• Title/Summary/Keyword: Z.-M. method

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Phyto-Sociological Study of Resource Plant in Mt. Daedun

  • Lee, Yoon-Won
    • Plant Resources
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    • v.2 no.2
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    • pp.113-126
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    • 1999
  • Through the research of tracheophytes type around Mt. Daedun, we are aiming at figuring out the habitat condition of useful resource plants by the classification of vegetation units and communities using the Z-M phyto-sociological method in the basis of the traits of species composition and by the analysis of vegetation and environment by way of coincidence method. Tracheophytes in our research sites was classifid into 117 family, 475 genus 797, species 102 variety,18 breed, in total to 917 kinds. The forest around Mt. Daedun district was classified into 6 communities, 12 groups, 2 sub-groups according to feature species group, differential species group and differential. Judging the result from the examination of community classification factors by the coincidence method, vegetation unit was decided by altitude and topography.

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Predicting Scour at Bridge Piers

  • Briaud, Jean-Louis
    • Proceedings of the Korean Geotechical Society Conference
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    • 1999.03a
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    • pp.3-46
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    • 1999
  • A new method called SRICOS is proposed to predict the scour depth z versus time t around a cylindrical bridge pier of diameter D founded in clay. The steps involved are ; 1. taking samples at the bridge pier site, 2. testing them in an Erosion Function Apparatus called the EFA to obtain the scour rate z versus the hydraulic shear stress applied $\tau$, 3. predicting the maximum shear stress r max which will be induced around the pier by the water flowing at ν Ο before the scour hole starts to develop, 4. using the measured z versus r curve to obtain the initial scour rate zi corresponding to r max , 5. predicting the maximum depth of scour zmax for the pier, 6. using zi and zmarx to develop the hyperbolic function describing the scour depth z versus time t curve, and 7. reading the z vs. t curve at a time corresponding to the duration of the flood to find the scour depth which will develop around the pier. A new apparatus is developed to measure the z vs t curve of step 2, a series of advanced numerical simulations are performed to develop an equation for the $\tau$ max value of step 3, and a series of flume tests are performed to develop an equation for the zmax value of step 5. The method is evaluated by comparing predictions and measurements in 42 flume experiments.

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Synthesis of Powder of the System Si-Al-O-N from Alkoxides II. Properties of Powders and Sintered Ceramics of Si3N4 and $\beta$-Sialon Prepared from Alkoxides (알콕사이드로부터 Si-Al-O-N계 분말합성 II. 알콕사이드로부터 합성한 Si3N4 및 $\beta$-Sialon의 분말 및 소결체의 특성)

  • 이홍림;전명철
    • Journal of the Korean Ceramic Society
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    • v.26 no.2
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    • pp.201-209
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    • 1989
  • Fine Si-Al-OH coprecipitate powders were prepared from Si- and Al-alkoxides by the hydrolysis method. $\beta$-Sialon powder was obtained from prepared Si-Al-OH coprecipitate by the simultaneous reduction and nitridation method. The syntehsized Sialon powder was pressureless sintered at 175$0^{\circ}C$ for 90 min in N2 atmosphere. The characterization of the Sialon powder was performed with XRD, BET, SEM, TEM and particle size analysis. The sinterability and mechanical properties of sintered bodies were investigated in terms of relative density, M.O.R., fracture toughness, hardness and the morphology of microstructure. The highest values of their mechanical properties were obtained for the $\beta$-Sialon ceramics at Z=1 and those values are as follows : M.O.R., KIC and HV of $\beta$-Sialon ceramics(Z=1) are 499.1 MPa, 5.9MN/m3/2 and 18.7GPa, respectively.

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Validation of LC-MS/MS Method for Determination of Rabeprazole in Human Plasma : Application of Pharmacokinetics Study (인체 혈장중 라베프라졸의 정량을 위한 LC-MS/MS 분석법 검증 및 단일 용량 투여에 의한 약물동태 연구)

  • Tak, Sung-Kwon;Seo, Ji-Hyung;Ryu, Ju-Hee;Choi, Sang-Joon;Lee, Myung-Jae;Kang, Jong-Min;Lee, Jin-Sung;Hong, Seung-Jae;Yim, Sung-Vin;Lee, Kyung-Tae
    • Journal of Pharmaceutical Investigation
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    • v.39 no.1
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    • pp.73-78
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    • 2009
  • A simple LC-MS/MS method of rabeprazole in human plasma was developed and validated. Rabeprazole and Internal standard (I.S), omeprazole, were extracted from human plasma by liquid liquid extraction, chromatographic separation of rabaprazole in plasma was achieved at $45^{\circ}C$ with a Shiseido UG120 $C_{18}$ column and methanol-10 mM ammonium acetate buffer (pH 9.42 with ammonium water), as mobile phase. Rabeprazole produced a protonated precursor ion [$(M+H)^+$] at m/z 360.10 and corresponding product ion at m/z 242.21. Internal standard produced a protonated precursor ion [$(M+H)^+$] at 346.09 and corresponding product ion at m/z 198.09. This method showed linear response over the concentration range of $1{\sim}500\;ng/mL$ with correalation coefficient greater than 0.99. The lower limit of quantitation (LLOQ) using 0.2 mL plasma was 1 ng/mL, which was sensitive enough for pharmacokinetics studies. The method was specific and validated with a limit of quantitation of 1 ng/mL. The intra-day and inter-day precision and accuracy were acceptable for all samples including the LLOQ. The applicability of the method was demonstrated by analysis of plasma after administration of a single 10 mg dose to 36 healthy subject. From the plasma rabeprazole concentration versus time curves, the mean $AUC_t$ (The area under the plasma concentration-time curve from time 0 to 12 hr ) was $691.36{\pm}321.88\;ng{\cdot}hr/mL$, $C_{max}$ (maximum plasma drug concentration) of $353.21{\pm}131.52\;ng/mL$ reached $3.4{\pm}1.1\;hr$ after adiministration. The mean biological half-life of rabeprazole was $1.37{\pm}0.75\;hr$. Based on the results, this simple method could readily be used in pharmacokinetics studies.

Analysis of Fluoroquinolone Antibiotics in Foods (식품 중 플루오로퀴놀론계 항생제의 분석)

  • Kim, Hee-Yun;Shin, Min-Su;Choi, Hee-Ju;Park, Se-Jong;Song, Jae-Sang;Cheong, So-Young;Choi, Sun-Hee;Lee, Hwa-Jeong;Kim, Young-Seon;Choi, Jae-Chun
    • Korean Journal of Food Science and Technology
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    • v.41 no.6
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    • pp.636-643
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    • 2009
  • Residual fluoroquinolone levels in animal foods retailed in Korea were monitored according to the method outlined in Korea Food Code using HPLC-FLD and HPLC-ESI-MS/MS for confirmation. The optimum ion transitions were $360{\rightarrow}316$, 342 m/z for enrofloxacin, $332{\rightarrow}314$, 288 m/z for ciprofloxacin, $320{\rightarrow}301$, 230 m/z for norfloxacin, $334{\rightarrow}315$, 290 m/z for pefloxacin, $362{\rightarrow}318$, 261, 334 m/z for ofloxacin, and $262{\rightarrow}201$, 126 m/z for flumequin. Enrofloxacin, ciprofloxacin and norfloxacin residues were found in 12 out of 388 samples. These antibiotics were only found in chicken samples, while no residues were found in beef, pork, milk and egg samples. Using this monitoring method, detection rates of 3.1, 1.3, and 0.3% were obtained for enrofloxacin, ciprofloxacin and norfloxacin, respectively. The levels of enrofloxacin, ciprofloxacin and norfloxacin detected in food samples ranged from 0.01 to 0.73 mg/kg in 12 samples, 0.01-0.03 mg/kg in 5 samples, and 0.12 mg/kg in only a sample, respectively.

THE EVOLUTION OF THE GALACTIC GLOBULAR CLUSTERS.: II. HELIUM ABUNDANCES AND AGES

  • Lee, See-Woo
    • Journal of The Korean Astronomical Society
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    • v.18 no.2
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    • pp.41-69
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    • 1985
  • For the well observed 16 globular clusters with known metal abundance (Z), the helium abundances (Y) and ages are determined by various methods, and the relations between Y, Z and age are examined. The luminosity $L_{RR}$ of RR Lyrae stars is known to be dependent of evolutionary models and pulsation theory in the sense that the pulsation theory and horizontal branch (HB) models yield the anticorrelation between $L_{RR}$ and Z whereas main sequence (MS) and red giant branch (RGB) models yield the direct correlation between them. Similarly the anticorrelation between Y and Z is obtained from the HB models and pulsation theory whereas the direct correlation between them is obtained when the RGB model is applied. The current evolutionary models yield the anticorrelation between Z and age of clusters whenever the direct correlation between Y and Z holds. However when the anticorrelation between Y and Z is applied for age determination, the similar age of clusters is obtained as shown by Sandage (1982b). The ages, which are determined by the fitting of C-M diagrams to isochrones in the ($M_v$, B-V)-plane, suggest the two different chemical enrichment processes, which could be accounted for by the disk-halo model for the chemical evolution of the Galaxy (Lee and Ann 1981). Also it is known that the R-method is very useful for Y-determination and the derived Y's show the increasing rate of $\frac{{\Delta}Y}{{\Delta}Z}{\simeq}0.5$ which is comparable to the observed value of $\frac{{\Delta}Y}{{\Delta}Z}{\simeq}0.3$ from HII regions and planetary nebulae by Peimbert and Torres-Peimbert (1976). In this case, the age-metallicity relation of globular clusters could be explained by the disk-halo model.

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Crystal and Block Structures of Hexagonal Ferrites (육방정 페라이트의 결정과 Block 구조)

  • Shin, Hyung-Sup
    • Journal of the Korean Ceramic Society
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    • v.49 no.3
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    • pp.205-215
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    • 2012
  • It has been studied the crystal and block structures of the hexagonal ferrites with M, W, Y and Z types prepared by various coprecipitation-oxidation method. The structures have been refined with a Rietveld analysis of the powder X-ray diffraction pattern with high precision ($R_{WP}$ <0.09, $R_I$ <0.03). The density difference between the S-blocks was proportioned to the cobalt contents in hexagonal ferrites, but that between the R or T-blocks was relatively small. Compared with the blocks and cation-oxygen polyhedra in BaM ($BaFe_{12}O_{19}$), those were bulky to the normal direction for the c-axis in $Co_2W$ ($BaCo_2Fe_{16}O_{27}$) and to the parallel direction for the c-axis in $Co_2Y$ ($Ba_2Co_2Fe_{12}O_{22}$) and $Co_2Z$ ($Ba_3Co_2Fe_{24}O_{41}$). The S-blocks of $Co_2W$, $Co_2Y$, and $Co_2Z$ were unstable and distorted. Because the T-block of $Co_2Z$ was unstable, the T-block was decomposed into the Ba-rich phase and $Co_2W$ at high temperatures above $1200^{\circ}C$. A standard powder X-ray diffraction pattern for $Co_2Z$ was proposed as well.

A Study on the Maneuverabilities of the Training ship M.S. A-RA (실습선 아라호(M.S. A-RA)의 조종성능에 관한 연구)

  • 안영화;박명호;최환문;정용진
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.37 no.4
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    • pp.275-284
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    • 2001
  • The for this study, turning circle tests and maneuvering indices were conducted to study and evaluate the maneuverabilities of the fishery training ship M.S. A-RA(G/T : 990tons). The results obtained were summarized as follows : 1. The advances of the starboard and port of the turning circle were measured based on the dumb card test method were 198m, 192m, the size of tactical diameters of them were 194m, 188m, respectively. 2. The advances at the starboard and port of the turning circles were measured according to the DGPS positioning obtained 196m, 194m, the size of tactical diameters of them were 194m, 190m, respectively. 3. The results were compared which came from the sizes of turning circle measured up with the dumb card test method during the trial test and from the size of turning circle measured according to the DGPS positioning. The advance of the turning circle measured at the time of the starboard turning according to the DGPS positioning was 1m longer than that of the trial test. And it was 21m shorter at the time of the port turning. 4. The rudder was steered at $35^{\circ}$ of rudder angle each starboard and port while the ship M.S. A-RA was advancing at full speed of 13 k't. The velocity of the ship was reduced to 7.8 k't at $180^{\circ}$ of turning angle and 6.0 k't at $360^{\circ}$ of turning angle and mean values of turning angular velocity of the port and starboard were $2.4^{\circ}$/sec and $2.3^{\circ}$/sec, respectively. 5. The Z test at each $10^{\circ}$, $20^{\circ}$, and $30^{\circ}$ of rudder angle was carried out to have the maneuvering indices K and T measured. K for the each rudder angle were 1.24, 1.45, and 1.65 while T for the each rudder angle were 0.33, 0.20, and 0.14. That is, K at the Z test at $30^{\circ}$ was greater than at the Z test of $10^{\circ}$ and $20^{\circ}$ while T at the $30^{\circ}$ Z test was less than at the Z test of $10^{\circ}$ and 20.

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Quantitative Measurement of Surfactant Protein B mRNA by Filter Hybridization (Filter Hybridization 방법에 의한 Surfactant Protein B mRNA의 정량측정)

  • Park, Sung-Soo;Lee, Dong-Hoo;Shin, Dong-Ho;Lee, Jung-Hee
    • Tuberculosis and Respiratory Diseases
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    • v.39 no.3
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    • pp.242-247
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    • 1992
  • Background: The ability to precisely measure specific mRNA levels by hybridization to complementary DNA probes is an important tool for analyzing the regulation of gene expression. Surfactant proteins have important roles in regulating surfactant metabolism as well as in determing its physical properties. Method: The complete coding regions for rat surfactant protein complementary DNA of surfactant protein B were subcloned into pGem 3Z or 4Z such that either antisense or sense transcripts were obtained by using SP 6 RNA polymerase. Surfactant protein B mRNA was measured by filter hybridization. Results: Equation of standard curve between counts per minute (Y) and surfactant protein B mRNA transcript input (X) was Y=2034.9 X+159.1. Correlation coefficient was 1.0. Couclusions: Filter hybridization assay is suited to situation when rapid, accurate quantitation of multiple samples is required.

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Isolation and Purification of Decursin and Decursinol Angelate in Angelica gigas Nakai (참당귀(Angelica gigas Nakai) 중 Decursin 및 Decursinol Angelate의 분리 및 정제)

  • Kim, Kang-Min;Jung, Jae-Yeon;Hwang, Sung-Woo;Kim, Myo-Jeong;Kang, Jae-Seon
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.38 no.5
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    • pp.653-656
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    • 2009
  • This paper is intended as an investigation of the method of extraction and the analysis by high-performance liquid chromatography mass spectroscopy of decursin and decursinol angelate in the dried root of Angelica gigas Nakai. The extracted decursin and decursinol angelate were the purity of >95% using 60% ethanol at $-20^{\circ}C$ for 12 hours by HPLC analysis. Decursin and decursinol angelate were efficiently isolated using recycling HPLC. The purity of isolated decursin and decursinol angelate was identified as 99.97 and 99.40% by HPLC analysis, respectively. The molecular weights of Decursin and decursinol angelate were also identified as m/z=329 ($[M+H]^+$) and m/z=351 ($[M+Na]^+$) by mass spectroscopy.