• 한국결정학회지
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• 제8권2호
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• pp.132-137
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• 1997

N,N'-di-tert-butoxycabonyl-2, 7-diazabicyclo[3.3.0]oct-4-ene의 분자 및 결정구조를 X-선 회절법으로 연구하였다. 이 결정의 분자식은 C16H26N2O4, 결정계는 삼사정계이고 공간군은 P1이다. 단위세포상수 a=11.119(1) Å, b=13.638(1) Å, c=6.214(1) Å이며, α=92.14(1)°, β=103.49(1)°, γ=73.35(1)°, V=877.4(2)Å3, T=293(2)K, Z=2이다. 구조해석에 사용한 X-선은 Cu Kα선(λ=1.5418Å)이다. 구조는 직접법으로 풀었으며, 최소자승법으로 정밀화하였다. 최종 신뢰도 R값은 F0>4σ(F0)인 2389개의 독립회절데이타에 대해 5.38%이였다.

• Elastomers and Composites
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• 제50권4호
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• pp.297-303
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• 2015

Ammonium polyphosphate-polyurethane foam composite (APP-PUF) was prepared from poly(adipate)diol/ammonium polyphosphate composite (f = 2), polyether polyol (f = 4.6), and PMDI (f = 2.5). As a blowing agent, $H_2O$ was used at various concentrations. The thermal decomposition behavior, morphology, closed-cell content, and density of APP-PUF were characterized. At the $H_2O$ concentrations lower than 3.5 php, the cell size of pure polyurethane foams (PUF) and APP-PUFs were close each other. As the $H_2O$ concentration became greater than 5.0 php, the cell size of the PUFs greatly increased compared to that of APP-PUFs. Addition of 1.5~1.9 wt% ammonium polyphosphate to the PUFs greatly enhanced the thermal stability of the PUFs, so 50 wt% residual temperature of APP-PUFs increased to $380{\sim}488^{\circ}C$, which were $30{\sim}70^{\circ}C$ higher than those of the PUFs. Thermal stability of the PUFs and APP-PUFs increased with $H_2O$ content and then decreased once $H_2O$ content exceeded 5 php.

• 한국표면공학회지
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• 제50권6호
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• pp.523-530
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• 2017

In this study, we developed the h-BN interphase for ceramic matrix composites (CMCs) through a wet chemical coating method, which has excellent price competitiveness and is a simple process as a departure from the existing high cost chemical vapor deposition method. The optimum condition for nitriding an h-BN interphase using boric acid and urea as precursors were derived, and the h-BN interphase coating through a wet method on a carbon preform of 2.5 D was conducted to apply the optimum conditions to the CMCs. In order to control the coating property via the wet coating method, four parameters were investigated such as dipping time of the specimen in the precursor solution, the ratio of boric acid and urea in the precursor, the concentration of solution where the precursor was dissolved, and the cycle of dipping and dry process. The CMCs was fabricated through polymer impregnation and pyrolysis (PIP) processes and a three-point flexural strength test was conducted to verify the role of the coated h-BN interphase.

• 한국결정학회지
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• 제3권1호
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• pp.31-36
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• 1992

플루오로시노론 아세토나이드, C24H30F2O6, 삼사 정계, 공간군 R3(육방정계 단위세포), a=b=17. 896 A., c: 18365 ,3,, V=5094.3 A',2:9 A(MoK a) =0.7107 k, D-: 1.31 g/cm", D.: 1.328 g/cm", T=298 K,1101 개의 독립된 회절반점에 대한 최종신뢰도값 R=0.050. 분자구조는 관련된 코티코 스테로이드 화합물의 구조와 일치한다. 3회 회전 대칭 관계에 있는 세개의 분자가 수소결합에 의해 서로 연결되어, c-축에수직한 층을 형성한다.

• 한국신뢰성학회지:신뢰성응용연구
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• 제16권3호
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• pp.171-179
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• 2016

Purpose: The purpose of this study is to provide a comparison of reliability prediction models between MIL-HDBK-217F and Telcordia SR-332 and to analyze the reliability prediction results. Methods: The reliability of industrial tablet PC was predicted using MIL-HDBK-217F and Telcordia SR-332. To analyze the results, sensitivity analysis was conducted. Results: The reliability of MIL-HDBK-217F was predicted lower than the one of Telcordia SR-332. Considering the factors such as temperature, quality and environment, those provided reliability change of a particular part which highly contribute to the system failure. Conclusion: It is necessary to design the industrial tablet PC that consists of integrated circuits such as microprocessor and memory considering the operating temperature and quality factors.

• 한국진공학회지
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• 제6권1호
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• pp.91-96
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• 1997

평면형 유도 결합 플라즈마의 전기적 특성을 측정하였고 Langmuir probe를 이용하 여 전자의 밀도와 온도를 측정하였다. 코일과 플라즈마를 포함한 총 부하의 저항 성분은 1 에서 4$\Omega$까지 변하였고 인덕턱스는 $1.5\mu$H와 2$\mu$H사이의 값을 가졌다. $10^{11}/\textrm{cm}^3$ 이상의 고밀 도 플라즈마를 발생시켰으며 전자의 온도는 공정 조건에 따라 3에서 5eV까지 변하였다. 산 화막 식각시 선택도를 개선하기 위한 방법으로 바이어스 전압을 변조하는 방법을 모색하였 다. C4F8플라즈마에서 바이어스 변조 방법을 사용하였을 때 선택도는 크게 향상 되었으나 산화막 식각율이 400$\AA$/min 이하였다. 선택도 향상을 위해 수소를 첨가한 실험에서 $C_4F_8$ 플 라즈마에 60% $H_2$를 첨가하였을 때 선택도 50이상, 산화막 식각율 2000$\AA$/min 이상의 결과 를 얻을 수 있었다.

• E2M - 전기 전자와 첨단 소재
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• 제8권3호
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• pp.324-331
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• 1995

0.36[wt%l $SiO_{2}$ and 0.1[wt%] $H_{3}$B $O_{3}$ were added to strontium ferrite magnets of the magnetoplumbite phase SrO.5.7F $e_{2}$ $O_{3}$ to hinder grain growth and accelerate sintering, respectively. This experiment was carried out to investigate effect of particle size distribution as a function of milling time(20, 30, 40, 50, 60, 70 hours) on the magnetic properties of SrO.5.7F $e_{2}$ $O_{3}$ ferrite magnet. The B-H curve, density and the degree of orientation were measured. And the microstructure of ferrite magnets was examined with a SEM. The optimal conditions and properties of the typical sample are the following : The milling time was 60 hours. Magnetic and physical properties are $B_{r}$=4, 000[G], $_{b}$ $H_{c}$=3, 330[Oe], (BH)max=3.786[MGOe], $_{I}$ $H_{c}$=3, 525[Oe], density=5.0063[g/c $m^{3}$] and orientation factor f=0.813.0.813.3.3.

• 대한수학회보
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• 제54권6호
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• pp.1969-1980
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• 2017

Let ${\Gamma}$ be a nonzero torsionless commutative cancellative monoid with quotient group ${\langle}{\Gamma}{\rangle}$, $R={\bigoplus}_{{\alpha}{\in}{\Gamma}}R_{\alpha}$ be a graded integral domain graded by ${\Gamma}$ such that $R_{{\alpha}}{\neq}\{0\}$ for all ${\alpha}{\in}{\Gamma},H$ be the set of nonzero homogeneous elements of R, C(f) be the ideal of R generated by the homogeneous components of $f{\in}R$, and $N(H)=\{f{\in}R{\mid}C(f)_v=R\}$. In this paper, we introduce the notion of graded t-almost Dedekind domains. We then show that R is a t-almost Dedekind domain if and only if R is a graded t-almost Dedekind domain and RH is a t-almost Dedekind domains. We also show that if $R=D[{\Gamma}]$ is the monoid domain of ${\Gamma}$ over an integral domain D, then R is a graded t-almost Dedekind domain if and only if D and ${\Gamma}$ are t-almost Dedekind, if and only if $R_{N(H)}$ is an almost Dedekind domain. In particular, if ${\langle}{\Gamma}{\rangle}$ isatisfies the ascending chain condition on its cyclic subgroups, then $R=D[{\Gamma}]$ is a t-almost Dedekind domain if and only if R is a graded t-almost Dedekind domain.

• 대한수학회지
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• 제47권6호
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• pp.1147-1165
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• 2010

In this paper we compare a torsion free sheaf F on $P^N$ and the free vector bundle $\oplus^n_{i=1}O_{P^N}(b_i)$ having same rank and splitting type. We show that the first one has always "less" global sections, while it has a higher second Chern class. In both cases bounds for the difference are found in terms of the maximal free subsheaves of F. As a consequence we obtain a direct, easy and more general proof of the "Horrocks' splitting criterion", also holding for torsion free sheaves, and lower bounds for the Chern classes $c_i$(F(t)) of twists of F, only depending on some numerical invariants of F. Especially, we prove for rank n torsion free sheaves on $P^N$, whose splitting type has no gap (i.e., $b_i{\geq}b_{i+1}{\geq}b_i-1$ 1 for every i = 1,$\ldots$,n-1), the following formula for the discriminant: $$\Delta(F):=2_{nc_2}-(n-1)c^2_1\geq-\frac{1}{12}n^2(n^2-1)$$. Finally in the case of rank n reflexive sheaves we obtain polynomial upper bounds for the absolute value of the higher Chern classes $c_3$(F(t)),$\ldots$,$c_n$(F(t)) for the dimension of the cohomology modules $H^iF(t)$ and for the Castelnuovo-Mumford regularity of F; these polynomial bounds only depend only on $c_1(F)$, $c_2(F)$, the splitting type of F and t.

• 한국자기학회지
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• 제7권2호
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• pp.90-96
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• 1997

ThM $n_{12}$ 구조를 갖는 NdF $e_{10.7}$ $Ti_{1.2}$M $o_{0.1}$의 미세구조 및 자기적 성질을 Mossbauer 분광법과 X-선 회절 분석 그리고 VSM으로 연구하였다. NdF $e_{10.7}$ $Ti_{1.2}$M $o_{0.1}$ 합금은 알곤 가스 분위기의 아크 ㅇ용해로에서 제조하였으며, X-선 회절 분석 결과 결정구조는 상온에서 tetragonal 구조를 갖고 있으며, 격자상수는 $a_{0}$ = 8.637 .angs. , $c_{0}$ = 4.807 .angs. 으로 결정하였다. Mossbauer spectrum을 13 K에서 800 K 까지 취하였으며, Curie 온도는 600 K로 결정하였다. Mossbauer spectrum 분석은 Curie 온도 이하의 온도에서는 Fe-site가 (8 $i_{1}$, 8 $i_{2}$, 8 $j_{2}$, 8 $j_{1}$, 8f)의 5 site로 나타났으며, 400 K 근처에서 .alpha. -Fe 상이 나타나기 시작하여 온도가 증가함에 따라서 점진적으로 증가하여 Curie 온도에서 20.7%의 .alpha. -Fe 상이 존재함을 알았다. 각 site에서의 초미세 자기장은 온도가 증가함에 따라 감소하였으며, 그 크기는 $H_{hf}$(8i)> $H_{hf}$(8j)> $H_{hf}$(8f) 임을 알았고 spin파 여기에 의한 T/ $T_{c}$<0.7 이하에서의 평균 초미세 자기장 $H_{hf}$(T)의 변화는 [ $H_{hf}$(T)- $H_{hf}$(0)]/ $H_{hf}$(0)=-0.34(T/ $T_{c}$)$^{3}$2/-0.14(T/ $T_{c}$)$^{5}$ 2/로 나타났다. 또한 원자간 결합력을 알 수 있는 Debye 온도는 .THETA. = 340 .+-. 5 K로 나타났다.ETA. = 340 .+-. 5 K로 나타났다.