhance the recycling potential of LED modules. LED package was separated from PCBs using heat treatment under optimal conditions: temperature of above 250 ℃ and time of 20 minutes. The separation equipment can be established using a hot air injector with controlling the rotational speed of the internal screw. The separation efficiency of each type of substrate (aluminum and glass fiber) was investigated with the thickness range of the adhesive materials (0.25-0.30 and 0.30-0.35 mm). Under the optimal conditions, the efficiency can reach to 97.5% for both types of substrates with adhesive materials of thickness 0.25~0.30mm. Characterization of the residual adhesive substances from the separated LED package and PCB using microwave digestion and ICP analysis showed that the residue contained of 95% of Sn, less than 5% of Cu and Ag.

• Restorative Dentistry and Endodontics
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• v.27 no.1
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• pp.34-43
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• 2002

The purpose of this study was to compare microleakage and marginal hybrid layer in class V restorations using two one-bottle adhesives and one self-etching adhesive. Class V cavity preparations with occlusal margins in enamel and gingival margins in dentin were pre-pared on buccal and lingual surfaces of 30 extracted human molar teeth. Prepared teeth were randomly divided into three treatment groups (n=30) and restored with three adhesives and composites: Single Bond/Filtek Z-250 (Group 1), Prime&BondNT/Esthet.X (Group 2), UniFil Bond/UniFil F (Group 3). For microleakage, samples were stored in room temperature water for 24 hours, thermocycled stained with 2% methylene blue dye, sectioned into halves, scored and analysed using Mann-whitney test and Wilcoxon signed rank sum test. For marginal hybrid layer, samples were sectioned into halves, treated with 10% phosphoric acid for 5 seconds, stored in 5% NaOCL solution for 24 hours, dried and gold coated. Occlusal and gingival margins of each sample were inspected under SEM. The results of this study were as follows ; 1. Microleakage at the occlusal margins was not evident in group 1 and group 2, but it showed in group 3 (p<0.05). 2. Microleakage in group 1 and group 3 was significantly lower than in group 2 at gingival margins (p<0.05). 3. Microleakage at gingival margins was greater than at occlusal margins in group 1 and group 2, but microleakage at occlusal margins was greater than at gingival margins in group 3 (p<0.05). 4. In group 1 and group 2, no gaps at occlusal margins showed. But gaps showed in group 3. Occlusal margins were free from a hybrid layer in all groups 5. The thickness of the marginal hybrid layers was 2.5~5 $\mu\textrm{m}$ thick in group 5 $\mu\textrm{m}$ thick in group 2 and 1.5 $\mu\textrm{m}$ thick in group 3. 6 There was no corelation between microleakage and thickness of marginal hybrid layer. In coclusion, the effect of dentin adhesives on microleakge in class V composite restorations was excellent when one-bottle adhesives were applied on enamel margin, and it was good when a self-etching adhesive was applied on dentinal margin. There was no corelation between microleakage and thickness of marginal hybrid layer.

• Restorative Dentistry and Endodontics
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• v.33 no.1
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• pp.45-53
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• 2008

The purpose of this study was to determine the effects on the elastic moduli of the adhesive and the hybrid layer from thermocycling. Twenty one human molars were used to create flat dentin surfaces. Each specimen was bonded with a light-cured composite using one of three commercial adhesives (OptiBond FL [OP], Clearfil SE Bond [CL], and Xeno III [XE]). These were sectioned into two halves and subsequently cut to yield 2-mm thickness specimens; one specimen for immediate bonding test without thermocycling and the other subjected to 10,000 times of thermocycling. Nanoindentation test was performed to measure the modulus of elasticity of the adhesive and the hybrid layer, respectively, using an atomic force microscope. After thermocycling, XE showed a significant decrease of the modulus in the adhesive layer (p < 0.05). Adhesives containing hydrophilic monomers are prone to hydrolytic degradation. It may result in the reduced modulus of elasticity, which leads to the mechanically weakened bonding interface.