• Title/Summary/Keyword: adhesive resistance

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Effect of the type of resin cement on the fracture resistance of chairside CAD-CAM materials after aging

  • Laura Vitoria Rizzatto;Daniel Meneghetti;Marielle Di Domenico;Julia Cadorin Facenda;Katia Raquel Weber;Pedro Henrique Corazza;Marcia Borba
    • The Journal of Advanced Prosthodontics
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    • v.15 no.3
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    • pp.136-144
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    • 2023
  • PURPOSE. The study objective was to evaluate the influence of the type of resin cement on the flexural strength and load to fracture of two chairside CADCAM materials after aging. MATERIALS AND METHODS. A polymer-infiltrated ceramic network (PICN) and a nanoceramic resin (RNC) were used to produce the specimens. Two types of dual-cure resin cements, a self-adhesive and a universal, were investigated. Bilayer specimens were produced (n = 10) and aged for 6 months in a humid environment before the biaxial flexural strength test (σf). Bonded specimens were subjected to a mechanical aging protocol (50 N, 2 Hz, 37℃ water, 500,000 cycles) before the compressive load test (Lf). σf and Lf data were analyzed using two-way ANOVA and Tukey tests (α = .05). Chi-square test was used to analyze the relationship between failure mode and experimental group (α = .05). RESULTS. The type of resin cement and the interaction between factors had no effect on the σf and Lf of the specimens, while the type of restorative material was significant. RNC had higher σf and Lf than PICN. There was a significant association among the type of cracks identified for specimens tested in Lf and the restorative material. CONCLUSION. The type of resin cement had no effect on the flexural strength and load to fracture of the two investigated CAD-CAM chairside materials after aging.

Effect of Silica Particle Size and Aging Time on the Improvement of Mechanical Properties of Geopolymer-Fiber Composites (실리카의 입자 크기와 Aging 시간이 지오폴리머 섬유 복합체의 기계적 물성 향상에 미치는 효과)

  • Yoonjoo Lee;Seokhun Jang;Minkyeong Oh;Dong-Gen Shin;Doo Hyun Choi;Jieun Lee;Chang-Bin Oh
    • Korean Journal of Materials Research
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    • v.34 no.3
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    • pp.175-183
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    • 2024
  • Geopolymer, also known as alkali aluminum silicate, is used as a substitute for Portland cement, and it is also used as a binder because of its good adhesive properties and heat resistance. Since Davidovits developed Geopolymer matrix composites (GMCs) based on the binder properties of geopolymer, they have been utilized as flame exhaust ducts and aircraft fire protection materials. Geopolymer structures are formed through hydrolysis and dehydration reactions, and their physical properties can be influenced by reaction conditions such as concentration, reaction time, and temperature. The aim of this study is to examine the effects of silica size and aging time on the mechanical properties of composites. Commercial water glass and kaolin were used to synthesize geopolymers, and two types of silica powder were added to increase the silicon content. Using carbon fiber mats, a fiber-reinforced composite material was fabricated using the hand lay-up method. Spectroscopy was used to confirm polymerization, aging effects, and heat treatment, and composite materials were used to measure flexural strength. As a result, it was confirmed that the longer time aging and use of nano-sized silica particles were helpful in improving the mechanical properties of the geopolymer matrix composite.

An Experimental Evaluation on Performance of Surface Protector for Concrete Structures (콘크리트 구조물 표면 보호재의 성능에 대한 실험적 평가)

  • Nam, Yong-Hyuk;Chung, Young-Jun;Jang, Suk-Hwan;An, Young-Ki
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.10 no.5
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    • pp.157-163
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    • 2006
  • This study is on the evaluation of double surface protection method using water repellent primer and final top coat to protect concrete. Water repellent agent has been applied on the final top coat to protect concrete. However, to make up for the weakness to the ultraviolet of the water repellent, the work procedure of these protectors is done vice versa. This combination of protectors was compared with existing ones in this study. Even though the final top coat was applied on the water repellent primer, its adhesive strength met to KS F 4936-' 03 with other protectors used in this study. All surface protectors used in this study were excellent in protecting concrete. Especially, in case of applying with final top coat in conjunction with water repellent primer, the resistance against chloride ion penetration and neutralization by $CO_2$ was more efficient than other surface protectors used in this study under this given condition.

Moment Resistance Performance Evaluation of Larch Glulam Joints using GFRP-reinforced Laminated Plate and GFRP Rod (GFRP 보강적층판 및 GFRP rod를 이용한 낙엽송 집성재 접합부의 모멘트저항 성능평가)

  • Jung, Hong-Ju;Song, Yo-Jin;Lee, In-Hwan;Hong, Soon-Il
    • Journal of the Korean Wood Science and Technology
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    • v.44 no.1
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    • pp.40-47
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    • 2016
  • Instead of metal connector generally used on the structural glued laminated timber rahmen joints, the GFRP reinforced laminated plates combining veneer and GFRP (Glass Fiber Reinforced Plastic) and bonded type GFRP rod were used as the connectors. As a result of moment resistance performance evaluation on the joint part applied with these connectors, the yield moment of specimen using the GFRP reinforced laminated plates and GFRP rod pin was measured 4 % lower in comparison to the specimen (Type-1) using the metal connectors, but the initial rotational stiffness was measured 29% higher. Also, the yield moment and rotational stiffness of the specimen using the GFRP-reinforced laminated plates and wood (Eucalyptus marginata) pin showed were measured 11% and 56% higher in comparison to the Type-1 specimen, showing the best performance. It was also confirmed through the failure shape and perfect elasto-plasticity analysis that it showed ductility behavior, not brittle fracture, from the shear resisting force by the pin and the bonding strength increased and the unification of member was carried out. On the other hand, in case of the specimen bonded with GFRP rod, it was impossible to measure the bonding performance or it was measured very low due to poor bonding.

Embedment Properties of Reflective Beads for Thermoplastic Road Markings (열가소성 차선도장에서 반사유리알의 함침특성)

  • Hong, In Kwon;Lee, Chang Geun;Lee, Seung Bum
    • Applied Chemistry for Engineering
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    • v.26 no.2
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    • pp.199-204
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    • 2015
  • Thermoplastic road markings are one of the most widely used road markings in the world. However, the durability of domestic road markings is relatively shorter than that of the global average of, approximately, three years. To overcome it, the conventional thermoplastic road markings were prepared by adding polyolefin and oxidized PE wax to conventional petroleum resin. In addition, the melting viscosity was designed below 500 cP at $220^{\circ}C$ as well as the optimum viscosity for spray painting, and embedding ratio of glass beads were controlled about 50~60% by spraying in an interval of 1 second. Also the glass bead adhesive ratio was improved by reducing the amount of $CaCO_3$ below 40 wt%. The retroreflectivity was tested under four different conditions to evaluate the abrasion resistance of thermoplastic road markings. The retroreflectivity coefficient satisfied the international standard ($150mcd{\cdot}m^{-2}{\cdot}lux^{-1}$) in this study, and TPRM-7 was determined as an optimal ratio.

Joint Displacement Resistance Evaluation of Waterproofing Material in Railroad Bridge Deck (철도교량상판 방수재료 선정을 위한 균열거동저항 성능평가)

  • Bae, Young-Min;Oh, Dong-Cheon;Park, Yong-Gul
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.11
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    • pp.683-692
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    • 2020
  • A joint displacement resistance evaluation method for selecting waterproofing materials in railway bridge decks is proposed. The displacement range for an evaluation is determined by finite element method (FEM) analysis of a load case based on an existing high-speed PSC Girder Box railroad bridge structure. The FEM analysis results were used to calculate the minimum joint displacement range to be applied during testing (approximately 1.5 mm). For the evaluation, four commonly used waterproofing membrane types, cementitious slurry coating (CSC), polyurethane coating system (PCS), self-adhesive asphalt sheet (SAS), and composite asphalt sheet (CAS), were tested, with five specimens of each membrane type. The joint displacement width range conditions, including the minimum displacement range obtained from FEM analysis, were set to be the incrementing interval, from 1.5, 3.0, 4.5, and 6.0 mm. The proposal for the evaluation criteria and the specimen test results demonstrated how the evaluation method is important for the sustainability of high-speed railway bridges.

A Study on the Performance Improvement of ta-C Thin Films Coating on Tungsten Carbide(WC) Surface for Aspherical Glass Lens by FCVA Method Compared with Ir-Re coating (Ir-RE 코팅 대비 자장여과필터방식을 이용한 비구면 유리 렌즈용 초경합금(WC)표면의 ta-C 박막 코팅 성능 개선 연구)

  • Jung, Kyung-Seo;Kim, Seung-Hee
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.20 no.12
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    • pp.27-36
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    • 2019
  • The demand for a low dispersion lens with a small refractive index and a high refractive index is increasing, and accordingly, there is an increasing need for a releasable protective film with high heat resistance and abrasion resistance. On the other hand, the optical industry has not yet established a clear standard for the manufacturing process and quality standards for mold-releasing protective films used in aspheric glass lens molding. Optical lens manufacturers treat this technology as proprietary information. In this study, an experiment was conducted regarding the optimization of ion etching, magnetron, and arc current at each source and filter part, and bias voltage in FCVA (filtered cathode vacuum arc)-based Ta-C thin film coatings. This study found that compared to iridium-rhenium alloy thin film sputtering products, the coating conditions were improved by approximately 50%, 20%, and 40% in terms of thickness, hardness, and adhesive strength of the film, respectively. The thin-film coating process proposed in this study is expected to contribute significantly to the development and utilization of glass lenses, which will help enhance the minimum mechanical properties and quality of the mold-release thin film layer required for glass mold surface forming technology.

Mechanical Properties and Wear Behaviour of $Al/SiC/Al_{2}O_{3}$ Composite Materials ($Al/SiC/Al_{2}O_{3}$복합재료의 기계적 성질 및 마멸특성)

  • 임흥준;김영한;한경섭
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.17 no.10
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    • pp.2498-2508
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    • 1993
  • $Al/SiC/Al_{2}O_{3}$ hybrid composites are fabricated by squeeze infiltration method. From the misconstructive of $Al/SiC/Al_{2}O_{3}$ hybrid composites fabricated by squeeze infiltration method, uniform distribution of reinforcements and good bondings are found. Hardness value of $Al/SiC/Al_{2}O_{3}$ hybrid composites increases linearly with the volume fraction of reinforcement because SiC whisker and $Al_{2}$O$_{3}$ fiber have an outstanding hardness. Optimal aging conditions are obtained by examining the hardness of $Al/SiC/Al_{2}O_{3}$ hybrid composites with different aging time. Tensile properties such as Young's modulus and ultimate tensile strength are improved up to 30% and 40% by the addition of reinforcements, respectively. Failure mode of $Al/SiC/Al_{2}O_{3}$ hybrid composites is ductile on microstructural level. Through the abrasive wear test and wear surface analysis, wear behaviour and mechanism of 6061 aluminum and $Al/SiC/Al_{2}O_{3}$ hybrid composites are characterized under various testing conditions. The addition of SiC whisker to $Al/SiC/Al_{2}O_{3}$ composites gives rise to improvement of the wear resistance. The wear resistance of $Al/SiC/Al_{2}O_{3}$ hybrid composites is superior to that of Al/SiC composites. The wear mechanism of aluminum alloy is mainly abrasive wear at low speed range and adhesive and melt wear at high speed range. In contrast, that of $Al/SiC/Al_{2}O_{3}$ hybrid composites is abrasive wear at all speed range, but severe wear when counter material is stainless steel. As the testing temperature increases, wear loss of aluminum alloy decreases because the matrix is getting more ductile, but that of $Al/SiC/Al_{2}O_{3}$ hybrid composites is hardly varied. Oil lubricant is more effective to reduce the wear loss of aluminum alloy and $Al/SiC/Al_{2}O_{3}$ hybrid composites at high speed range.

Microbiological and chemical properties of sourdough fermented with probiotic lactic acid bacteria (프로바이오틱 유산균으로 제조한 사워도우의 미생물학적 및 이화학적 특성)

  • Lim, Eun-Seo
    • Korean Journal of Microbiology
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    • v.52 no.1
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    • pp.84-97
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    • 2016
  • Isolates from Korean fermented soybean paste were identified as Enterococcus faecium SBP12, Pediococcus halophilus SBP20, Lactobacillus fermentum SBP33, Leuconostoc mesenteroides SBP37, Pediococcus pentosaceus SBP41, Lactobacillus brevis SBP49, Lactobacillus acidophilus SBP55, and Enterococcus faecalis SBP58 according to conventional morphological and biochemical characteristics, carbohydrate fermentation profiling, and 16S rRNA sequence comparison. Strain SBP20, SBP33, SBP49, and SBP55 showed very resistance to simulated gastric and intestinal juices with final populations exceeding 6 log CFU/ml, whereas cells of SBP12 and SBP58 after exposure to low pH were dramatically decreased within 2 h. Among 4 strains having good tolerance to gastrointestinal conditions, the high adhesive ability to HT-29 cells, antibiotic resistance, and antimicrobial activity against food-borne pathogens Bacillus cereus ATCC 11778 and Staphylococcus aureus ATCC 6538 were observed with SBP49 and SBP55, therefore, these two strains were confirmed as putative probiotic candidates. There was no significant difference between the sourdoughs fermented with SBP49 and SBP55 with respect to the values of pH, total titratable acidity, and viable cell count. During sourdough fermentation, SBP49 strain produced significantly greater amounts of lactic acid than SBP55 strain, which secreted large quantities of hydrogen peroxide. SBP49 and SBP55 strains producing the antimicrobial substances such as lactic acid, hydrogen peroxide, and bacteriocin effectively inhibited B. cereus and S. aureus inoculated in the sourdough.

A Study on the Eco-Friendly Durable Pre-Painting for Concrete Structure (콘크리트 구조물의 친환경 내구성 도장에 관한 기초 연구)

  • Jo, Byung Wan;Choi, Ji Sun;Lee, Seong Won
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.17 no.2
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    • pp.110-116
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    • 2013
  • A concrete structure has become bigger and higher because of development of construction technology and a change in construction environment. Also it tends to focus on repairing, reinforcement and exterior in harmony with environment for structure maintenance and performance improvement. The research is about eco friendly durable painting applicable to concrete structure using civil and architecture. it purpose to improve external beauties and durable problems due to flexibility by variation of temperature, adhesion of exterior wall, crack and delamination in existing organic and mineral painting. For those problems, we made a eco friendly pre-paint that is made with preliminary treatment mixture as a highly enriched waterproof agent and adhesive increasing agent in preprocessing mixture. Then we performed an experiment on durability of prevention neutralization of concrete, durability abrasion, hiding power, adhesion, temperature resistance and resistance to chemical attack. The result of an experiment shows that hiding power is over 0.96 in standard test, durability abrasion test got higher value 1mg than water paint 75mg and tensile strength is 6 times higher than standard waterproof specification.