• 한국결정학회지
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• 제8권1호
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• pp.20-25
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• 1997

고분해도의 X-선 산란을 위해 두 실험 방법이 개발됐다. 그 방법들은 (1) 2-결정 회절 스펙트로메터 (DCD)설치와 (2) 3-결정 회절 스펙트로메터 (TCD) 설치였다. Si(511)-시료(hkl)의 DCD배열로 Si(333), Si(004), GaAs(004)의 rocking curve를 그렸다. 또한 단일체 단색 평행기와 $K_{\alpha1}$ 선택기를 포함하는 Si(111)-Si(111)-Si(511)-sample(hkl)의 TCD배열로 Si(333), Si(004) 그리고 GaAs(004)의 rocking curve를 그렸다. DCD와 TCD에 의한 rocking curve의 FWHM의 차이가 논의됐다. DCD에 의한 $In_{0.037}Ga_{0.0963}As/GaAs$의 (004) 및 (115) 반사 토포그라프가 행해졌다.

• Tribology and Lubricants
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• 제20권1호
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• pp.7-13
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• 2004

High strength steels are widely used as tribo-materials in the field. Previous study revealed that for mild steel, the states of strain on the worn surface measured by X-ray diffraction has a good relationship with the state of wear. The objective of this study is to identify the relationship between the state of strain on the worn surface and the state of wear in high strength steels. Sliding wear tests were carried out using several hardened steels. X-ray diffraction tests were conducted to analyze the state of strain on the worn surface during wear. The experimental results indicated that the state of strain on worn surface in the hardened steel shows the same tendency as in the mild steel. It is clear that change of half value width on the worn surface as a function of sliding speeds is broadly similar in shape to wear characteristics curve and its magnitude has a good relationship with the wear rate at two different wear modes in the hardened steel.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2000년도 봄 학술발표회 논문집
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• pp.159-162
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• 2000

The purpose of this study is to develope an accurate procedure for measuring the glass content of fly ash produced by bituminous coal to assist in predicting their behavior in concrete. Quantitative mineralogical compositions of fly ashes were obtained by internal standard method using powder X-ray diffraction analysis. In the X-ray diffraction method, the specimen and standard fluorite were cautiously mixed and pulverized to 22$\mu$m in wet process so as to avoid the prefered orientation of the crystal and microabsorption effect of X-ray. calibration curve were fitted for several references peaks of four phases:$\alpha$-quartz. mullite, magnetite, hematite. The amount of glass was calculated by subtracting the amount of crystal phase and loss on ignition from the total amount. Glass content determined with this method ranged from 66.7 to 75.wt%.

• 한국정밀공학회지
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• 제25권7호
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• pp.116-123
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• 2008

In the fossil power plant, the reliability of the components which consist of the many welded parts depends on the quality of welding. The residual stress is occurred by the heat flux of high temperature during weld process. This decreases the mechanical properties as the strength of fatigue and fracture or causes the stress corrosion cracking and fatigue fracture. Especially, the accidents due to the residual stress occurred at the weld parts of high-temperature and high-pressure pipes and steam headers. Also, the residual stress of the welded part in the recently constructed power plants has been brought into relief as the cause of various accidents. The aim of this study is the measurement of the residual stress using the x-ray diffraction method. The merits of this are more accurate and applicable than other methods. The materials used for the study is P92 steel for the use of high temperature pipe on super critical condition. The variables of tests are the post-weld heat treatment, the surface roughness and the depth from the original surface. The test results were analyzed by the distributed characteristics of the full width at half maximum intensity (FWHM) in x-ray diffraction intensity curve and by the relation of hardness with FWHM.

• E2M - 전기 전자와 첨단 소재
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• 제9권10호
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• pp.1013-1018
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• 1996

The annealing effects of Au/Te/Au/n-GaAs structure was investigated by using x-ray diffraction, scanning electron microscope, the specific contact resistance and I-V measurement. Increasing the annealing temperature, the intensity of Au-Ga peak by X-ray diffraction was increased. The Ga$\_$2/Te$\_$3/peak got evident for the samples annealed at 400.deg. C and GaAs peak by recrystallization appeared for the samples annealed at 500.deg. C. The variation from the schottky to low resistance contact was confirmed by I-V curve. The lowest value of the specific contact resistance of the samples annealed at 500.deg. C was 3.8*10$\^$-5/.ohm.-cm$\^$2/ but the value increased above 600.deg. C.

• 분석과학
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• 제25권1호
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• pp.33-38
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• 2012

염화물 고정화능력의 중요성에도 불구하고 고정화능력을 측정하는 것은 어려우며 특히, 이미 건설되어 공용중인 구조물에서는 더욱 어렵다. 실제로 고정염화물을 측정하는 과정은 온도, 시료의 분말도, 공극수 추출기법 등과 같은 환경적 요인에 의해 큰 영향을 받는다. 본 연구에서는 X-선 회절분석법(XRD; X-ray diffraction)을 이용하여 콘크리트 내 염화물 이온의 고정화능력을 정량화하는 방법에 대해 중점을 두고 연구를 진행하였다. 염화물의 고정능력 isotherm은 물/시멘트비, 양생기간, 결합재 종류에 영향을 받으며 Langmuir isotherm 을 통하여 일단 결정된 고정염화물(Friedel 염)은 XRD를 이용하여 동시에 분석을 진행한다. XRD 그래프에서 나타난 고정염화물량의 피크 강도와 측정된 고정염화물의 총량의 관계를 결정한다. 결과적으로 양생기간이 증가될수록, 물/시멘트비가 감소될수록 고정화 능력은 증가하였다.

• The Korean Journal of Ceramics
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• 제4권4호
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• pp.394-398
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• 1998

$Pb_{1-x}Sr_x(Mg-{1}2}W_{1}2})O_3$$ ceramics for application in the microwave frequency range were investigated by dielectric constant and X-ray diffraction measurements. The dielectric constant curves showed two concentration dependent characteristics in the $$Pb(Mg-{1}2}W_{1}2})O_3$-rich$ region. As the Sr constant further increases to x=0.3 the dielectric curve levels off. In the concentration range between x=0.4 and x=1 in which dielectric constant dependence on temperature is negligible, it decreases and Qf value increases in the microwave frequency with increasing Sr. The temperature coefficient (${\tau}_{\varepsilon} $) of the dielectric constant changes from the negative to positive value between x=0.9 and x=1. The dielectric constant, Qf and $\tau\varepsilon$ are correlated with tolerance factor(t). From the X-ray diffraction results for $0.1{\le}x{\le}1$ the cell parameter is found to decrease as x increases and B-site ordering is observed in all the composition ranges.

• 한국결정성장학회지
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• 제26권2호
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• pp.58-61
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• 2016

Basic 암모노써멀 방법을 사용하여 벌크 GaN 단결정을 성장시켰다. 종자 결정은 Hydride vapor phase epitaxy법으로 성장한 c면의 GaN 템플릿을 사용하고 광화제는 sodium metal, amide, azide를 사용하였다. 결정 성장 온도는 $500{\sim}600^{\circ}C$, 성장 압력은 2~3 kabr에서 실시하였다. c 축의 결정 성장 속도는 운용 압력이 증가함에 따라 선형적으로 증가하였다. Cathodoluminescence로 측정한 평균 전위 밀도는 $1{\times}10^5/cm^2$였다. Double Crystals X-ray Diffraction로 측정한 (002)면의 반치폭은 Ga 면에 대해서는 약 270 arcsec, N 면에 대해서는 약 80 arcsec이었다.

• 한국자기학회:학술대회 개요집
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• 한국자기학회 2009년도 정기총회 및 동계학술연구발표회
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• pp.204-205
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• 2009

The magnetic properties and structure of FeRh thin film pitaxially grown onto MgO(001) substrate were studied by MPMS(Magnetic Properties Measure System) and in-situ temperature synchrotron XRD(X-ray Diffraction). The transition temperature of FeRh thin films was around 380K. Both M-T curve and d-spacing changes correspond to each other very closely.

• Archives of Pharmacal Research
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• 제9권1호
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• pp.55-61
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• 1986

To increase the dissolution rate of piroxicam, chitin and chitosan which are widely occurring biodegradable natural materials were used as drug carriers. The ground mixtures of piroxicam with chitin or chitosan were prepared by grinding in a ball mill. The dissolution rates of piroxicam from the ground mixtures were enhanced markedly than that from the physical mixtures or from intact piroxicam. The X-ray diffraction peaks disappeared in the ground mixture indicating the production of the amorphous form. The comparison of infrared spectra of the physical mixture and the ground minture showed an interaction such as association between the functional groups of piroxicam and chitin or chitosan in the molecular level. The weight losses in TGA curves shoed all the same patterns. However, in the ground mixture by DTA curve, the undothermic peak due to the fusion of piroxicam was disappeared indicating the different thermal property.