• 제목/요약/키워드: absorbance method

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Effects of Lavender Extract on Damaged Hair (라벤더 추출물이 손상모발에 미치는 영향)

  • Kim, Ju-Sub
    • Journal of the Korean Applied Science and Technology
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    • v.39 no.5
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    • pp.614-622
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    • 2022
  • This study attempted to investigate the effect of manufacturing a formulation with lavender extract and applying it to damaged hair. The experimental material was prepared by adding 0 g, 3 g 6 g, and 9 g of lavender extract to the perm base agent. The prepared formulation was applied to four damaged hair samples and compared and analyzed. As a measurement method for the effect on damaged hair, tensile strength, absorbance using methylene blue, and gloss were measured. Statistical analysis was conducted for the reliability of the research results. The tensile strength measurement results showed that the tensile strength of the sample applied with a formulation containing 6 g and 9 g at 8 levels increased, affecting damaged hair. As a result of absorbance analysis using methylene blue, it was found that the absorbance of all samples applied by adding extracts decreased, affecting damaged hair. The gloss measurement results showed that the addition of 9 g affected the damaged hair. In conclusion, it can be seen that lavender extract affects damaged hair, so it is considered to have an effect of improving Damage hair.

A Study of Oil of Basil Extract on Improvement of Hair Damage (바질 오일의 손상모발 개선효과에 관한 연구)

  • Kim, Ju-Sub
    • Journal of the Korean Applied Science and Technology
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    • v.39 no.2
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    • pp.294-302
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    • 2022
  • This study attempted to investigate the effect of improving damaged hair by preparing a hair improving agent with basil oil and applying it to damaged hair. An experimental material was added to a perm base agent containing 0 g, 3 g, 6 g, 9 g of basil oil to prepare the preparation. It was applied to sample hair bleached at 8 levels with the prepared formulation. Each sample and damaged hair were measured and analyzed. The measurement method measured tensile strength, absorbance and gloss using methylene blue to determine the effect of improving maternal quality. Statistical analysis was conducted on the reliability of the study results. Studies have shown that all samples with basil oil have higher tensile strength than damaged hair. As a result of the absorbance analysis using methylene blue, it was found that the absorbance was lower than that of damaged hair in all samples. Gloss measurement showed that all samples showed increased luster compared to damaged hair. In conclusion, basil oil was found to improve damaged hair. In the future, research on various types of oil and research methods is needed.

Preparation of Regenerated Cellulose Fiber via Carbonation. I. Carbonation and Dissolution in an Aqueous NaOH Solution

  • Oh, Sang Youn;Yoo, Dong Il;Shin, Younsook;Lee, Wha Seop;Jo, Seong Mu
    • Fibers and Polymers
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    • v.3 no.1
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    • pp.1-7
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    • 2002
  • Cellulose carbonate was prepared by the reaction of cellulose pulp and $CO_2$ with treatment reagents, such as aqueous $Zncl_2$ (20-40 wt%) solution, acetone or ethyl acetate, at -5-$0^{\circ}C$ and 30-40 bar ($CO_2$) for 2 hr. Among the treatment reagents, ethyl acetate was the most effective. Cellulose carbonate was dissolved in 10% sodium hydroxide solution containing zinc oxide up to 3 wt% at -5-$0^{\circ}C$. Intrinsic viscosities of raw cellulose and cellulose carbonate were measured with an Ubbelohde viscometer using 0.5 M cupriethylenediamine hydroxide (cuen) as a solvent at $20^{\circ}C$ according to ASTM D1795 method. The molecular weight of cellulose was rarely changed by carbonation. Solubility of cellulose carbonate was tested by optical microscopic observation, UV absorbance and viscosity measurement. Phase diagram of cellulose carbonate was obtained by combining the results of solubility evaluation. Maximum concentration of cellulose carbonate for soluble zone was increased with increasing zinc oxide content. Cellulose carbonate solution in good soluble zone was transparent and showed the lowest absorbance and the highest viscosity. The cellulose carbonate and its solution were stable in refrigerator (-$5^{\circ}C$ and atmospheric pressure).

Analytical Methods for Cationic Surfactants Sorbed by Fabrics (직물에 흡착된 양이온계면활성제 정량방법에 관한 연구)

  • 박선경;정혜원
    • Journal of the Korean Society of Clothing and Textiles
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    • v.24 no.3
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    • pp.422-428
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    • 2000
  • At present, analytical methods available for determining the amount of cationic surfactants(DSDMAC) on the fabrics are spectrophotometric method based on formation and extraction of the colored ion pair with anionic dye, radiochemical analysis and HPLC analysis. This study presents new analytical methods based on the formation of cationic surfactant(DSDMAC)-disulfine blue complex on the cotton fabric. Test methods for determining the amount of DSDMAC-disulfine blue complex on the cotton fabrics are measuring the reflectance of the colored fabric and the absorbance of the methanol solution of DSDMAC-disulfine blue complex extracted from dyed cotton fabric. Linear relationships between the K/S value of the fabric treated with DSDMAC followed by disulfine blue and the amount of DSDMAC sorbed by cotton fabric were obtained. Thus, the amount of DSDMAC sorbed by cotton fabric can be determined by K/S value of the fabric. DSDMAC-disulfine blue complex on the cotton fabric was extracted with methanol. The amount of DSDMAC sorbed by cotton fabric was estimated by measuring the absorbance of the methanol solution extracted from dyed cotton fabric.

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Oxygen-atom Transfer of Bis(pyrroridinedithiocarbamato)dioxomolybdenum (Ⅵ) with Triphenylphosphine in 1,2-Dichloroethane (1,2-디클로로에탄에서 트리페닐포스핀과 비스(피로리딘디티오카바마토) 디옥소몰리브덴 (Ⅵ) 착물의 산소이동 반응)

  • Kim, Chang Su;Song, Se Jun
    • Journal of the Korean Chemical Society
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    • v.34 no.2
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    • pp.171-178
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    • 1990
  • The rates of the reaction Of $[MoO_2(S_2CNC_4H_8)_2]$ with triphenylphosphine in 1,2-dichloroethane have been by the spectrophotometric method. The increase in absorbance at 514 nm has been interpreted as a result of production of $[Mo_2O_3(S_2CNC_4H_8)_4]$ and the decrease in absorbance then corresponds to the reduction of $[Mo_2O_3(S_2CNC_4H_8)_4]$. The data suggest mechanisms involving the formation of $\mu$-oxo dimer in the first stage and molybdenum(IV) in the second stage.

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Electrochemical Degradation of Phenol Using Dimensionally Stable Anode (촉매성 산화물 전극을 이용한 페놀의 전기화학적 분해)

  • Kim, Dong-Seog;Park, Young-Seek
    • Journal of Environmental Science International
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    • v.22 no.8
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    • pp.999-1007
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    • 2013
  • Electrochemical degradation of phenol was evaluated at DSA (dimensionally stable anode), JP202 (Ru, 25%; Ir, 25%; other, 50%) electrode for being a treatment method in non-biodegradable organic compounds such as phenol. Experiments were conducted to examine the effects of applied current (1.0~4.0 A), electrolyte type (NaCl, KCl, $Na_2SO_4$, $H_2SO_4$) and concentration (0.5~3.0 g/L), initial phenol concentration (12.5~100.0 mg/L) on phenol degradation and $UV_{254}$ absorbance as indirect indicator of by-product degraded phenol. It was found that phenol concentration decreased from around 50 mg/L to zero after 10 min of electrolysis with 2.5 g/L NaCl as supporting electrolyte at the current of 3.5 A. Although phenol could be completely electrochemical degraded by JP202 anode, the degradation of phenol COD was required oxidation time over 60 min due to the generation of by-products. $UV_{254}$ absorbance can see the impact of as an indirect indicator of the creation and destruction of by-product. The initial removal rate of phenol is 5.63 times faster than the initial COD removal rate.

The study of Phellodendron amurense Rupr. Dyeing (황벽의 염색성에 관한연구)

  • 소황옥
    • Journal of the Korean Society of Costume
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    • v.27
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    • pp.121-132
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    • 1996
  • This study showed the proper pigment extract in the Phe. Dyeing which is the basic dye of the natural plants dyeing,. Also it compared and examined the K/S the promotion of the color fastness and the effect of color difference change were attended by mordants and method of mordanting. 1. The most absorbance of Phellodendron. sol-ution is 330nm berberine is 430nm. 2. The best and proper temperature to extrat Phe,. was 80 and dyeing solution for 24 hours. 3. The pH effect was stable in the absorbances and color differences change. 4. Mordanted group increased the absorbances compared to non-mordanted sample. In case depth the most absorbance of Al. Sn. K. Cu and C. A solution were in 3% Fe and Cr were in 5%. In the color difference change they became dark reduced greenish and increased yellowish when their absorbances were in 3% 5. K./S was recoginzed by tainnin and fe, K/S was more increased pre-mordants than post-mordants. 6. Fe is the unchangable mordant in the color difference change and pre-mordants is more stable than post-mordants in the difference color. 7. Generally light C. F indicated more than grade 2 and light C. F, was much improved in post-mordanted by alumium potassium potass-ium dichromate. Washing C.F was improved in mordanted by tainnin and ferrous suulfate mordanted group was better than non-mordanted sample. Perspir-ation C,F was more stable in acid than alkali. Dry cleaning C.F indicated more than grade. 4.

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Preparation of Monodispersed $SiO_2/ZnO$ Composite Fine Powders by Sol-Gel Method (졸-겔법엔 의한 단분산 $SiO_2/ZnO$ 복합미립자의 졔조)

  • Lee, Chang-Woo;Shim, Won;Hahm, Yeong-Min;Hur, Yun-Haeng
    • Journal of environmental and Sanitary engineering
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    • v.13 no.3
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    • pp.58-65
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    • 1998
  • Monodispersed $SiO_2/ZnO$ composite fine powders were prepared by Sol-Gel processing and their surface electrical and UV absorbance properties were investigated. Pseudomorph ZnO fine powders were microcapsuled by $SiO_2/ZnO$ sol fabricated using TEOS[tetraethylorthosilicate, purity 98% and ethanol as a solvent with $NH_3$ catalyst. The effects of experimental parameters such as molar ratio of starting materials on the final particle size and shape of $SiO_2/ZnO$ composite fine powder were discussed. As a result, we could controlled the size of monodispersed $SiO_2/ZnO$ composite fine powders without agglomeration, as well as the good dispersibility in aquous solution. The prepared powders were observed to have the mean particle sizes of $0.26-0.78{\mu}m$ with standard deviations of $0.020-0.063{\mu}m$.

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Matrix Modification for Graphite Furnace Atomic Absorption Spectrophotometric Determination of Volatile Elements(III) Trace Bismuth

  • Kim, Young-Sang;Choi, Jong-Moon;Kim, Young-Man
    • Analytical Science and Technology
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    • v.8 no.4
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    • pp.435-442
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    • 1995
  • A matrix modification was studied for the determination of trace bismuth in water samples by graphite furnace atomic absorption spectrophotometry. The type and quantity of modifiers as well as the use of auxiliary modifiers were investigated to realize the efficient modification. Palladium was chosen as a single modifier. By the addition of palladium($5{\mu}g/mL$) to 100 ng/mL bismuth solution, the temperatures could be raised from $500^{\circ}C$ to $1,300^{\circ}C$ for the charring and from $2,000^{\circ}C$ to $2,200^{\circ}C$ for the atomization as well as the sensitivity and reproducibility were improved. The absorbance of bismuth was maximum and not changed in the range of Pd $3-25{\mu}g/mL$. And several materials were examined as an auxiliary modifier. The mixed solution of $1{\mu}g/mL$ palladium and $200{\mu}g/mL$ nickel have raised the temperatures as with $5{\mu}g/mL$ palladium only. The maximum absorbance of bismuth was shown in the nickel concentration range of $100-300{\mu}g/mL$ in $1{\mu}g/mL$ palladium modified system. With such optimum conditions, the trace amount of bismuth in several water samples could be determined by a calibration curve method, and good recoveries were also obtained.

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The Study of Cochineal Dyeing. (코치닐의 염색성에 관한 연구)

  • 주영주;소황옥
    • Textile Coloration and Finishing
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    • v.10 no.1
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    • pp.11-19
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    • 1998
  • For the purpose of standardization and practicability of dyeing by natural dyes, the mordanting and dyeing properties of cochineal and carminic acid were studied. Appropriate extraction, dyeing and mordanting condition of cochineal were determined, and the effect of mordanting method on dye uptake and color fastness of dyed fabric was investigated. The maximum absorbance of cochineal solution was 495nm, carminic acid was 533nm and 577nm. The color of carminic acid solution was affected by pH 6~9. The optimum temperature to extract cochineal was $80-100^\circ{C}$ and dyeing solution for 1 hour. And effective dyeing time to silk was 60min. Effective mordanting temperature was $80^\circ{C}$, and its time was 30min. In case mordants concentration, the maximum absorbance of Sn solution was 3%, K, Cu and Cr were in 1%. K/S value of dyeing fabrics was recoginazed by mordant treatment, specially Fe, Sn, Al, Cu. In the case of cochineal light fastness was increased by mordant treatment, specially Fe treatment. Perspiration fastness was good in acidic solution than in alkaline solution and perspiration fastness of cochineal was poor. Fastness of abrasion and dry-cleaning were good and these fastness improvement were generally effective for post-mordanting treatment.

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