• 통합자연과학논문집
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• 제12권4호
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• pp.116-121
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• 2019

This experiment is to evaluate the physical properties of the hydrogel lens with the addition of carbon-based nanomaterials, Graphene oxide and Carbon nanotube, and to confirm the improvement of strength. Hyaluronic acid, a hydrophilic substance, was used as an additive by using HEMA (2-hydroxyethyl methacrylate) and ethylene glycol dimethacrylate (EGDMA) as a base monomers. Graphene oxide and two types of Carbon nanotubes(Amide functionalized and Carboxilic acid functionalized) were added 0.1%, 0.3%, 0.5%, respectively, and the physical properties were analyzed by measuring water content, refractive index, breaking strength and SEM image. In the case of the sample added with each carbon nano material, the water content tended to increase for all three materials. The breaking strength tended to increase in Graphene oxide and Carbon nanotube; Carboxilic acid functionalized, but in the case of Carbon nanotube; amide fuctionalized, the breaking strength tended to decrease. However, Carbon nanotube; amide fuctionalized had the highest breaking strength among the three nano materials. Thus, the addition of certain carbon nanomaterials seems to be appropriate for improving the strength of hydrogel lenses.

• 접착 및 계면
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• 제14권2호
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• pp.68-74
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• 2013

Acid group을 도입하여 접착 및 그립성이 향상된 casting 폴리우레탄을 합성하였다. 폴리우레탄의 그립 특성 및 접착 특성을 확인하였고, 접촉각 및 인장강도, 기계적 물성 등을 연구하였다. Acid 함량에 따른 특성들을 조사하기 위해 acid 함량별로 경화제를 제조하여 각각의 특성들을 연구하였다. Acid group을 도입함으로써 접착력 및 wet slip이 증가하는 것을 확인할 수 있었으며, 인장강도 및 마모 등 기계적 물성 또한 증가하는 것을 확인할 수 있었다. Acid 함량별로 물성을 측정한 결과 일정한 함량까지 기계적 물성은 증가하며, 일정 함량 이상에서는 기계적 물성 및 접착력이 감소하는 것을 확인할 수 있었다. Wet slip과 접촉각의 경우에는 acid group 도입에 의해 친수성이 증가함으로 acid 함량이 증가할수록 wet slip은 증가하며 접촉각의 경우에는 감소하는 것을 확인할 수 있었다.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2006년도 춘계학술논문 발표대회 제6권1호
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• pp.81-84
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• 2006

This study is intended for how to utilize the recycled fine aggregate which is produced by concrete wastes. It analyzes the quality of the fine aggregate which is reproduced through the acid treatment process, and comprehends the characteristics of mortar using the recycled fine aggregate to review whether it can be put to practical use for concrete. The conclusion of the study are as follows 1. The recycled fine aggregate through the acid treat shows the low rate of absorption and high density. 2. Compared to the mortar made from acid liquid precipitated recycled fine aggregate, using nature water precipitated one reduces the flow. 3. The compressive strength of mortar using recycled fine aggregate tends to be reduced according to the kind of precipitated water. Based on the above results, the recycled fine aggregate through the acid treatment process satisfies the quality standards of the first-grade recycled fine aggregate of KS F 2573 (recycled fine aggregate for concrete) but it is concluded that the recycled fine aggregate through the acid treatment process can not used as fine aggregate used concrete because it has destructive characteristics when the mortar is produced

• 한국농공학회지
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• 제45권7호
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• pp.20-26
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• 2003

The ultra-lightweight high strength polymer concrete could be used for the drain structures under severe condition. In this study, materials used were unsaturated polyester resin, heavy calcium carbonate, artificial lightweight coarse aggregate and perlite. In the test results, the unit weight of the ultra-lightweight high strength polymer concrete was 946 kg f/$\textrm{m}^3$ and the compressive strength was appeared in 34.5 MPa. The compressive strength, splitting tensile strength, flexural strength, acid resistance and weather resistance were shown in excellently than that of the normal cement concrete. The draining trench had 1m length, 0.24 m width, 0.02 m thickness and 0.07 m height. The developed trench could be effectively used at the draining structures.

• Restorative Dentistry and Endodontics
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• 제20권1호
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• pp.362-371
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• 1995

The purpose of this study was to evaluate the shear bond strength between composite resin and glass ionomer cement according to surface treatment methods of glass ionomer cement. Sixty round acrylic cylinders were fabricated. And then, a round undercut cavity(8 mm diameter, 2.5mm depth) was prepared in the center of the every acrylic cylinder. After all cavities were restored by using light-cured glass ionomer cement. A total of sixty acrylic cylinders restored with glass ionomer cement were divided into 4 groups according to surface treatment methods of glass ionomer cement. The surface treatment of each group were as follows : control group : no treatment Group 1 : acid etching Group 2 : sandblasting Group 3 : air-podwer abrasive polishing The composite resin was bonded to glass ionomer cement of each specimens. And the shear bond strength was tested with a universal testing machine at a cross-head speed of 1mm/min and 500kg in full scale. The results were as follows : 1. The sandblasting group(group 2) had the highest shear bond strength with $272.50{\pm}24.96\;kg/cm_2$ and the acid etching group(group 1) had the lowest shear bond strength with $192.89{\pm}29.32kg/cm_2$. 2. The no treated group(control group) had higher shear bond strength than acid etching group(group 1) (p<0.05). 3. The sandblasting group(group 2), air-powder abrasive polishing group(group 3) and no treated group(control group) had higher shear bond strength than the acid etching group(group 1) (p<0.05). 4. The sandblasting group(group 2) and air-powder abrasive polishing group(group 3) had higher shear bond strength than the no treatment group(control group), but there was not significant(p>0.05).

• 폴리머
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• 제37권2호
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• pp.184-195
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• 2013

아크릴 점착테이프는 자동차, 전기전자 및 디스플레이 모듈 접합에 사용된다. 본 연구는 이러한 모듈 접합에 사용되는 고강도 준구조형 점착테이프 제조를 위해 2-ethylhexylacrylate(2-EHA)와 acrylic acid(AAC)를 사용하여 UV 조사에 의한 광중합 및 점착테이프 제조를 위해 광경화를 진행하였고, AAC의 함량 및 무기물 충전제 $SiO_2$ 함량에 따라 아크릴 점착테이프의 물성에 미치는 영향을 고찰하였다. 공단량체로 사용된 AAC의 함량이 많을수록 아크릴고분자 사슬의 강직성이 증가하여 초기 점착력이 낮았고, 시간경과에 따라 점착력이 증가하였으며 테이프의 젖음성, 접촉각 및 SEM 이미지를 통해 확인할 수 있었다. 충전제를 첨가하지 않은 점착테이프의 박리강도와 전단접착강도는 반비례 관계였으나 충전제를 첨가하면 함량 증가에 따라 박리강도 증가와 함께 전단접착강도가 증가하는 비례관계를 보였다. 이러한 상관관계로부터 고강도 준구조형 접착물성을 필요로 하는 용도에 최적화된 아크릴 점착테이프를 제시할 수 있었다.

• 산업기술연구
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• 제22권B호
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• pp.13-20
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• 2002

The purpose of this study is to investigate the effect of acid fog on the rust formation behavior of weathering steel (SMA50) which is used in uncoated bridges. Weathering steel didn't form the passive film under the environment of acid fog(pH5,6), whereas the environment of distilled water formed the protective oxide film. Therefore, the construction of weathering steel under the environment extremely exposed to SOx and NOx which are the main compositions of acid fog is not adequate. Fatigue limits of weathering steel under acid fog environment are remarkably decreased as compared with environment of distilled water. The corrosive constituents in acid fog has piled up the corrosion products on specimen surface and generated the corrosion pits. Because of the high stress concentration arising at this corrosion pit, relatively low fatigue limits were obtained for acid fog specimens.

• 대한소아치과학회지
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• 제25권4호
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• pp.761-771
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• 1998

In this study, attempt has been made to evaluate the effect of $CO_2$ laser irradiation on enamel surface structure and the bond strength of sealant material. Conventional acid etching was used as a control technic for comparison. The results obtained from this experiment were as follows; 1. The highest mean shear bond strength value was observed in samples of Group I (acid-etching) with the statistical significance(p<.05) between all the other groups. 2. The shear bond strength in Group IV was the lowest among laser etching groups. but there were no significant difference between them(p>.05). 3. Scanning electron microscopic observation showed that the rough and irregular surface was created by $CO_2$ laser treatment with the formation of numerous pores, micro-cracks, and small bubble-like inclusion. Increasing the energy density induced localized surface melt with a thin smooth glaze-like appearance. 4. In acid-etched control specimen cohesive failure predominated, whereas adhesive failure was the main mode in laser-treated group. Based upon the above-mentioned results, it can be assumed that the $CO_2$ laser is not an adequate substitute for the acid-etch technique in enamel preconditioning. More studies are required to explore the effective condition of laser irradiation which could attain the better bond strength of restorative materials.

• The Journal of Advanced Prosthodontics
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• 제9권2호
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• pp.77-84
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• 2017

PURPOSE. The aim of this study was to compare the surface roughness of zirconia when using Zircos E etching system (ZSAT), applying a nitric acid-hydrofluoric acid compound as a pretreatment agent, and also to compare the shear bonding strength according to different resin cements. MATERIALS AND METHODS. ZSAT, air abrasion, and tribochemical silicacoating were applied on prepared 120 zirconia specimens (10 mm in diameter, 7 mm in height) using CAD/CAM. Each 12 specimens with 4 different resin cements (Panavia F 2.0, Rely X Unicem, Superbond C&B, and Hot bond) were applied to test interfacial bond strength. The statistical analysis was performed using SAS 9.1 (SAS Institute Inc., Cary, NC, USA). The results are as follows: after application of the ZSAT on the zirconia specimens, surface roughness value after 2-hour etching was higher than those after 1- and 3-hour etching on SEM images. RESULTS. For Superbond C&B and Rely X Unicem, the specimens treated with ZSAT showed higher shear bond strength values than those treated with air abrasion and tribochemical silicacoating system. Regarding the failure mode of interface over cement and zirconia surface, Rely X Unicem and Hot bond showed cohesive failures and Panavia F 2.0 and Superbond C&B showed mixed failures. CONCLUSION. Zircos E etching system in zirconia restoration could increase its shear bond strength. However, its long term success rate and clinical application should be further evaluated.

• Restorative Dentistry and Endodontics
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• 제8권1호
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• pp.107-113
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• 1982

The purpose of this study was to observe the tensile strength of composite resins to etched dentin surface with the various methods of placing bonding agent before composite resin or placing composite resin alone. Recently extracted 60 maxillary incisors were chosen. These were divided into 6 groups: Group I : Immediate Silar adaptation to the etched dentin surface with 37% phosphoric acid for 60 seconds without bonding agent. Group II : Immediate Silar adaptation to the etched dentin surface with 37% phosphoric acid for 60 seconds with bonding agent. Group III : Silar adaptation to the etched dentin surface with 37% phosphoric acid for 60 seconds after 5 minutes of bonding agent. Group IV : Immediate Enamelite adaptation to the etched dentin surfaces with 50% phosphoric acid for 120 seconds without bonding agent. Group V : Immediate Enamelite adaptation to the etched dentin surface with 50% phosphoric acid for 120 second s with bonding again. Group VI : Enamelite adaptation to the etched dentin surface with 50% phosphoric acid for 120 seconds after 5 minutes of bonding agent. All specimens were immersed in water at $37^{\circ}C$ for 24 hours before testing. The results were as follows: 1. The tensile strength of powder/liquid composite resin system was higher than that of pastel paste composite resin system. 2. The tensile strength of the composite resin group II, III, V, & VI with bonding agent was higher than that of the composite resin group I & IV without bonding agent. 3. The tensile strength of the composite resin group III & VI after 5 minutes added to bonding agent was higher than that of the composite resin group II & V immediately added to bonding agent.