• Title/Summary/Keyword: adhesion test

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Failure Mode and Strength of Unidirectional Composite Single Lap Bonded Joints II. Failure Prediction (일방향 복합재료 Single Lap 접합 조인트의 파손 모드 및 파손 강도 II. 파손 예측)

  • Yi Young-Moo;Kim Chun-Gon;Kim Kwang-Soo
    • Composites Research
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    • v.18 no.1
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    • pp.1-9
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    • 2005
  • A methodology is presented for the failure prediction of composite single-lap bonded joints considering both of composite adherend failure and bondline failure. An elastic-perfectly plastic model of adhesive and a delamination failure criterion are used in the methodology. The failure predictions have been performed using finite element method and the proposed methodology. The failure prediction results such as failure mode and strength have very good agreements with the test results of joint specimens with various bonding methods and parameters. The influence of variations in the effective strength (that is, adhesion performance) and plastic behavior of adhesive on the failure characteristics of composite bonded Joints are investigated numerically. The numerical results show that optimal joint strength is archived when adhesive and delamination failure occur in the same time.

Development of Relief Valves for the Domestic Gas-fired Hot Water Boilers (가정용 가스보일러 과압방지밸브의 개발 연구)

  • Kim Young Gyu;Kwon Jeong Rock;Kim Ji Yoon;Suh Joon Suk
    • Journal of the Korean Institute of Gas
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    • v.4 no.1 s.9
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    • pp.63-68
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    • 2000
  • We have developed a new relief valve which is a safety device for the domestic gas-fired hot water boilers. The relief valve has been designed to expand the inner diameter of the inlet, the outlet and the seat of the valve considering the relief capacity, and also to separate the spring from the room heating water. Therefore, we could minimize the adhesion and/or obstruction of the inlet and the corrosion phenomena of the spring which used to be the problem of the conventional relief valves. Test results of the developed relief valve showed that the performance of the opening pressure, reseating pressure, tightness, endurance were excellent, and the operating boiler with developed relief valve was evaluated as very good. The standardization and application of the relief valve can provide the advantage of component exchange and easy maintenance and repair.

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Reliability Evaluation System of Hot Plate for Photoresist Baking (Hot Plate 신뢰성 시험.평가시스템 개발)

  • Song, Jun-Yeop;Song, Chang-Gyu;No, Seung-Guk;Park, Hwa-Yeong
    • Journal of the Korean Society for Precision Engineering
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    • v.19 no.8
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    • pp.180-186
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    • 2002
  • Hot Plate is the major unit that it used to remove damp of wafer surface, to strength adhesion of photoresist (PR) and to bake coated PR in FAB process of semiconductor. The badness of Hot Plate (HP) has directly influence upon the performance of wafer, it is necessary to guarantee the performance of HP. In this study, a reliability evaluation system has been designed and developed, which is to measure and to estimate thermal uniformity and flatness of HP in range of temperature 0~$250^\circC$. This system has included the techniques which measures and analyzes thermal uniformity using infrared thermal vision, and which compensates measuring error of flatness using laser displacement sensor For measuring flatness, a measurement stage of 3 axes are developed which adapts the precision encoder. The allowable error of this system in respect of thermal uniformity is less $than\pm0.1^\circC$ and in respect of flatness is less $than\pm$1mm . It is expected that the developed system can measure from $\Phi200mm\;(wafer 8")\;to\;\Phi300mm$ (wafer 12") and also can be used in performance test of the Cool Plate and industrial heater, etc.

Cu/Ni-Mo-Nb/Polyimide FCCL (Flexible Copper Clad Laminate)의 개발 및 플렉시블 전자기기 응용을 위한 접착 특성

  • Bang, Seong-Hwan;Kim, Gyeong-Gak;Jeong, Ho-Yeong;Seol, Jae-Bok
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.171-171
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    • 2013
  • 2층 FCCL (연성회로기판, Flexible Copper Clad Laminate)에 있어서 폴리이미드 필름과 구리의 접착력을 향상 시키기 위해 기존에 사용되고 있는 Ni-Cr대신 박리강도가 높고 에칭성도 매우 뛰어난 Ni-Mo-Nb 박막을 Roll-to roll 스퍼터 장비를 이용하여 개발하였다. 새롭게 개발된 Ni-Mo-Nb 박막은 기존 연구되어진 Ni-Cr 물질 대비 고온 박리강도 약 1.5~2.0배, 에칭성 8배 이상의 매우 우수한 특성을 보였다. Ni-Mo-Nb 접착층의 두께가 7~40 nm로 증가함에 따라 상온 박리강도가 향상 되는 것을 확인하였다. Ni-Mo-Nb 박막을 증착 하기 전 폴리이미드 기판표면을 RF 플라즈마 전처리 하였을 때 0.67 kg f/cm의 우수한 상온 박리강도를 나타내었으며 FCCL 샘플을 $150^{\circ}C$에서 168시간동안 열처리 한 후 접착력을 측정하였을 때도 0.54 kg f/cm의 높은 고온 박리강도를 보였다. FCCL의 박리강도, 표면 거칠기, 원소들의 화학적 결합, 박막의 미세구조를 peel test, atomic force microscopy, X-ray photoelectron spectroscopy, transmission electron microscopy를 이용하여 폴리이미드 기판 플라즈마 전처리 효과를 확인하였다. 그 결과 플라즈마 전처리를 한 폴리이미드 기판의 경우 처리하지 않은 기판보다 상온과 고온에서 더 우수한 접착력을 가지는 것을 확인 할 수 있었는데 이것은 폴리이미드 기판의 표면 거칠기 증가에 의한 mechanical interlocking effect가 아닌 전처리를 통한 폴리이미드 표면 개질로 C-0, C-N와 같은 chemical functional group이 증가했기 때문인 것으로 확인되었다.

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Silk Protein as a Fetal Bovine Serum Substitute for Animal Cell Culture

  • Jo, You-Young;Kweon, HaeYong;Ji, Sang Deok;Kim, Jong Gil;Kim, Kee Young
    • Microbiology and Biotechnology Letters
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    • v.47 no.4
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    • pp.487-497
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    • 2019
  • Fetal Bovine Serum (FBS) is an essential substance added to animal cell culture medium. However, its composition is unclear causing problems such as development of an immune response when cultured cells are transplanted into the human body. In this study, silk sericin, silk fibroin, and hemolymph obtained from silkworms were added to the cell culture medium in order to determine if it can replace FBS. After establishment of the cell culture, cell proliferation and expression levels of cell growth-related genes were compared with those of control cells (cells cultured in the medium with 10% FBS). Results showed that the test group treated with silk fibroin extracted from a Korean silkworm variety, Kumokjam could replace 10% FBS. In addition, expression levels of cell growth related genes such as Fibronectin and TGF-β1 increased significantly in cells cultured using silk fibroin, depending on the concentration used in cell adhesion and cell proliferation [24]. To date, no studies have been conducted to find a replacement for FBS. Thus, this study was carried out to develop a substitute for FBS by using silkworm-derived alternatives such as silkworm hemolymph, silk sericin, and silk fibroin, which are cheap and have various physiological effects, cell promoting effects, and can be mass produced.

Deterioration Characteristic of Shotcrete Immersed in Chemical Solution (화학적 침식에 의한 숏크리트의 열화특성 분석 - 단기거동)

  • Lee, Gyu-Phil;Kim, Dong-Gyou;Bae, Gyu-Jin;Shin, Hyu-Soung
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.7 no.2
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    • pp.143-152
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    • 2005
  • Shotcrete for support of tunnel structures may contact with groundwater. The hazardous components in groundwater may cause corrosion of shotcrete. Also, the hazardous components may deteriorate the engineering properties of shotcrete, such as compressive strength, bond strength, flexural strength and so forth. The more the effect of the hazardous components on the shotcrete may increase, the more the stability of tunnel structure may decrease. The specimens were artificially immersed in various chemical solutions including hazardous components after the specimens were made at the tunnel construction site. It was performed to analyze the effect of the hazardous components in ground water on the engineering properties of shotcrete. The uniaxial compressive strength test, XRD, SEM were conducted to evaluate the durability and corrosion of shotcrete.

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The change of the physiological response of the Crassostrea gigas exposed to PAHs (다환방향족탄화수소 (PAHs) 에 노출된 굴, Crassostrea gigas의 생리 반응 변화)

  • Choi, Eun Hee;Choi, Joong Ki;Lee, Won Young;Yoon, Ju Hyun;Shim, Na Young;Kim, Su Kyoung;Lim, Hyun Jeong
    • The Korean Journal of Malacology
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    • v.30 no.3
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    • pp.169-175
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    • 2014
  • PAHs (Polycyclic Aromatic Hydrocarbons: PAHs) is the hydrophobic inorganic material composed of carbon and hydrogen that is easily adsorbed biological organisms in the ocean. Bivalves is the indicator of environment monitoring because of reflect growth, physiological response of bivalve followed their habitat environment. The aim of research is understand the change of oysters (Crassostrea gigas) physiological response under exposed PAHs concentration for control, 1, 10 and $100{\mu}g/L$. We investigated induced immune change response for oyster hemocyte and effect of tissue RNA/DNA ratio for mantle, gill and adductor muscle individually. As a result of experiment change of immune response the oyster hemocyte when exposed PAHs showed that viability and adhesion is no significant difference (ANOVA test, p < 0.05). However phagocytosis decreased under the over $10{\mu}g/L$ of PAHs concentration and ROS increased with the increase of PAHs concentration. The change of RNA/DNA ratio is R/D ratio decreased with the increase of PAH concentration in adductor muscle. However gill and mantle showed no change of R/D ratio with PAHs concentration. The oysters when exposed inorganic pollutant that decreased of physiological condition and damaged protein synthesis of adductor muscle.

A study on chemical bonding characteristics of the interface between curved FRP panels for consecutive structural assembly (곡면 FRP 패널 부재 연속시공을 위한 연결부 화학적 접합 특성에 관한 연구)

  • Lee, Gyu-Phil;Shin, Hyu-Soung;Jung, Woo-Tai
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.14 no.1
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    • pp.79-91
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    • 2012
  • A curved fiber reinforced polymer (FRP) panel is produced with a certain width depending on allowances of manufacturing processes and facilities. An targeted arch-shaped structure could be built by sequential connection of series of the FRP panels. The connection manner between the FRP panels could be given by chemical treatment, mechanical treatment and hybrid method. Among those, the connection between the panels by chemical treatment is commonly adopted. Therefore, For an optimized design of the connected part between FRP pannels, a number of direct shear tests have been undertaken in terms of a number of parameters: surface treatment conditions, bonding materials, etc.. As results, surface grinding condition by sand paper or surface treatment by sand blasting appear properly acceptable methods, and epoxy and acryl resins are shown to be effective bonding materials for the purpose in this study.

A Shear Bond Chracteristics of Composite Slab with Closed-Shape Deckplate (폐쇄형 데크플레이트를 사용한 합성슬래브의 전단부착 특성에 관한 연구)

  • Ju, Gi Su;Park, Sung Moo
    • Journal of Korean Society of Steel Construction
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    • v.13 no.5
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    • pp.557-566
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    • 2001
  • Composite slab with deckplate needs sufficient bond strength between deckplate and concrete to conduct composite behavior Composite slab can transfer the shear by either chemical adhesion interface interlock, or active friction. There are several way of mechanical shear connection in composite slab. that is embossments shear connector shape of deckplate etc. Effect of mechanical interaction is deped on shape of deckplate which is to prevent peeling between deckplate and concrete and an amount of shear connector. The behavior and strength of the connection between the decking and the concrete slab due to embossments and end anchorage may be estimated using the push-off tests described in this paper We proposed the equation of shear bond strength in the composite slab It will be use to design by basic data in composite slab.

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High Efficient and Stable Dye-sensitized Solar Cells (DSSCs) with Low Melting Point Glass Frits

  • Kim, Jong-U;Kim, Dong-Seon;Kim, Hyeong-Sun
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2011.05a
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    • pp.42.2-42.2
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    • 2011
  • $TiO_2$ films were modified by adding a glass frit as a light scattering particle and applied to an anode electrode in dye-sensitized solar cells (DSSCs) to enhance the adhesion between $TiO_2$ and fluorine doped transparent oxide (FTO). Low melting point glass frits at contents of (3 to 7wt%) were added to the nano crystalline $TiO_2$ films. The light scattering properties, photovoltaic properties and microstructures of the photo electrodes were examined to determine the role of the low glass transition temperature ($T_g$) glass frit. Electrochemical impedance spectroscopy, Brunauer-Emmett-Teller method and scratch test were conducted to support the results. The DSSC with the $TiO_2$ film containing 3wt% low Tg glass frit showed optimal performance (5.1%, energy conversion efficiency) compared to the $TiO_2$-based one. The photocurrent density slightly decreased by adding 3wt% of the frit due to its large size and non conductivity. However, the decrease of current density followed by the decrease of electron transfer due to the large frit in $TiO_2$ electrode was compensated by the scattering effect, high surface area and reduced the electron transfer impedance at the electrolyte-dye-$TiO_2$ interface. The stability of the photo electrodes was improved by the frit, which chemically promoted the sintering of $TiO_2$ at relatively low temperature ($450^{\circ}C$).

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