• Title/Summary/Keyword: X-ray measurement

검색결과 1,305건 처리시간 0.035초

광/엑스선 복합간섭계를 이용한 나노미터 영역의 변위 측정 및 trnasducer의 비선형 교정 (Displacement measurement in nanometer region and calibration of transducers using combined optical and x-ray interferometer)

  • 박진원;조재근;변상호;엄천일
    • 한국정밀공학회:학술대회논문집
    • /
    • 한국정밀공학회 2005년도 춘계학술대회 논문집
    • /
    • pp.515-518
    • /
    • 2005
  • 현재 정밀한 길이를 측정하기 위해서는 광 간섭계를 이용한 측정기술이 주로 사용되어지고 있다. 이러한 광 간섭계의 발전과 더불어 이보다 더 높은 분해능을 얻기 위해 광파장보다 1000배 정도 짧은 엑스선을 이용한 변위 측정 기술개발이 진행되고 있다. 본 연구에서는 이러한 엑스선을 이용한 간섭계를 제작하고, 광 간섭계와 결합된 광/엑스선 복합간섭계를 구성하여 광 간섭계가 안고 있는 자체의 비선형성이 제거된 정밀 변위 측정 시스템을 구성하였다. 그 응용으로써, 제작된 광/엑스선 복합간섭계를 이용하여 나노미터 영역에 서 사용하는 transducer의 비선형성을 측정하였다.

  • PDF

Synthesis and Characterization of Tungsten Trioxide Films Prepared by a Sol-Gel Method for Electrochromic Applications

  • Kim, Tae-Ho;Nah, Yoon-Chae
    • 한국분말재료학회지
    • /
    • 제22권5호
    • /
    • pp.309-314
    • /
    • 2015
  • Tungsten trioxide thin films are successfully synthesized by a sol-gel method using tungsten hexachloride as precursors. The structural, chemical, and optical properties of the prepared films are characterized by scanning electron microscopy, X-ray diffraction, X-ray photoelectron spectroscopy, and UV-Vis spectrophotometry. The electrochemical and electrochromic properties of the films before and after heat treatment are also investigated by cyclic voltammetry, chronoamperometry, and in situ transmittance measurement system. Compared to as-prepared films, heat-treated tungsten trioxide thin films exhibit a higher electrochemical reversibility of 0.81 and superior coloration efficiency of $65.7cm^2/C$, which implies that heat treatment at an appropriate temperature is a crucial process in a sol-gel method for having a better electrochromic performance.

FCVA 방법으로 증착된 다이아몬드상 탄소 박막의 XPS 및 XRR 특성 연구 (A Study on XPS and XRR Characteristics of DLC films Deposited by FCVA Method)

  • 박창균;장석모;엄현석;서수형;박진석
    • 대한전기학회논문지:전기물성ㆍ응용부문C
    • /
    • 제52권3호
    • /
    • pp.109-115
    • /
    • 2003
  • Diamond-like carbon (DLC) films are deposited at room temperature using a filtered cathodic vacuum arc (FCVA) technique. The influence of negative bias voltage (applied to the substrate from 0 to -250V) on the $sp^3$ hybridized carbon fraction is examined by Raman spectroscopy and x-ray photoelectron spectroscopy (XPS) for C 1s core peak. For the first time, depth profile of C 1s, Si 2p, and O 1s XPS peaks for the deposited DLC film are obtained. DLC film is modeled as a multilayered structure. composing of surface, bulk, and interface. In addition, the x-ray reflectivity (XRR) is proposed as a method for estimating the density, surface roughness, and thickness of each layer constituting the DLC film. The estimated thickness of DLC film is in good agreement with the result obtained from the transmission electron microscope (TEM) measurement.

In-situ Synchrotron X-ray Diffraction Measurement of Epitaxial FeRh thin Films

  • Jang, Sung-Uk;Hyun, Seung-Min;Lee, Hwan-Soo;Kwon, Soon-Ju;Kim, Ji-Hong;Park, Ki-Hoon;Lee, Hak-Joo
    • 한국자기학회:학술대회 개요집
    • /
    • 한국자기학회 2009년도 정기총회 및 동계학술연구발표회
    • /
    • pp.204-205
    • /
    • 2009
  • The magnetic properties and structure of FeRh thin film pitaxially grown onto MgO(001) substrate were studied by MPMS(Magnetic Properties Measure System) and in-situ temperature synchrotron XRD(X-ray Diffraction). The transition temperature of FeRh thin films was around 380K. Both M-T curve and d-spacing changes correspond to each other very closely.

  • PDF

근접장 마이크로파 현미경을 이용한 ITO 박막 면저항의 비파괴 관측 특성 연구 (Nondestructive measurement of sheet resistance of indium tin oxide(ITO) thin films by using a near-field scanning microwave microscope)

  • 윤순일;나승욱;윤영운;유현준;이영주;김현정;이기진
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2004년도 추계학술대회 논문집 Vol.17
    • /
    • pp.522-525
    • /
    • 2004
  • ITO thin films $({\sim}150\;nm)$ are deposited on glass substrates by different deposition condition. The sheet resistance of ITO thin films measured by using a four probe station. The microstructure of these films is determined using a X-ray diffractometer (XRD) and a scanning electron microscope (SEM) and a atomic force microscope (AFM). The sheet resistance of ITO thin films compared $s_{11}$ values by using a near field scanning microwave microscope.

  • PDF

전자장치용 Passivation 유리의 결정화에 관한 연구 (Crystallization of Passivation Glass for Electronic Devices)

  • 손명모;박희찬;이헌수
    • 한국세라믹학회지
    • /
    • 제30권2호
    • /
    • pp.107-114
    • /
    • 1993
  • Zinc-Borosilicate(ZnO 65.0wt%, B2O3 21.5wt%, SiO2 9.0wt%, PbO or tiO2 4wt%) passivation glasses were studied using differential thermal analysis(DTA), scanning electron microscopy(SEM) observations, X-ray diffraction (XRD) patterns and measurement of thermal expansion coefficients. Passivation glasses containing 4wt% TiO2 and 4wt% PbO had crystallization temperature of 680~73$0^{\circ}C$ and major crystalline phases were identified by X-ray diffraction as $\alpha$-ZnO.B2O3 and $\alpha$-5ZnO.2B2O3. As increasing firing temperature, the size of crystalline phases increased by observation of SEM. The thermal expansion coefficient of crystallized glass frits was smaller than that of unfired glass.

  • PDF

함평, 교촌 점토의 특성과 점토-유기물 복합체에 관한 연구 (Hampyong, Kyochon Clay-Its Characteristics and the Effects of Clay-organic Complexes on its.)

  • 정창주;백용혁;박현수
    • 한국세라믹학회지
    • /
    • 제14권2호
    • /
    • pp.95-103
    • /
    • 1977
  • Characteristics of Ham Pyong clay and clay-organic complexes were investigated by means of geological exploration, chemical analysis, X-ray diffraction, differential thermal analysis, electron microscopy, thermal mechanical analysis, cation exchange capacity and viscosity measurement. The results are as follows; 1) This caly is a transported clay which has black and white colors, and the amounts of deposit are estimated about 1, 600, 000M/T. 2) The major mineral phases identified by X-ray diffraction are kaolinite, sericite and halloysite and the minor phases are quartz and feldspar, these mineral phases can be seperated very easily by the elutriation method. 3) It was supposed that the black colored clay involved a certain clay-organic complexs by the mechanism of intercalation as well as surface absorption. 4) The clay-organic complexes in clay seemed to improve dispersity, to increase the fluidity of clay-water slips, to decrease the firing shrinkage and to promote the thermo-chemical reaction at temperature range up to 50$0^{\circ}C$, but not to effect on the resulted firing color.

  • PDF

Dose Estimation of Patient by X-ray Positioning in Particle Cancer Therapy

  • Hirai, Masaaki;Nishizawa, Kanae;Shibayama, Kouichi;Kanai, Tatsuaki
    • 한국의학물리학회:학술대회논문집
    • /
    • 한국의학물리학회 2002년도 Proceedings
    • /
    • pp.206-207
    • /
    • 2002
  • The effective dose due to the X-Ray radiography in the patient positioning for the heavy ion radiotherapy was measured on three regions, chest, upper-abdomen and pelvis. All the radiographic systems and the conditions used in the measurements were same as the clinical trial being performed in National Institute of Radiological Sciences, Japan. The organ or tissue for measurements was selected by following ICRP60$^1$ and the effective dose was calculated from measured organ doses and the surface dose.

  • PDF

Weak Lensing Analysis On The Merging Galaxy Cluster Abell 115

  • Kim, Mincheol;Jee, Myungkook J.
    • 천문학회보
    • /
    • 제42권1호
    • /
    • pp.51.1-51.1
    • /
    • 2017
  • The galaxy cluster Abell 115 shows ongoing merger features, which suggest that it might be in an intermediate phase of dynamical evolution. As merging clusters often show, the characteristic hints of A115's merging activities include radio relics, double X-ray peaks, and large offsets between the cluster member galaxies and the X-ray distributions. To constrain the exact stage of the merger, it is necessary to obtain its dark matter distribution. In this study, we carry out a precision weak lensing study of this interesting system based on Subaru images. We present our mass reconstruction together with descriptions on our core procedure of the analysis: Subaru data reduction, galaxy shape measurement, and source selection. We find that Abell 115 consists of two massive dark matter clumps, which closely follow the cluster galaxies. Our weak lensing mass estimate is a few factors lower than the published dynamical mass obtained from velocity dispersion. This large mass discrepancy may be attributed to a significant departure from dynamical equilibrium.

  • PDF

Study on visible emission of Cu-ion-doped perovskite hafnate in view of excitation energy dependence

  • Lee, D.J.;Lee, Y.S.;Noh, H.J.
    • 한국초전도ㆍ저온공학회논문지
    • /
    • 제17권4호
    • /
    • pp.8-11
    • /
    • 2015
  • We studied on the visible emission of Cu-ion-doped perovskite hafnate $SrHfO_3$ (SHO:Cu) with the photo-excitation energy dependence. The polycrystalline SHO:Cu samples were newly synthesized in the solid state reaction method. From the X-ray diffraction measurement it was found that the crystalline structure of SHO:Cu is nearly identical to that of undoped $SrHfO_3$. Interestingly, the photoluminescence excitation (PLE) spectra change significantly with the emission energy, which is linked to the strong dependence of the visible emission on the photo-excitation energy. This unusual emission behavior is likely to be associated with the mixed valence states of the doped Cu ions, which were revealed by X-ray photoelectron spectroscopy. We compared our finding of tunable visible emission in the SHO:Cu compounds with the cases of similar materials, $SrTiO_3$ and $SrZrO_3$ with Cu-ion-doping.