• Title/Summary/Keyword: adhesive bonding resin

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Shear bond strength of a self-adhesive resin cement to resin-coated dentin (간접수복용 복합레진과 자가 접착 레진 시멘트의 전단결합강도에 레진코팅법이 미치는 영향)

  • Hong, Jee-Youn;Park, Cheol-Woo;Heo, Jeong-Uk;Bang, Min-Ki;Ryu, Jae-Jun
    • The Journal of Korean Academy of Prosthodontics
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    • v.51 no.1
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    • pp.27-32
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    • 2013
  • Purpose: The aims of this study were to evaluate the effect of a resin coating on the shear bond strength of indirect composite restoration bonded to dentin with a self adhesive resin cement and to compare the shear bond strength with that of a conventional resin cement. Materials and methods: The occlusal enamels of thirty six extracted noncarious human molars were removed until the dentin flat surfaces of the teeth were exposed. Then, they were divided into 3 groups. The dentin surfaces of group 1 and 3 were left without any conditioning, while the dentin surfaces of group 2 were resin-coated with Clearfil SE bond and a flowable resin composite, Metafil Flo. After all specimens were temporized for 24 hours, indirect composite resin blocks fabricated by Tescera were bonded to dentins by Unicem for group 1 and 2, and by Panavia F for group 3. After 48 hours of water storage, shear bond strengths were measured. The data was analyzed with one-way analysis of variance and multiple comparison test (Tukey method). Results: The shear bond strengths of Unicem applied to resin coated dentin surfaces were significantly higher than those of Unicem and Panavia F used to uncoated dentin surfaces (P<.0001). Conclusion: Application of a resin coating to the dentin surface significantly improved the shear bonding strength of a self adhesive resin cement in indirect restoration.

Examination of Newsprint Residue as a Plywood Adhesive Filler (합판의 충전제로서 신문용지 잔사의 조사)

  • Oh, Yong-Sung
    • Journal of the Korean Wood Science and Technology
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    • v.24 no.2
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    • pp.42-45
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    • 1996
  • A residue from the newsprint waste was investigated as a filler in adhesive for bonding southern pine plywood. The residue was prepared by drying the wet residue to 8% moisture content and grinding the dry material using a laboratory Wiley mitt with a 75-${\mu}m$(200-mesh) screen. The residue was compared to a commercial filler commonly used in structural plywood adhesives. A total of 48 three-ply panels. 12.7mm nominal thickness and 0.3 by 0.3 m in size, were fabricated at two press times(4 and 5 min) and three assembly times(20, 40 and 60 min). Evaluations of the residue were carried out by performance tension shear tests after two 4-hour boil accelerated aging tests on plywood. The test results included tension shear strength and estimated wood failure values. All plywood made with the residue filler were comparable to the control-bonded plywood. These results indicate that residue from the newsprint waste streams would be suitable as filler for plywood adhesives.

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A comparison study on shear bond strength of 3D printed resin and conventional heat-cured denture base resin to denture relining materials (3D-프린팅 의치상 레진과 열중합 의치상 레진에서의 의치 첨상 재료 간의 전단결합강도 비교 연구)

  • Cho, Sung-Yoon;Song, Young-Gyun
    • Journal of Dental Rehabilitation and Applied Science
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    • v.37 no.4
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    • pp.232-243
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    • 2021
  • Purpose: The purpose of this study was to evaluate the shear bond strength of various 3D printed denture base resins and the conventional denture base resin to various denture relining materials. Materials and Methods: For denture base materials, a heatcured (Vertex RS) and two types of 3D printed DENTCA Denture base II, NextDentTM Base) were used. And 4 types denture relining materials (Tokuyama Rebase II fast, Kooliner, Denture Liner, Denture Liner, Lang Jet Denture Repair Kit) with different components were used. It was classified into 12 groups. Adhesion was performed between the resin base and the relining materials in accordance with ISO/TS 11405 standard. The shear bonding strength was measured, and then the adhesion interface was observed with a stereoscopic microscope and a scanning electron microscope. The fracture pattern was investigated through the analysis of the fragment. Results: In the 3D printed denture resin group, the shear bonding strength with relining materials was significantly lower than that of the heat-cured resin group (P < 0.05). The group of polymethyl methacrylate -based relining materials, high shear bonding strength was shown regardless of the type of denture. As for the fracture pattern, adhesive fracture appeared in most groups, and cohesive, mixed fracture appeared in some groups. Conclusion: The polymethyl methacrylate -based denture relining materials showed high shear bonding strength values compared to other denture relining materials. But, for direct methods, it is considered advantageous in terms of shear bonding strength to use a isobutyl methacrylate-based denture relining materials.

Study of Adhesion according to Various Surface Treatments for Lithium Ion Secondary Battery Pouch Film (다양한 표면처리에 따른 리튬이온 이차전지용 파우치 필름을 위한 접착성에 관한 연구)

  • Kim, Do Hyun;Bae, Sung Woo;Cho, Jung Min;Yoo, Min Sook;Kim, Dong Soo
    • Journal of the Korean Society for Precision Engineering
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    • v.33 no.3
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    • pp.231-234
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    • 2016
  • Pouch film is manufactured by laminating aluminum foil, polyamide film and polypropylene film with an adhesive or extrusion resin. However, a surface treatment is required for the aluminum because bonding does not occur easily between the aluminum foil and the polymer film. Thus, for this study, surface treatment experiments were performed in order to confirm the effect on adhesion strength. First, a variety of surface treatment solutions were coated on aluminum foil, and contact angle and surface morphology analysis was carried out for the surface-treated aluminum. For lamination of the surface-treated aluminum foil with polyamide film, a polyurethane base adhesive was prepared for the adhesive strength test specimens. The adhesive strength between the aluminum foil and the polyamide film of the resulting specimens was measured (UTM). With such an experiment, it was possible to evaluate the effect on adhesive strength of the various surface treatments.

A Study on the Taro Extension of UF and PF Resin Bonding Plywoods (요소(尿素) 및 석탄산수지(石炭酸樹脂) 합판(合板)의 토란증량(土卵增量)에 관(關)한 연구(硏究))

  • Lee, Phil Woo;Bae, Young Soo
    • Journal of Korean Society of Forest Science
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    • v.57 no.1
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    • pp.32-38
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    • 1982
  • This study was carried out to examine the possibility to replace imported wheat flour with taro. Taro and wheat flour were used for the extenders after oven drying($100{\pm}3^{\circ}C$)and pulverized into 80-100mesh minute powder by laboratory willey mill. Urea- and phenol-formaldehyde resin adhesives were used for plywood manufacture, and the extending materials mixed with the extension at the ratio of 10, 20, 30, and 50% to each resin solution. The results obtained at this study were summarized as follows; 1) In dry and wet shear strength of urea-formaldehyde resin adhesive, taro showed very excellent bonding strength compared with wheat flour in all extending ratio. Therefore taro showed the possibility that be usable to taro in place of wheat flour. 2) In dry and wet shear strength of phenol-formaldehyde resin adhesive, in general, wheat flour showed higher bonding strength than taro. But in dry shear strength, taro showed higher shear strength than wheat flour in 30 and 50% extension.

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Effect of Timing of Light Curing on the Shear Bond Strength of Three Self-adhesive Resin Cements

  • Yoo, Yeon-Kwon;Kim, Sung-Hun;Ryu, Jae-Jun;Ryu, Jae-Jun
    • Journal of Korean Dental Science
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    • v.1 no.1
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    • pp.28-34
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    • 2008
  • Objectives. The objectives of this study were: 1) to compare the effect of varying timing of light curing on shear bond strength, and; 2) to compare the shear bond strength of three self-adhesive cements. Materials and methods. A total of 72 extracted non-carious teeth were divided into 24 for Unicem tests, 24 for Maxcem tests, and 24 for Biscem tests; they were assigned 3 * 2 subgroups of 12 teeth each. The specimens were prepared as follows: 1) The calculus and periodontal ligament were removed from the teeth; 2) The teeth were stored in normal saline; 3) The occlusal enamel of each tooth was removed using high-speed coarse diamond burs under water cooling, and; 4) Finally, the teeth were flattened by 600-grit silicone carbide paper disks. Resin blocks were adhered using either Unicem, Maxcem, or Biscem. Light curing timing was divided into two groups: U10, M10, and B10 were exposed to light after 10 seconds, and; U150, M150, and B150 on the other side were exposed to light after 150 seconds. Shear bond strength was measured by a Universal testing machine with cross head speed of 1mm/min. T-test and One way ANOVA were used for the statistical analysis of data. Results. The shear bond strength of U150 was not significantly higher than that of U10 (U150: 20.55.7Mpa, U10: 18.73.80Mpa). On the other hand, the shear bond strength of M150 was significantly higher than that of M10. The shear bond strength of B150 was also significantly higher than that of B10 (M150:14.45.7Mpa, M10: 9.94.2Mpa, B150: 24.38.3Mpa, B10: 17.27.3Mpa). When the light curing timing was 10sec after bonding, the shear bond strength of Unicem was highest; the shear bond strength of Biscem was highest when the light curing timing was 150sec after bonding (U10: 18.73.80Mpa, B150: 24.38.3Mpa). Significance. Since Unicem is less sensitive based on light curing timing, dentists seem to use it without considering the light curing timing. Maxcem showed the lowest bonding strength (especially M10). Thus, when using Maxcem, dentists need to delay the light curing after adhesion.

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Utilization of Waste Bone Powders as Adhesive Fillers for Plywood (합판용 접착제의 충전제로서 폐기 골분의 이용)

  • Ko, Jae Ho;Roh, JeongKwan
    • Journal of the Korean Wood Science and Technology
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    • v.43 no.4
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    • pp.528-537
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    • 2015
  • To reuse the waste bone from restaurants or butcher houses, the possibility of using waste bone powder after cooking as a filler for wood adhesives used in manufacturing plywood was investigated. Radiata pine (Pinus radiata D. Don) plywoods were manufactured by using commonly used wood adhesives such as urea-melamine formaldehyde (UMF) resin, urea-formaldehyde (UF) resin, and phenol-formaldehyde (PF) resin and the prepared fillers from cattle bone powder, pig bone powder, and seashell powder. Plywood fabricated by using cattle bone powder, pig bone powder, and seashell powder showed weaker performance in dry and wet glue-joint shear strength and wood failure than those of the plywood with wheat flour. The result showed that it was hard to use only bone powder for the replacement of wheat flour. However, the filler mixed with wheat flour and bone powders showed equivalent dry bonding strength and better water resistance than the wheat flour, indicating that bone powders mixed with wheat flour might be used for the manufacture of plywood. When bone powders were mixed with wheat flour as adhesive fillers the shell powder showed the lowest bonding properties and there was no big difference between the cattle bone powder and the pig bone powder.

Reduction of Formaldehyde Emission from Particleboardsby Bio-Scavengers

  • Eom, Young-Geun;Kim, Jong-Sung;Kim, Sumin;Kim, Jin-A;Kim, Hyun-Joong
    • Journal of the Korean Wood Science and Technology
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    • v.34 no.5
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    • pp.29-41
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    • 2006
  • This study was to investigate the effect of adding additive as tannin, rice husk and charcoal, for reducing the formaldehyde emission level, on the adhesion properties of urea-formaldehyde (UF) resin for particleboard. We controlled the hot-pressing time, temperature and pressure to determine the bonding strength and formaldehyde emission. Blends of various UF resin/additives (tannin, rice husk and charcoal) compositions were prepared. To determine and compare the effect of additives (tannin, rice husk and charcoal) content, 0, 5, 10 and 15%, by weight of UF resin, were used. $NH_4Cl$ as hardener added. To determine the level of formaldehyde emission, we used the desiccator, perforator and 20 L-small chamber method. The formaldehyde emission level decreased with increased additions of additive (except rice husk). Also, increased hot-pressing time decreased formaldehyde emission level. At a charcoal replacement ratio of only 15%, the formaldehyde emission level is under F ✩ ✩ ✩ ✩ grade (emit < $0.3mg/{\ell}$). Curing of the high tannin additive content in this adhesive system indicated that the bonding strength increased. But, in the case of rice husk and charcoal, the bonding strength was much lower due to the inorganic substance. Furthermore, rice husk was poor in bonding strength as well as formaldehyde emission than tannin and charcoal.

The shear bond strength and adhesive failure pattern in bracket bonding with different light-curing methods (브라켓 접착시 광중합방식에 따른 전단결합강도와 파절양상 비교)

  • Shin, Jai-Ho;Lim, Yong-Kyu;Lee, Dong-Yul
    • The korean journal of orthodontics
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    • v.34 no.4 s.105
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    • pp.333-342
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    • 2004
  • The purpose of this study was to evaluate the clinical effectiveness of a plasma arc light and light emitting diode (LED), compared with shear bond strength and the failure pattern of brackets bonded with visible light in direct bonding. Brackets were bonded with Transbond XT to 60 human premolars embedded in the resin blocks according to different light-curing methods. Then, the shear bond strength of each group was measured using a universal testing machine (Instron) and the adhesive failure pattern after debonding was visually examined by light microscope. The results were as follows: 1. The shear bond strength showed no significant difference between the visible light and light emitting diode, but the plasma arc light exhibited a significantly lower shear bond strength compared with the visible light and light emitting diode. 2. In the visible light and light emitting diode, adhesive failure patterns were similar. Bond failure occurred more frequently at the enamel-adhesive interface. 3. The bonding failure of brackets bonded with plasma arc light occurred more frequently at the bracket-adhesive interface. The results of this study suggest that plasma arc light, light emitting diode and visible light are all clinically useful in the direct bonding of orthodontic brackets.

Effect of applying adhesive after enamel etching on the shear bond strength of orthodontic brackets using light curing resin cements (광중합형 레진시멘트를 사용한 치열교정용 브라켓 접착 시 접착제 사용 유무가 산 부식한 법랑질의 전단접착강도에 미치는 영향)

  • Kim, Eung-Hyun;Kim, Jin-Woo;Park, Se-Hee;Lee, Yoon;Cho, Kyung-Mo
    • Journal of Dental Rehabilitation and Applied Science
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    • v.37 no.4
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    • pp.209-216
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    • 2021
  • Purpose: The purpose of this study is to compare the shear bond strength of resin cement for orthodontic brackets without applying an adhesive primer, to the case of applying an adhesive primer. Materials and Methods: The specimens were divided into three experimental groups, Transbond XT, GC Ortho Connect and Orthomite LC, and the enamel surface was divided into two sections, one with 37% phosphoric acid and the other with 37% phosphoric acid and an adhesive primer or universal adhesive. Each of three types of cement was applied to orthodontic bracket, and after bonding, the shear bond strength was measured. Results: Transbond XT and Orthomite LC significantly increased shear bond strength when orthodontic brackets were bonded after applying an adhesive primer and universal adhesive, respectively. Conclusion: It is expected that application of an adhesive primer or universal adhesive after acid etching will improve shear bond strength of orthodontic brackets in Transbond XT and Orthomite LC.