• 비파괴검사학회지
• /
• 제22권5호
• /
• pp.508-515
• /
• 2002

다층재료의 접합특성 평가는 오랫동안 많은 논의가 있어 왔는데, 본 연구에서는 후방복사 초음파 기술을 사용하여 여러 충이 있는 재료의 특성을 평가하기 위한 자동화된 시스템을 개발하고 스틸 판재와 고무가 접합된 스틸 판재의 후방복사 프로파일을 획득하였다. 후방복사의 rf 파형과 주파수 스펙트럼은 리키 램파 모드들의 특성을 나타내고 있다. 집합된 고무 두께의 증가에 따라 입사각이 $13.4^{\circ}$일 때의 후방복사 진폭이 지수적으로 감소함을 보이며 부분적으로 고무가 접합된 시편에서 선택되어진 입사각으로 입사위치를 바꾸어가며 스캐닝한 결과 정확하게 고무가 접합되어 있지 않은 지역을 결정할 수 있었다. 리키 램파에 의한 후방복사는 판재의 물성은 물론이고 다층 재료의 접합특성 평가에 활용할 수 있다.

• 대한토목학회논문집
• /
• 제30권3A호
• /
• pp.221-228
• /
• 2010

탄소섬유시트 보강공법은 열화 손상된 콘크리트 구조물의 보강에 가장 많이 사용되는 보강공법 중 하나이다. 탄소섬유시트 보강공법은 에폭시접착제를 사용하여 탄소섬유시트를 콘크리트의 외부에 부착하는 보강공법으로 탄소섬유시트에 의한 휨보강이 에폭시 접착 경계면을 통하여 콘크리트로 전달된다. 따라서 사용기간이 경과함에 따라 에폭시 접착 경계면에 발생하는 크리프 등의 시간의존적 거동은 보강효과를 감소시키는 요인이 된다. 본 연구에서는 경계면에서 발생하는 크리프 영향을 해석하기 위하여 콘크리트의 크리프 거동에 대한 기존의 연구들을 고찰하고, 이를 바탕으로 에폭시 접착 경계면의 크리프 영향을 예측할 수 있는 이론적인 연구를 수행하였다. 제안된 유한요소해석기법은 기존의 콘크리트 크리프 거동 분석을 위해 사용되던 유변모델을 에폭시 접착 경계면에 적용한 것으로 기존 실험결과와 비교를 통하여 타당성을 검증하였다. 또한, 제안된 유한요소해석을 통하여 탄소섬유시트로 보강된 콘크리트 구조물의 시간의존적 거동에 경계면 재료의 크리프 영향을 반드시 고려해야 한다는 것을 입증하였다.

• Journal of Welding and Joining
• /
• 제33권4호
• /
• pp.44-49
• /
• 2015

The structural epoxy adhesive used in car body assembly needs the highest level of joint mechanical strength under lap shear, T-peel and impact peel conditions. In this study, the effect of nano functionalized block copolymer addition on the impact peel strength of epoxy adhesive was investigated. DSC analysis showed that the addition of nano functionalized block copolymer did not affect the curing reaction of epoxy adhesive. From single lap shear test, it was found out that the addition of nano functionalized block copolymer slightly decreased the cohesive strength of cured adhesive layer. The addition of nano functionalized block copolymer showed beneficial effect on T-peel strength by changing the adhesive failure mode to the mixed mode. However, the addition of nano functionalized block copolymer just decreased the room temperature impact peel strength. It was considered that the addition of nano functionalized block copolymer could have effect on disturbing the crack propagation only for the case of slow strain rate.

• Journal of Welding and Joining
• /
• 제34권6호
• /
• pp.28-34
• /
• 2016

Galvannealed(GA) steels are now generally used in car body manufacturing for corrosion resistance. In this study, the weldability and joint mechanical behavior of a newly developed 1.2GPa grade GA ultra high strength TRIP(transformation induced plasticity) steel was investigated for three joining processes, such as adhesive bonding, resistance spot welding and weldbonding. Under both shear and peel stress conditions, the failure mode of the adhesive joints were the mixture of the adhesive cohesive failure, adhesive interface failure and coating layer failure. It means that the adhesion strength of GA coating onto the base metal was similar to that of adhesive bonding onto the GA coating. Under the shear stress condition, the weldbonding exerted to expand the optimal spot welding condition of 1.2GPa GA TRIP steel because the strength of adhesive bond overwhelmed that of the resistance spot weld. Under the peel stress condition, the weldbonding also exerted to expand the optimal spot welding condition of 1.2GPa GA TRIP steel by inducing the tear fracture mode rather than the partial plug fracture mode.

• Tribology and Lubricants
• /
• 제23권1호
• /
• pp.14-18
• /
• 2007

SCM415 alloy was implanted with nitrogen ions using plasma source ion implantation (PSII), at a dose range of $1{\times}10^{17}\;to\;6{\times}10^{17}N^{+}cm^{-2}$. Auger electron spectrometry (AES) was used to investigate the depth profile of the implanted layer. Friction and wear tests were carried out on a block-on-ring wear tester. Scanning electron microscopy (SEM) was used to observe the micro-morphology of the worn surface. The results revealed that after being implanted with nitrogen ions, the frictional coefficient of the surface layer decreased, and the wear resistance increased with the nitrogen dose. The tribological mechanism was mainly adhesive, and the adhesive wear tended to become weaker oxidative wear with the increase in the nitrogen dose. The effects were mainly attributed to the formation of a hard nitride precipitate and a supersaturated solid solution of nitrogen in the surface layer.

• Restorative Dentistry and Endodontics
• /
• 제12권2호
• /
• pp.101-108
• /
• 1987

The purpose of this study was to investigate the pulpal responses of dental adhesive resins. A total of 40 cavities of the permanent healthy teeth from 4 dogs were prepared. In the experimental group, the cavities were etched for 1 minute with citric acid and filled with experimental resins (ie. Super-Bond C & B$^{(R)}$). In the control group, the cavities were filled with calcium hydroxide base materials (ie. Dycal$^{(R)}$) without etching. The dogs were sacrificed at one, two, three and four weeks after the time of filling and the specimens were routinely prepared and stained with Hematoxylin-Eosin. The microscopic findings were as follows: Infiltration of inflammatory cells was not observed in both experimental and control groups. Change in the odontoblastic layer was not observed in all control groups but severe swelling was observed in deep dental pulp tissue of the control two and three week cases. Pulp tissue was recovered with plenty of fibrous component in the control four week case and reparative dentin formation was not occurred in all cases. Slight changes of the odontoblastic layer beneath the cavity were observed in the experimental one week case. In experimental two and three week cases, swelling of deep pulp tissue was increased and localized reparative dentin formation was observed. In the experimental four week case, odontoblastic layer was recovered with regular appearance and fibrous component of the pulp was increased, but reparative dentin formation was not evident.

• 한국추진공학회:학술대회논문집
• /
• 한국추진공학회 2012년도 제38회 춘계학술대회논문집
• /
• pp.230-237
• /
• 2012

확대부 내열재의 스틸과 FRP 사이에 존재하는 미접착 결함과 미충전 결함을 검출하기 위해 초음파 공진법을 적용하였다. 초음파 공진법은 초음파 신호가 증폭되기 때문에 펄스에코법으로 검출하기 어려운 미접착 결함 및 에폭시 미충전 결함을 쉽게 검출할 수 있다. 공진 주파수는 삼중 매질의 음압 반사계수를 이용하여 예측하였고, 시험편의 초음파 신호에 대해 고속푸리에변환을 실시하여 측정하였다. 예측한 공진 주파수는 측정한 공진 주파수와 일치하므로 초음파 공진을 입증하였다.

• 한국염색가공학회지
• /
• 제34권3호
• /
• pp.173-184
• /
• 2022

In this study, the TPU film was laminated on an aramid fabric or circular knits in order to implement an air cushion material that can respond to high impact forces in case of a fall and is easy to expand. To increase the bonding strength between the fabric layer and the film layer, a primer layer was formed in two ways: one for thermally bonding and laminating PET film and two for coating and aging hot melt type PUR adhesive. The tensile strength of the aramid air cushion was 2.5 times higher than that of the circular knits, but the tensile elongation of the aramid air cushion was very low compared to that of the circular knits. The tear strength of the aramid air cushion was about twice or more superior to that of the circular knits, the primer treatment method was good at A, and the peel strength was excellent at method A. The aramid air cushion was the lightest in weight. Summarizing the above results, it was best to combine the air cushion material with aramid woven fabric and primer treatment method A to cope with the high impact force applied when falling.

• Restorative Dentistry and Endodontics
• /
• 제27권1호
• /
• pp.34-43
• /
• 2002

The purpose of this study was to compare microleakage and marginal hybrid layer in class V restorations using two one-bottle adhesives and one self-etching adhesive. Class V cavity preparations with occlusal margins in enamel and gingival margins in dentin were pre-pared on buccal and lingual surfaces of 30 extracted human molar teeth. Prepared teeth were randomly divided into three treatment groups (n=30) and restored with three adhesives and composites: Single Bond/Filtek Z-250 (Group 1), Prime&BondNT/Esthet.X (Group 2), UniFil Bond/UniFil F (Group 3). For microleakage, samples were stored in room temperature water for 24 hours, thermocycled stained with 2% methylene blue dye, sectioned into halves, scored and analysed using Mann-whitney test and Wilcoxon signed rank sum test. For marginal hybrid layer, samples were sectioned into halves, treated with 10% phosphoric acid for 5 seconds, stored in 5% NaOCL solution for 24 hours, dried and gold coated. Occlusal and gingival margins of each sample were inspected under SEM. The results of this study were as follows ; 1. Microleakage at the occlusal margins was not evident in group 1 and group 2, but it showed in group 3 (p<0.05). 2. Microleakage in group 1 and group 3 was significantly lower than in group 2 at gingival margins (p<0.05). 3. Microleakage at gingival margins was greater than at occlusal margins in group 1 and group 2, but microleakage at occlusal margins was greater than at gingival margins in group 3 (p<0.05). 4. In group 1 and group 2, no gaps at occlusal margins showed. But gaps showed in group 3. Occlusal margins were free from a hybrid layer in all groups 5. The thickness of the marginal hybrid layers was 2.5~5 $\mu\textrm{m}$ thick in group 5 $\mu\textrm{m}$ thick in group 2 and 1.5 $\mu\textrm{m}$ thick in group 3. 6 There was no corelation between microleakage and thickness of marginal hybrid layer. In coclusion, the effect of dentin adhesives on microleakge in class V composite restorations was excellent when one-bottle adhesives were applied on enamel margin, and it was good when a self-etching adhesive was applied on dentinal margin. There was no corelation between microleakage and thickness of marginal hybrid layer.

• Restorative Dentistry and Endodontics
• /
• 제32권4호
• /
• pp.313-326
• /
• 2007

본 연구는 단일 접착과정 상아질 접착제와 복합레진 사이에는 부적합성이 존재하며, 이를 개선하기 위해 중간 레진층이 필요하다는 가설을 규명하기 위해 시행되었다. 발치된 치아의 협설측 상아질에 3종의 단일 접착과정 상아질 접착제를 도포 후 광중합, 2종의 중간 레진층 적용, 광중합 또는 자가중합형 복합레진의 사용여부에 따라 30개의 실험군으로 분류하였다. 미세전단 결합강도를 측정하고 투과전자현미경 (TEM)을 이용하여 접착계면에서의 미세 누출과 수분의 이동경로를 관찰하여 접착제의 투과성을 평가하여 다음과 같은 결론을 얻었다. 중간 레진층을 적용 시 접착층의 투과도가 감소되었고 복합레진에 대한 단일 접착과정 상아질 접착제의 결합강도가 증가되었다. 따라서 시간 절약 및 간단한 접착과정을 선호하여 단순화된 상아질 접착제를 선택하는 것은 재고되어야 한다.