• Title/Summary/Keyword: X-ray 분석

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Phase identification and degree of orientation measurements far fine-grained rock forming minerals using micro-area X-ray diffractometer -$Al_{2}SiO_{5}$ Polymorphs- (미소부 X-선 회절분석기를 이용한 미립조암광물의 상동정 및 배향도 측정 -$Al_{2}SiO_{5}$ 3상다형-)

  • 박찬수;김형식
    • The Journal of the Petrological Society of Korea
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    • v.9 no.4
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    • pp.205-210
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    • 2000
  • Measurements of phase identification and degree of orientation for fine-grained (about 0.3 mm in diameter) minerals in rock samples performed by micro-area X-ray diffractometer.$Al_{2}SiO_{5}$ polymorphs (andalusite, kyanite and sillimanite) were chosen for the measurements and target minerals were existed on thin sections. Micro-area X-ray diffractometer is composed of 3(${\omega}\;{\chi}\;{\phi}$)-circle oscillating goniometer and position sensitive proportional counter (PSPC). $CuK_{\alpha}$ radiation was used as X-ray source and a pin hole ($50\;\mu\textrm{m}$$ in diameter) collimator was selected to focus radiation X-ray onto the target minerals. Phase identification and diffracted X-ray peak indexing were carried out by 3(${\omega}\;{\chi}\;{\phi}$)-circle oscillation measurement. Then, 2(${\omega}\;{\phi}$)-circle oscillation measurement was made for the purpose of searching the prevailing lattice plane of the minerals on thin section surface. Finally, for a selected peak by 2-circle oscillation measurement, X-ray pole figure measurement was executed for the purpose of check the degree of orientation of the single lattice direction and examine its pole distribution. As a result of 3-circle oscillation measurement, it was possible that phase identification among $Al_{2}SiO_{5}$ polymorphs. And from the results of 2-circle oscillation measurement and X-ray pole figure measurement, we recognized that poles of andalusite (122), kyanite (200) and sillimanite (310) lattice plances were well developed with direction normal to each mineral surface plane respectively. Therfore, the measurements used with micro-area X-ray diffractometer in this study will be a useful tool of phase identification and degree of orientation measurement for fine-grained rock forming minerals.

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The Measurement and Evaluation of X-ray Characteristics of Cadmium Sulfide as a Multi-function Dosimeter (다기능 선량계로서의 Cadmium sulfide의 X-선에 대한 특성 평가)

  • Park, Sung-Kwang;Park, Young-Min;Cho, Heung-Lae;Nam, Sang-Hee
    • Progress in Medical Physics
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    • v.14 no.3
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    • pp.161-166
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    • 2003
  • To evaluate the performance of cadmium sulfide as a multi-function X-ray dosimeter, we made an X-ray detector that was based on cadmium sulfide using evaporation technology, and measured its response to X-ray exposure. The voltages of cadmium sulfide were measured on the various X-ray tube potentials, X-ray tube currents and exposure times. The regression analysis of the voltage response of CdS on the tube-potential variation was y=0.0995x-0.1146 ($R^2$=0.9595, $\sigma$=0.08, standard error=2%) and the regression analysis of the voltage response of CdS on the tube-potential variation was y=0.0439x+1.1891 ($R^2$=0.9021, $\sigma$=0.04, standard error=1.8%) The regression analysis of the voltage response of CdS on the X-ray exposure time variation was y=8.2853+5.5878 ($R^2$=0.7287, $\sigma$=0.06, standard error=1.9%). In conclusion, cadmium sulfide responded linearly to the variation X-ray conditions, suggesting cadmium sulfide to be a feasible X-ray sensor of multi-function dosimeter related instruments.

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A Study on Three Dimensional Coordinates Analysis Using x-Ray (X-Ray 를 이용한 삼차원(三次元) 좌표해석(座標解析)에 관한 연구(硏究))

  • Yeu, Bock Mo;Park, Joon Kyu;Kim, In Sop
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.7 no.2
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    • pp.89-98
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    • 1987
  • X-Ray photogrammetry is the method that register and analize the anatomical or physiological information about the human body by the photography form. In this paper, using X-Ray, accuracy of three dimensional coordinates of objects which are deformed and a part of human body is analyzed. An objective of this analysis lies in improving the accuracy of three dimensional coordinates and enhancing the practical use. Through the observation, X-Ray Photogrammetry is used in practical use. And X-Ray photograph is used the reform of graphical model by the determination of the three dimensional coordinates about all sides of object.

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The Correlations between Mineralogy and Engineering Characteristics of Soft Clay in Sihwa Area (시화지구 연약점토의 광물학적 특성과 공학적 특성의 상관관계)

  • Kim Nak-Kyung;Park Jong-Sik;Joo Yong-Sun
    • Journal of the Korean Geotechnical Society
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    • v.20 no.9
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    • pp.155-166
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    • 2004
  • The characteristics of soft clays are very important for the land development plan. This study is to investigate correlations between the engineering properties and the characteristics of clay minerals of the undisturbed clay samples obtained from Sihwa area. This study included X-Ray diffraction analysis, X-Ray fluorescence spectrometer analysis, scanning electron microscopy analysis and energy dispersive X-Ray spectrometer analysis. The correlations between the clay mineral properties and the laboratory and field testing results were investigated. The characteristics of soft clay in Sihwa area were compared with those in Yangsan and Kunsan area.

Wireless Triggering Pulse Generation for Digital X-ray Imaging System (디지털 x-ray 영상시스템을 위한 무선 트리거 발생기)

  • Ko, Dae-Sik;Lee, Jae-Cheol;Lee, Joo-Shin
    • Journal of Advanced Navigation Technology
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    • v.11 no.2
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    • pp.163-169
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    • 2007
  • In this paper, we propose a method of trigger pulse generation to capture the image on time by making a synchronization between the x-ray generator and digital x-ray image acquisition system. we designed a wireless trigger pulse generation circuit to make a synchronization between x-ray generator and digital image acquisition system and analysis its performance. When it starts to detect a certain level of x-ray radiation or above from the air, this method starts to generate a ACQ_START signal to indicate the timing for image acquisition starting from digital image acquisition system. Hence, when it starts to detect under certain level of x-ray signal from the air, this method starts to generate a ACC_END signal to indicate the timing for image acquisition stop from digital image acquisition system. Image acquisition is activated only this time between ACQ_START and ACQ_END signal. By doing this wireless detecting of x-ray signal from remote, we can get more accurate timing for capturing the x-ray image and any type of x-ray generator can be connected to digital image acquisition system, regards of wired protocol. This makes easy installation. We could get 3.5 line pair / mm resolution at 20 mAs of x-ray level with resolution chart. This is same or better image comparing to conventional wired result.

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Modification of conventional X-ray diffractometer for the measurement of phase distribution in a narrow region

  • Park, Yang-Soon;Han, Sun-Ho;Kim, Jong-Goo;Jee, Kwang-Yong;Kim, Won-Ho
    • Analytical Science and Technology
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    • v.19 no.5
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    • pp.407-414
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    • 2006
  • An X-ray diffractometer for spatially resolved X-ray diffraction measurements was developed to identify phase in the narrow (micron-scaled) region of high burn-up fuels and some nuclear materials. The micro-XRD was composed of an X-ray microbeam alignment system and a sample micro translation system instead of a normal slit and a fixed sample stage in a commercial XRD. The X-ray microbeam alignment system was fabricated with a microbeam concentrator having two Ni deposited mirrors, a vertical positioner, and a tilt table for the generation of a concentrated microbeam. The sample micro translation system was made with a sample holder and a horizontal translator, allowing movement of a specimen at $5{\mu}m$ steps. The angular intensity profile of the microbeam generated through a concentrator was symmetric and not distorted. The size of the microbeam was $4,000{\times}20{\mu}m$ and the spatial resolution of the beam was $47{\mu}m$ at the sample position. When the diffraction peaks were measured for a $UO_2$ pellet specimen by this system, the reproducibility ($2{\Theta}={\pm}0.01^{\circ}$) of the peaks was as good as a conventional X-ray diffractometer. For the cross section of oxidized titanium metal, not only $TiO_2$ in an outer layer but also TiO near an oxide-metal interface was observed.

A Study on the Scatter X-ray Signal and Noise Characteristics of Indirect Conversion-Type Detector for Radiography (산란선이 간접변환방식 엑스선 검출기의 신호 및 노이즈 특성에 미치는 영향에 관한 연구)

  • Kim, Junwoo
    • Journal of the Korean Society of Radiology
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    • v.15 no.3
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    • pp.345-353
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    • 2021
  • Digital radiography imaging systems can also help diagnose lesions in patients, but if x-rays that enter the human body cause scatter x-ray due to interaction with substances, they affect the signal and noise characteristics of digital x-ray images. To regard the human body as polymethyl methacrylate (PMMA) and observe the properties of scattered x-ray generated from PMMA on x-ray images, we analyze signal and noise in the spatial domain as well as noise-power spectrum (NPS), and detective quantum efficiency (DQE) at zero frequency. As PMMA thickness increased, signals decreased, the noise increased, and NPS degradation was identified in overall spatial frequencies. Based on these characteristics, zero-frequency performance was also shown to be degraded. Comparative analysis with Monte-carlo simulations will need to be made to analyze the zero-frequency performance by scattered x-ray of indirect conversion-type x-ray detectors more quantitatively.

Simulation of amorphous selenium considering diffraction and interference models (간섭과 회절 모델을 고려한 비정질 셀레늄(a-Se) 시뮬레이션)

  • Kim, Si-hyung;Song, Kwang-soup
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2012.10a
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    • pp.997-999
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    • 2012
  • Digital X-ray image detector is widely used for radiodiagnosis. Amorphous selenium has been received attention as one of the major material that confirmed photoconductor of direct methode detector. We analysis the photocurrent using 2-dimensional device simulator when blue-ray (${\lambda}=486nm$) is irradiated and high voltage is biased. We evaluate electron-hole generation rate, electron-hole recombination rate, and electron/hole distribution in the amorphous selenium. This simulation methode is helpful to the analysis of digital X-ray image detector. We expect that many applications will be developed in digital X-ray image detector using 2-dimensional device simulator.

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The analytical application for cement using X-Ray diffraction and X-Ray fluorescence spectrometer (X-Ray Diffraction과 X-Ray Fluorescence를 이용한 시멘트 비교 분석)

  • Jung, Ji Eun;Jang, Yu Rim;Kim, Ki-Wook;Heo, Sangcheol;Min, Ji-Sook
    • Analytical Science and Technology
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    • v.26 no.5
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    • pp.340-351
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    • 2013
  • The chemical element and structural characterization of different types of cements and its brick stones are been investigated under forensic aspects using X-ray florescence (XRF) and X-ray diffraction (XRD) spectrometer. The XRF provides rapid compositional data for controlling almost all stages of raw materials, clinker and cement. The decisive advantage of XRD methods is based on the unique character of the diffraction patterns of crystalline substances, the ability to distinguish between elements and their oxides, and the possibility to identify chemical compounds, polymeric forms, and mixed crystals by non-destructive examination. Therefore, combination of these examinations is useful and able to apply for the forensic analysis in comparison of cements and brick stones. There are more study remained to determine the viability of method for forensic analysis of brick stones and the limits of the discrimination that can be achieved.