• Title/Summary/Keyword: a-C:Ti

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Evaluation of the characteristics of plasma sprayed ceramic coatings by Indentation test (압입 시험에 의한 플라즈마 세라믹 용사코팅의 특성 평가)

  • Choi, Se-Young;Chae, Young-Hun;Kim, Seock-Sam
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2002.05a
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    • pp.248-254
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    • 2002
  • The most controversial topics in plasma sprayed ceramic coating system are recently mechanical properties such as bond strength, cohesive strength, toughness and so on. Determination of bond strength of coatings is one of the most important problems. In the industry, the bond strength of coating system has been estimated by Pull-off test(ASTM standard C633-79). But, without a fixed jig and specimen, it is impossible to obtain the bond strength. Therefore, it is necessary to study the critical fracture load on interface of the coating by indentation test. Because the critical fracture load plays an important role in evaluating the bond strength for plasma sprayed ceramic coating system. So, we have estimated critical fracture load in plasma sprayed ceramic coating system, and it was shown that inverse relationship between the cross-section hardness of coating and the critical fracture load(Pc). In case of the high load(1kgf, 2kgf) in $Al_{2}O_{3}+13%TiO_{2}$, it was found that the critical point(Pco), which the coating was broken on.

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Synthesis and Characterization of Al Film using N-methylpyrrolidine Alane (N-methylpyrrolidine Alane 전구체를 사용한 Al 필름 합성 및 특성 분석)

  • Seo, Moon-Kyu
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.22 no.7
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    • pp.549-554
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    • 2009
  • Al thin films were synthesized on TiN/Si substrate by MOCVD using N-methylpyrrolidine alane (MPA) precursor. Effects of substrate temperature, reaction pressure on the deposition rate, surface roughness and electrical resistivity were investigated. The early stage of Al thin film formation was analyzed by in-situ surface reflectivity measurement with a laser and photometer apparatus. From the Arrhenius plot of deposition rate vs. substrate temperature, it was found that the activation energy of surface reaction was 91.1kJ/mole, and the transition temperature from surface-reaction-limited region to mass-transfer-limited region was about $150^{\circ}C$. The growth rate increased with the reaction pressure, and average growth rates of $200{\sim}1,200nm/min$ were observed at various experimental conditions. Surface roughness of the film increased with the film thickness. The electrical resistivity of Al film was about $4{\mu}{\Omega}{\cdot}cm$ in the case of optimum condition, and it was close to the value of the bulk Al, $2.7{\mu}{\Omega}{\cdot}cm$.

Implementation of the Audio CODEC for Digital Audio Broadcasting Service (디지털 오디오 방송 서비스를 위한 오디오 코덱의 구현)

  • 장대영;홍진우
    • Journal of Broadcast Engineering
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    • v.6 no.1
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    • pp.66-71
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    • 2001
  • This paper Introduces an implementation of MPEG-2 AAC codec system for digital audio broadcasting. This system consists of the encoder and the decoder. This system includes MPEG-2 system multiplexing and demultiplexing modules for Interfacing to the ETRI-DAB system. Four DSPs are adopted for the encoder and three DSPs for 7he decoder. Each DSP Processes system control. 1/0 control, audio signal processing. multiplexing and demultiplexing. This Paper also discusses some near future estimations relaxed to the DAB system and it\`s services. Currently a stereo audio codec is available but multi-channel audio codec and MPEG-4 audio cosec wall be also Implemented.

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A Study on the Pharmacetical Characteristics and Analysis of Green-tea Extract (녹차 추출물의 약리적 특성 및 분석)

  • Sung, Ki-Chun
    • Journal of the Korean Applied Science and Technology
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    • v.23 no.2
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    • pp.115-124
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    • 2006
  • From the result of pharmacetical characteristics and analysis of Green-tea extract, it could obtain some conclusions as follows. The extract experiment of Green-tea appeared about 10%-extraction ratio as semi-solid state, and after dried in freezing from Green-tea extract of semi-solid state, it obtained about 65% Green-tea extract as solid state. In the results on antimicrobial experiment of Green-tea extract, number of S-typhimurium and fungus in microbe decreased more and more according to the time passage. This phenomenon could show that Green-tea extract keeps antimicrobial effect. In the results on antioxidation experiment of Green-tea extract, DPPH scavenging activity of free radical showed that Green-tea extract appears more remarkable reduction ability than reference samples. This phenomenon means that antioxidation of Green-tea extract appears higher than Vitamin-C and BHA sample. In the results on intrument analysis, the fatty and aromatic components of aniline, acetaldehyde, acetic acid, trichloroethylene, caffeine etcs from Green-tea extract was detected with GC/MS analysis and inorganic components of Ca, Mg, Cu, Mo, Sb, Ti etcs from Green-tea extract was detected with ICP/OES analysis.

Characterization of Hardenability and Mechanical Properties of B-Bearing Microalloyed Steels for Cold Forging (붕소함유 냉간단조용 비조질강의 경화능 및 기계적 특성평가)

  • Park H. G.;Nam N. G.;Choi H. G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2004.05a
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    • pp.395-399
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    • 2004
  • Four microalloyed steels containing B were investigated in terms of hardenability, mechanical properties and microstructure depending upon the cooling rates in order to develop the steel grade for the cold forged fasners. The alloy with the largest DI value among 4 alloys, which contains $0.12\%\;C,\;1.54\%\;Mn,\;0.65\%\;Cr,\;0.11\%V,\;0.040\%Ti\;and\;0.0033\%B$, showed the larest shift to the right hand side in the TTT diagram, implying the wide allowable cooling rate range subsequent to hot rolling in long bar processing, Mechanical tests indicated that yield strength are dependent upon the DI value in water quenched specimens but other properties showed almost the same values. In the same grade of steel, the increase in cooling rates causes the decrease in elongation but the increase in strength, reduction of area and Charpy impact values. Microstructural examination in steel grade with the larest DI values revealed martensitic structure In the water quenched state, a mixture of martensite and bainite in the oil quenched, and ferrite + pearlite in the air cooled and the forced air cooled but the latter showed finer microstructure.

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A Study on the Grinding of Titanium Alloy Part 1 : Grinding force, Specific grinding energy, Surface roughness, G-ratio (티타늄 합금의 연삭에 관한 연구 Part 1: 연삭력, 비연삭에저니, 표면거칠기 , 연삭비)

  • Kim, S. H.;Lim, J. G.;Ha, S. B.;Choi, H.;lee, J. C.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2000.11a
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    • pp.870-874
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    • 2000
  • This investigation reports the grinding characteristics of titanium alloy(Ti-6Al-4V). Grinding experiments were performed at various grinding conditions and the grinding forces and specific grinding energies were measured to investigate the grindability of titanium alloy with the three different wheels including Diamond, Green carbide and Alumina. To investigate the grinding characteristics of titanium alloy grinding force, force-ratio, specific grinding energy and grinding -ratio, were measured. Surface roughness was also measured with tracer and the ground surfaces were observed with SEM. Force-ratio of grinding of titanium alloy was very lower than that of grinding of SKD-11. Specific grinding energy are almost five times larger and rougher surface was obtained in titanium grinding.

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A study on the relationship of various characterizations for undoped ZnO thin films (Undoped ZnO 박막의 다양한 특성의 상관관계에 대한 연구)

  • Baek, Kyung-Hyun;Park, Hyeong-Sik;Jang, Kyung-Soo;Jung, Sung-Wook;Ryu, Kyung-Yul;Yun, Eui-Jung;Yi, J.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.147-147
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    • 2010
  • PTC Thermistors specimens were fabricated by added $MnO_2$ as donors, and $Nb_2O_5$ as acceptors and sintered $1250^{\circ}C$/2hrs. Average grain size decreased with increased in added $MnO_2$, and increased with added in $Nb_2O_5$. But, appeared liquid phase as $Bi_2O_3$ and $TiO_2$, affect to grain growth. XRD result, peak strength waslowed then crystallization not well, but, secondary phase were not showed all specimens. All specimens resistance were so high, about $40M{\Omega}$ over, couldn't measured to those resistance and doesn't appear PTCR effect.

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A Study on the Grinding of Titanium Alloy, Part2 : Grinding characteristics by using Superabrasives (티타늄 합금의 연삭에 관한 연구, Part2 : 초연마재를 사용한 연삭특성)

  • Kim, S. H.;Choi, H.;lee, J. C.;Cheong, S. H.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2001.04a
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    • pp.1076-1079
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    • 2001
  • This investigation reports the grinding characteristics of titanium alloy(Ti-6Al-4V). Grinding experiments were performed at various grinding conditions. The grinding forces and grinding force ratio were measured to investigate the grindability of titanium alloy with the Diamond and CBN wheel. To investigate the grinding characteristics of titanium alloy grinding force ratio and grinding ratio were measured. Surface profile of wheel was also measured with tracer and the ground surfaces and chip were observed with SEM. Grinding-ratio of titanium alloy was much lower than that of other materials. Grinding-ratio of titanium alloy with Diamond wheel was almost six times larger than that with CBN wheel.

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A Study on Development of Insert Metal for Liquid Phase Diffusion Bonding of Fe Base Heat Resistance Alloy (Fe 기내열합금의 액상확상접합용 삽입금속의 개발에 관한 연구)

  • 강정윤;김인배;이상래
    • Journal of Welding and Joining
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    • v.13 no.3
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    • pp.147-156
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    • 1995
  • The change of microstructure in the bonded interlayer and tensile properties of joints were studied for liquid phase diffusion bonding using STS-310 and Incoloy-825 as base metal and base metal+B alloy as insert inetal. Main experimental results obtained in this study are as follows. 1) The optimum amount of B addition into the insert metal was found to be about 4mass%. 2) When isothermal solidification was completed, the microstructure in the bonded interlayer was the same with that of the base metal because of the grain boundary migration in the bonded interlayer. 3) All of the tensile specimen fractured at base metal and joints bonded at optimum condition exhibited tensile properties in excess of base metal requirements. 4) It was determined that fine car-borides and bordes such as M$_{23}$(C,B)$_{6}$, Cr$_{2}$B, and CrB in STS-310S and TiB in Incoloy-825 exist at the grain boundary around bonded interlayer. These precipitates almost disappeared after homogenizing treatment at 1373K for 86.4ks.s.

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Structural and electrical properties of $V_{1.8}W_{0.2}O_5$ thin films with $Ar/O_2$ Ratio ($Ar/O_2$ 비에 따른 $V_{1.8}W_{0.2}O_5$ thin film 의 구조적, 유전적 특성)

  • Lee, Seung-Hwan;Park, In-Gil;Bae, Seon-Gi;Lee, Young-Hie
    • Proceedings of the KIEE Conference
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    • 2008.07a
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    • pp.1252-1253
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    • 2008
  • The $V_{1.8}W_{0.2}O_5$ thin films deposited on $Pt/Ti/SiO_2/Si$ substrates by RF sputtering method with different $Ar/O_2$ ratio. The $V_{1.8}W_{0.2}O_5$ thin films were measured electrical and structural properties, fairly good Temperature coefficient of resistance(TCR). It was found that electrical and structural properties, TCR properties of thin films were strongly dependent upon the $Ar/O_2$ ratio. The dielectric constant of the $V_{1.8}W_{0.2}O_5$ thin films with 50/20 ratio were 93 with a dielectric loss of 0.535, respectively. Also, the TCR values of the $V_{1.8}W_{0.2}O_5$ thin films with 50/20 ratio were -3.15%/$^{\circ}C$.

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