• Title/Summary/Keyword: X-ray permeability

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Developemtn of the external fixator for a bone fracture (골절치료용 체외고정기기 개발을 위한 연구)

  • 윤희열
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2000.04a
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    • pp.310-315
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    • 2000
  • In this paper, the problems of the external fixator that have developed for a distal radius fracture so far are analyzed, and accordingly, the characterizations, which must have a prototype, are arranged. C-Arm is used. This instrument makes it possible for the real play of the internal body by x-ray permeability. From this data, it is possible to induce important design factors. Finally, a basic mechanism, which has to be applied, is decided, and the Solid Edge program, which used a 3-D design tool, completes then total instrument design.

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Helium/Oxygen Atmospheric Pressure Plasma Treatment on Poly(ethylene terephthalate) and Poly(trimethylene terephthalate) Knitted Fabrics: Comparison of Low-stress Mechanical/Surface Chemical Properties

  • Hwang Yoon Joong;McCord Marian G.;Kang Bok Choon
    • Fibers and Polymers
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    • v.6 no.2
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    • pp.113-120
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    • 2005
  • Helium-oxygen plasma treatments were conducted to modify poly(trimethylene terephthalate) (PIT) and poly(ethylene terephthalate) (PET) warp knitted fabrics under atmospheric pressure. Lubricant and contamination removals by plasma etching effect were examined by weight loss $(\%)$ measurements and scanning electron microscopy (SEM) analysis. Surface oxidation by plasma treatments was revealed by x-ray photoelectron spectroscopy (XPS) analyses, resulting in formation of hydrophilic groups and moisture regain $(\%)$ enhancement. Low-stress mechanical properties (evaluated by Kawabata evaluation system) and bulk properties (air permeability and bust strength) were enhanced by plasma treatment. Increasing interfiber and interyarn frictions might play important roles in enhancing surface property changes by plasma etching effect, and then changing low-stress mechanical properties and bulk properties for both fabrics.

Preparation and Characterization of Biopolymer-Based Nanocomposite Films: Chitosan-Based Nanocomposite Films with Antimicrobial Activity

  • Rhim, Jong-Whan
    • 한국포장학회:학술대회논문집
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    • 2006.11a
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    • pp.54-73
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    • 2006
  • Four different types of chitosan-based nanocomposite films were prepared using a solvent casting method by incorporating with four types of nanoparticles, i.e., an unmodified montmorillonite (Na-MMT), an organically modified montmorillonite (Cloisite 30B), a Nano-silver, and a Ag-zeolite (Ag-Ion). X-ray diffraction patterns of the nanocomposite films indicated that a certain degree of intercalation was formed in the nanocomposite films, with the highest intercalation in the Na-MMT-incorporated films followed by films with Cloisite 30B and Ag-Ion. SEM micrographs showed that in all the nanocomposite films, except the Nanosilver-incorporated one, nanoparticles were dispersed homogeneously throughout the chitosan polymer matrix. Consequently, mechanical and barrier properties of chitosan films were affected through intercalation of nanoparticles, i.e., tensile strength (TS) increased by 7-16%, while water vapor permeability (WVP) decreased by 25-30% depending on the nanoparticle material tested. In addition, chitosan-based nanocomposite films, especially silver-containing ones, showed a promising range of antimicrobial activity.

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The Characteristics of Hetero Junction Using NiCuZn Ferrite and Dielectric for LTCC (LTCC를 위한 NiCuZn 페라이트계와 유전체의 이종접합의 특성)

  • Kim, Nam Hyun;Park, Hyun;Kim, Kyung Nam
    • Journal of the Korean institute of surface engineering
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    • v.45 no.5
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    • pp.188-192
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    • 2012
  • The hetero junction on dielectrics and ferrite for LTCC was prepared by using NiCuZn ferrite. The shrinkage behaviour of ferrite tapes in combination with a dielectric tape was investigated. The characteristics of NiCuZn ferrite were investigated using XRD (X-ray diffractometer), Dilatometer, FE-SEM (Field emission scanning electron microscope), EDS (Energy dispersive spectrometer). NiCuZn ferrite calcined at $700^{\circ}C$ had a good apparent density and initial permeability of magnetic properties. The shrinkage rate of the NCZF700 ferrite and dielectric material was similar. The multilayer revealed dense, uniform morphologies with excellent interface quality. Diffusion of hetero junction such as dielectric and ferrite was not occuring at $900^{\circ}C$.

Preparation of Carrageenan-based Antimicrobial Films Incorporated With Sulfur Nanoparticles

  • Saedi, Shahab;Shokri, Mastaneh;Rhim, Jong-Whan
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.26 no.3
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    • pp.125-131
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    • 2020
  • Carrageenan-based functional films were prepared by adding two different types of sulfur nanoparticles (SNP) synthesized from sodium thiosulfate (SNPSTS) and elemental sulfur (SNPES). The films were characterized using Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction spectroscopy (XRD), and thermal gravimetric analysis (TGA). Also, film properties such as UV-visible light transmittance, water contact angle (WCA), water vapor permeability (WVP), mechanical properties, and antibacterial activity were evaluated. SNPs were uniformly dispersed in the carrageenan matrix to form flexible films. The addition of SNP significantly increased the film properties such as water vapor barrier and surface hydrophobicity but did not affect the mechanical properties. The carrageenan/SNP composite film showed some antibacterial activity against foodborne pathogenic bacteria, L. monocytogenes and E. coli.

The Utilization of Pond Ash as Embankment and Backfill Material (매립된 석탄 혼합회의 성토재 및 뒤채움재로서의 활용에 관한 연구)

  • Kim, Dae-Hyeon;Ki, Wan-Seo;Kim, Sun-Hak
    • The Journal of Engineering Geology
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    • v.20 no.3
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    • pp.297-310
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    • 2010
  • This study represents basic research into the utilization of mixed ash (fly ash and bottom ash) from the ash pond of the Taean Thermal Power Plant as a construction material. We conducted physical and mechanical experiments on the mixed ash and examined its engineering characteristics in terms of its use as a material for road landfill and structure backfill. We evaluated the physical and chemical characteristics of the ash by performing tests to determine specific gravity, maximum and minimum density, liquid limit and plastic limit, grain size distribution, composition (by X-ray diffraction), and loss on ignition. We also evaluated the mechanical characteristics by testing for permeability, compaction, CBR, and tri-axial compression. The experiments on the mixed ash yielded a specific gravity of 2.18-2.20, dry density of $9.38-13.32\;kN/m^3$, modified CBR of 16.5%-21%, permeability coefficient of 1.32 to $1.89-10^{-4}cm/sec$, and drained friction angle of $36.43^{\circ}-41.39^{\circ}$. The physical and mechanical properties of the mixed ash do not meet the quality standards stipulated for road landfill and structure backfill materials. Mixed ash with a high content of fly ash failed to meet some of the quality standards. Therefore, in order to utilize the mixed ash as a material for road landfill and structure backfill, it is necessary to improve its properties by mixing with bottom ash.

Study on the Gas Permeation Behaviors of Surface Fluorinated Polysulfone Membranes (표면불소화 폴리설폰 막의 기체 투과거동에 관한 연구)

  • Kim, Dae-Hoon;Im, Hyeon-Soo;Kim, Min-Sung;Lee, Byung-Seong;Lee, Bo-Sung;Yoon, Seok-Won;Kim, Beom-Sik;Park, You-In;Cheong, Seong-Ihl;Rhim, Ji-Won
    • Polymer(Korea)
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    • v.33 no.6
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    • pp.537-543
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    • 2009
  • The direct fluorination of polymers is a heterogeneous reaction using the mixture of $F_2$ and inert gas. In general, the resulting fluorinated polymers have good barrier property chemical stability similar to those of the fluoro-polymers, and could be prepared from the simple process. In this study, the polysulfone dense films were surface fluorinated using the direct fluorination technique and gas permeability and selectivity of the prepared membranes were measured with varying both $F_2$ concentration and reaction time. The introduction of $F_2$ was confirmed by X-ray photoelectron spectroscopy (XPS), water contact angles, and atomic force microscopy (AFM). As the $F_2$ increased, the permeability decreased while the selectivities for $O_2$, $CO_2$, and He gases relative to $N_2$ increased.

Investigation on the Self-Healing Performance of Cement Mortar Incorporating Inorganic Expansive Additives (무기질계 팽창재가 포함된 시멘트 모르타르의 자기치유성능에 관한 연구)

  • Shin, Jin-Wook;Her, Sung-Wun;Bae, Sung-Chul
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.8 no.4
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    • pp.404-412
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    • 2020
  • Herein, the properties and self-healing performance of cement mortar incorporating calcium sulfoaluminate(CSA), crystalline admixture(CA), and magnesium oxide(MgO) were investigated. Mortar strength test and water permeability experiments were conducted to analyze self-healing performance of the mortar. Also, variation in crack width were measured via digital optical microscope observation. The hydration products formed in the crack via self-healing were analyzed using x-ray diffraction(XRD), thermogravimetry(TG), and digital optical microscope. The analysis revealed that compressive strength and tensile strength increased as CA substitutional ratio increased. However, in the case of MgO replacement, the compressive strength and tensile strength decreased as the CA substitution ratio increased. The products in the recovered cracks are found to be mostly Ca(OH)2, MgCO3, and CaCO3. CaCO3 was shown to be the main healing product and had a higher portion than Ca(OH)2 and MgCO3 in the recovery products. Moreover, the optimal mix derived via water permeability and crack width results was 8% CSA + 1% CA + 2.5% MgO.

Characterization of Rockfish Skin Gelatin Composite Films (우럭 껍질 젤라틴 복합필름의 특성)

  • Beak, Song-Ee;Kim, Hyeri;Song, Kyung Bin
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.46 no.3
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    • pp.394-399
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    • 2017
  • To resolve environmental pollution caused by synthetic packaging materials, biodegradable films have been studied as an alternative. In this study, we prepared rockfish skin gelatin (RFG) and nano-clay (Cloisite $Na^+$ and Cloisite 10A) composite films to compare the effects of nano-clay on the physical properties of RFG film. Gelatin was extracted from rockfish skin and used to prepare RFG film with sorbitol as a plasticizer. Tensile strength (TS), water vapor permeability (WVP), and water solubility (WS) of the RFG film were 15.0 MPa, $2.70{\times}10^{-9}g\;m/m^2\;s\;Pa$, and 53.8%, respectively. Addition of nano-clay to the RFG film increased TS and decreased WVP and WS. The X-ray diffraction analysis and scanning electron microscopic results suggest that RFG/nano-clay composite films formed an exfoliated structure. These results indicate that RFG/nano-clay composite films can be applied as biodegradable packaging materials in the food industry.

Characteristics of composite membranes containing ionic liquid and acid for anhydrous high temperature PEFCs (무가습 고온 PEFC용 이온성 액체 및 산이 함유된 복합막의 특성)

  • Baek, Ji-Suk;Park, Jin-Soo;Park, Seung-Hee;Yang, Tae-Hyun;Park, Gu-Gon;Yim, Sung-Dae;Kim, Chang-Soo;Shul, Young-Gun
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.06a
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    • pp.378-378
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    • 2009
  • The ionic liquid-based sulfonated hydrocarbon composite membranes was prepared for use in anhydrous high temperature-polymer electrolyte fuel cells (HT-PEFCs). Ionic liquid behaves like water in the composite membranes under anhydrous condition. However the composite membranes show a low conductivity and high gas permeability as the content of ionic liquid increases due to its high viscosity and content of ionic liquid, respectively. Hence, in order to enhance the proton conductivity and to reduce the gas permeability of the composite membranes with low content of ionic liquids, the acid containing a common ion of ionic liquid was added to the composite membranes. The characterization of composite membranes was carried out using small-angle X-ray scattering (SAXS), thermogravimetric analyzer (TGA) and impedance spectroscopy. As a result, the composite membranes containing acid showed higher proton conductivity than those with no acid under the un-humidified condition due to a decrease in viscosity. In addition, the proton conductivity of composite membranes increased with increasing mole concentration of acid.

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