• Title/Summary/Keyword: Wet surface

Search Result 1,210, Processing Time 0.037 seconds

THE EFFECT OF MOISTENING OF ETCHED DENTIN AND ENAMEL SURFACE ON THE MICROLEAKAGE OF COMPOSITE RESINS (복합레진 수복시 상아질 표면 처리가 미세 변연 누출에 미치는 영향에 관한 연구)

  • Jeon, Cheol-Min;Kwon, Hyuk-Choon;Lee, Chung-Sik;Lee, Myung-Jon;Um, Chung-Moon
    • Restorative Dentistry and Endodontics
    • /
    • v.21 no.1
    • /
    • pp.321-338
    • /
    • 1996
  • The purpose of this study was to evaluate the effect of moistening and air-drying of acid conditioned dentin and enamel on the marginal microleakage. In this study, Class V cavity were prepared on both buccal and lingual surface of sixty extracted human premolars with cementum margin. These specimens were randomly devided into three groups and three dentin adhesives(Scotchbond Multi-Purpose, All bond 2, Prisma Universal Bond 3) were applied to each group. The specimens in each group were subdevided into four groups (Wet/primed, Dry/primed, Wet/not primed, Dry/not primed) and the etched dentin and enamel surface were treated these four surface treatments prior to the placement of a bonding agent or adhesive. Wet/primed group was simply blot-dried with a damp facial tissue before primer placement ; Dry/primed group was air dried for 30 seconds before the placement of a primer ; Wet/not primed group and Dry/not primed group were not primed after blot dried and air dried for 30 seconds each group. The bonding agent and composite resin were applied for each group. All specimens were exposed to 500 cycle of thermal stress. Specimens were placed in a silver nitrate solution and then sectioned buccolingually through the center of the restoration. The dye penetrations of the specimens were observed with a stereo microscope. The statistical test were applied to the results using a one way analysis variance (ANOVA) and Duncan's multiple range test. The aspects of silver ion penetration into the resin/dentin interface were examined under scanning electron microscopy. The results were as follows. 1. In all groups, the enamel margin showed significantly lower leakage value than the cementum margin (p<0.05). 2. Regardless of various surface treatment and dentin adhesives, there was no significant difference at the enamel margins (p>0.05). 3. At the dentin margins, the leakage values of Dry/not primed group showed significantly higher than that of the other groups (p<0.05). The leakage values of Wet/primed group showed significantly lower than that of the other groups, but, there was no significant difference between Wet group and Dry group. 4. There was no significantly difference between the dentin adhesives regarding the surface treatments in all groups(p>0.05). 5. On the backscatterd scanning electron microscopy observation, the penetration of the silver ion occured at the bonding resin/dentin interface. In the Wet/primed group, resindentin hybrid zone and resin penetration into the dentin was observed. The resin tags were compactively formed to a thickness of $3\sim4{\mu}m$ at the upper part of dentinal tubules. In the Dry/primed group, the thickness of the hybrid zone and the diameter, depth of the resin tags diminished. In the Non-primed groups, the hybrid zone was not identified and few resin tag was observed. There was the gap formation in the resin/dentin interface.

  • PDF

EFFECTS OF DENTIN SURFACE WETNESS OR DESICCATION AFTER ACID ETCHING ON DENTIN BONDING (산부식후 상아질 표면의 습윤 또는 건조가 상아질 결합에 미치는 영향)

  • Yang, Won-Kyung;Kwon, Hyuk-Choon;Son, Ho-Hyun
    • Restorative Dentistry and Endodontics
    • /
    • v.25 no.2
    • /
    • pp.243-253
    • /
    • 2000
  • The purpose of this in vitro study was to evaluate dentin bonding by two different dentin bonding systems(DBS) using acetone based primer or adhesive [All Bond 2(AB2), One Step(OS)] when they were applied by wet or dry bonding technique. Morphology of resin-dentin interface and hybrid layer thickness(HLT) were investigated using Confocal Laser Scanning Microscope(CLSM) and compared to shear bond strength(SBS). 72 extracted sound human molars were randomly divided into 4 groups of 18 teeth each - Group 1.(AW); AB2 by wet bonding. Group 2(AD); AB2 by dry bonding. Group 3.(OW); OS by wet bonding, Group 4.(OD); OS by dry bonding. In 6 teeth of each group, notch-shaped class V cavities(depth 2mm) were prepared on buccal and lingual surface at the cementoenamel juction(12 cavities per group). To obtain color contrast in CLSM observation, bonding resins of each DBS were mixed with rhodamine B and primer of AB2 was mixed with sodium fluorescein. Prepared teeth of each group were treated with AB2, OS, respectively according to the manufacturer's instructions except for dentin surface moisture treatment after acid etching. In group 1 and 3, after acid etching, excess water was removed with wet tissue(Kimwipes), leaving consistently shiny, visibly hydrated dentin surface. In group 2 and 4, dentin surface was dried for 10 seconds at 1 inch distance. The treated teeth were then packed with composite resin(${\AE}$litefil) and light-cured. 12 microscopic samples($60{\sim}80{\mu}m$ thickness) of each group were obtained after longitudinal section and grinding(Exakt cutting and grinding system). Morphological investigation of resin-dentin interface and HLT measurement using CLSM were done. For measurement of SBS, remaining 12 teeth of each group were flattened occlusally to remove all enamel and grinded to 500 grit SiC(Pedemet Specimen Preparation Equipment). After applying DBS on the exposed dentin surface, composite resin was applied in the shape of cylinder, which has 5mm diameter, 1.5mm thickness, and light cured. SBS was measured using Instron with a crosshead speed of 0.5mm/min. It was concluded as follows, 1. HLT of AW(mean: $2.59{\mu}m$) was thicker than any other group, and followed by AD, OW, OD in descending order(mean; 2.37, 2.28, $1.92{\mu}m$). Only OD had statistically significant differences(p<0.05) to AW and AD. 2. There were intimate contact of resin and dentin at the interface in wet bonding groups, but gaps or irregular interfaces were observed in dry bonding groups. 3. The length, diameter, density of resin tags were various even in the same group without significant differences between groups and lots of adhesive lateral branches were observed. 4. There were no statistically significant difference of SBS between AB2 and OS, but SBS of wet bonding groups were significantly higher(p<0.05) than dry bonding groups. 5. There were no consistent relationships between HLT and SBS.

  • PDF

Alginic acid-silica hydrogel coatings for the protection of ssmotic distillation membranes against wet-out by surface-active agents

  • Xu, J.B.;Spittler, D.A.;Bartley, J.P.;Johnson, R.A.
    • Proceedings of the Polymer Society of Korea Conference
    • /
    • 2006.10a
    • /
    • pp.354-354
    • /
    • 2006
  • Alginic acid-silica hydrogel films was prepared for testing as protective coating materials for PTFE OD membranes. Unprotected hydrophobic membranes are subject to wet-out when contacted by surface-active agents. Films were characterised using SEM, XRD, DSC, mechanical strength measurements, and water-swelling measurements. In OD trials using coated membranes, no wet-out occurred over the 15 h duration of three consecutive 5 h OD trials using orange oil-water mixtures. In the case of detergent solutions, the coating afforded protection to the membrane for 4-5 h. In a separate trial, no wet-out occurred when the coated side of the membrane was placed in contact with 1.2 wt % orange oil for 72 hours.

  • PDF

An Experimental Study of Tire-Road Friction Coefficient by Transient Brake Time (실차 실험을 통한 제동순시간에 의한 타이어-노면마찰계수에 관한 연구)

  • Han, Chang-Pyoung;Park, Kyoung-Suk;Choi, Myung-Jin;Lee, Jong-Sang;Shin, Un-Gyu
    • Journal of the Korean Society for Precision Engineering
    • /
    • v.24 no.7 s.196
    • /
    • pp.106-111
    • /
    • 2007
  • In this paper, the transient brake time was studied on the van type vehicle with accelerometer. Experiments were carried out on the asphalt(new and polished), unpacked road(earth and gravel) and on wet or dry road conditions. The transient brake time is not effected bzy the vehicle speed. The transient brake time is about 0.41$\sim$0.43second on the asphalt road surface and the error range is within 0.1$\sim$0.16second. For the asphalt road condition, the transient brake time is not effected by both new asphalt road surface and the polished asphalt road surface. With compared by dry and wet road surface condition, the transient brake time of wet condition is longer than dry road condition and compared with unpacked road condition and packed road condition, unpacked road condition is shorter than packed road condition. It is considered that the transient brake time is effected by the road surface fraction coefficient. In other words, the transients brake time increases as friction coefficient decreases.

A Comparative Study on the Influence of Etchant upon the Etching Rate and Quality in Laser Induced Wet Etching of Fused Silica (식각액에 따른 용융실리카의 레이저 습식 식각 특성 비교 연구)

  • 이종호;이종길;전병희
    • Transactions of Materials Processing
    • /
    • v.13 no.3
    • /
    • pp.268-272
    • /
    • 2004
  • Transparent materials such as fused silica are widely utilized in optical and optoelectronics field because of its outstanding properties, such as transparency in a wide wavelength range, strong damage resistance for laser irradiation, and high thermal and chemical stability. In this study, we made a few micro patterns on the surface of fused silica plate using laser induced wet etching. KrF excimer laser was used as a light source. There were no burrs and micro cracks on the etched surface of fused silica and the flatness of the etched surface was fairly good. We investigated the influence of etchant upon the etch rate and quality in laser induced wet etching. Pyrene-acetone solution and toluene were used as etchant. In the side of etch rate, toluene solution was better than pyrene-acetone solution. But we made in wider range of energy density using pyrene-acetone solution. But pyrene-acetone solution gave us wider window of energy density for successful micro patterning.

The Study on the Safety Adhesion Test of Wet Surface for Waterproofing and Anti Corrosion Materials of Water Supply Facility (수처리 시설물에 적용되는 방수·방식재의 습윤면 부착 안정 성능평가방법에 대한 연구)

  • Choi, Su-Young;Kim, Dong-Bum;Park, Jin-Sang;Park, Wan-Goo;Kim, Byoung-Il;Oh, Sang-Keun
    • Proceedings of the Korean Institute of Building Construction Conference
    • /
    • 2017.05a
    • /
    • pp.137-138
    • /
    • 2017
  • The Waterproofing and Anti corrosion materials applied to the water supply facility did not consider environment of water supply facility, thus defects occurred consistently on the site. In this study, it suggests safety adhesion test of wet surface and have a test for safety adhesion performance.

  • PDF

Optimizing Oily Wastewater Treatment Via Wet Peroxide Oxidation Using Response Surface Methodology

  • Shi, Jianzhong;Wang, Xiuqing;Wang, Xiaoyin
    • Journal of the Korean Chemical Society
    • /
    • v.58 no.1
    • /
    • pp.80-84
    • /
    • 2014
  • The process of petroleum involves in a large amount of oily wastewater that contains high levels of chemical oxygen demand (COD) and toxic compounds. So they must be treated before their discharge into the receptor medium. In this paper, wet peroxide oxidation (WPO) was adopted to treat the oily wastewater. Central composite design, an experimental design for response surface methodology (RSM), was used to create a set of 31 experimental runs needed for optimizing of the operating conditions. Quadratic regression models with estimated coefficients were developed to describe the COD removals. The experimental results show that WPO could effectively reduce COD by 96.8% at the optimum conditions of temperature $290^{\circ}C$, $H_2O_2$ excess (HE) 0.8, the initial concentration of oily wastewater 3855 mg/L and reaction time 9 min. RSM could be effectively adopted to optimize the operating multifactors in complex WPO process.

A Study on the Surface Roughness in Grinding Process by Frequency Analysis (평면연삭(平面硏削)에서 주파수(周波數) 분석(分析)에 의한 표면(表面) 거칠기 해석(解釋))

  • Kim, G.N.;Cheong, C.C.;Kim, K.S.
    • Journal of the Korean Society for Nondestructive Testing
    • /
    • v.11 no.2
    • /
    • pp.32-41
    • /
    • 1991
  • This paper is to analyze the surface roughness in wet and dry surface grinding in which working conditions are table feed, cross feed and down feed. FFT analyzer is used to identify the surface roughness and the data of surface roughness are stored and displayed using an interfaced computer. In results, components affecting surface roughness exist within 200Hz with respect the conditions and methods of grinding operation. Also, with increase of table feed, cross feed and down feed, the value of surface roughness increases. Of them, cross feed has first influence on surface roughness. In dry, preciser surface can be obtained than one in wet.

  • PDF

The effect of the surface activation treatment on the crystallization of amorphous silicon thin film (표면 활성화 처리가 비정질 규소 박막의 결정화에 미치는 영향)

  • 이의석;김영관
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.9 no.2
    • /
    • pp.173-179
    • /
    • 1999
  • The effect of the surface activation treatment on the crystallization of the amorphous silicon film was investigated. The amorphous silicon film was deposited on the silica substrate with LPCVD technique. Wet blasting with silica slurry or exposure with Nd:YAG laser beam was applied on the amorphous silicon film before annealing for the crystallization. For the analysis of the crystallinity, XRD, Raman, and SEM were employed. In this investigation, the prior surface activation treatment like silica wet blasting or Nd:YAG laser beam exposure before annealing for the crystallization were found to be effective in the enhancement of the crystallization. It is believed that these treatment lower the activation energy required for the crystallization of the amorphous silicon film.

  • PDF

Effects of Ditching on Seedling Stand in Wet Direct Seeding Rice Culture

  • Back, Nam-Hyun;Kang, Si-Yong;Kim, Sang-Su;Kwon, Tae-Oh
    • KOREAN JOURNAL OF CROP SCIENCE
    • /
    • v.46 no.1
    • /
    • pp.47-52
    • /
    • 2001
  • In order to develop more stable seedling stand method in wet direct rice seeding culture, the effect of making the drainage ditches was studied in both methods of broadcast seeding on floody paddy surface and puddled-soil drill seeding. In a broadcast seeding on floody paddy surface, the ditching after seeding using a tractor or small ditch maker improved the seedling stand, and reduced the floating seedling and herbicide injury by accelerating the drainage. Suitable ditching time was at 2 days after seeding (DAS) for the tractor and at 3 DAS for the ditch maker. In the puddled-soil drill rice seeding culture, the ditching before seeding with a ditch maker at 3 days after draining effectively improved the seedling stand due to quick draining through well formed the seeding furrows. In the puddled-soil drill seeding, seedling stand number showed higher in both ditching plots synchronized with seeding compared with both only draining treatment at 1 DAS without ditching and the flooding plot condition for 6 DAS. And the suitable ditching depth was 6 cm, as considered the ditching status and drained status. These results suggest that the ditching in wet direct rice seeding is an resonable practice for improving the seedling stand through the accelerating drainage of field.

  • PDF