• 한국식품과학회지
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• 제16권3호
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• pp.303-308
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• 1984

물성적(物性的) 특성(待性)을 다르게 제조한 츄잉검을 가지고 Rheometer를 사용하여 저작단계별로 초기(初期)에 puncture test, 중기(中期)에 penetration test, 후기(後期)에 penetration test 및 compression test를 하여 기계적(機械約) 물성(物性)을 측정 하였고 같은 시료로 훈련(訓練)된 파넬과 소비자(消費者) 관능검사를 실시하여 관능적(官能的) 물성(物性) 및 기호성(嗜好性)을 측정하였다. 이들 측정 된 물성값으로 기계적(機械約) 물성간(物性間)의 상관관계와 관능적(官能的) 물성간(物性間)의 상관관계를 구하여 물성간(物性間)의 유사성(類似性)과 상관성을 조사하였다. 기계적(機械的) 물성(物性)에서 초기(初期)의 puncture work와 puncture force, 중기(中期)의 hardness와 work, 후기(後期)의 hardness와 work 및 adhesion work와 adhesion force는 각각 유사(類似)한 물성(物性)으로 해석되었으며 후기(後期)의 yield force와 slope는 hardness와, springiness와 adhesion force는 slope와 상관관계가 높았다. 관능적(官能的) 물성(物性)에서 소비자(消費者)와 훈련(訓練)된 파넬의 관능검사 결과(結果)는 거의 일치(一致)하였고 소비자의 경우 초기(初期)의 stiffness가 중기(中期), 후기(後期)의 firmness와 상관관계가 높았다. 훈련(訓練)된 파넬의 경우 후기(後期)의 stiffness는firmness와, cohesion은 lift와 각각 유사(類似)한 물성(物性)으로 해석되었으며 adhesion은 firmness와 부(負)의 상관관계를 나타내었다.

• The Korean Journal of Ceramics
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• 제3권2호
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• pp.73-81
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• 1997

In this paper, it is intended to present more reproducible and quantitative method for adhesion assemssement. In scratch test, micromechanical analysis on the stress state beneath the indenter was carried out considering the additional blister field. The interface adhesion was quantified as work of adhesion through Griffith energy approach on the basis of the analyzed stress state. The work of adhesion for DLC film/WC-Co substrate calculated through the proposed analysis shows the identical value regardless of distinctly different critical loads measured with the change of film thickness and scratching speed. On the other hand, uniaxial loading was imposed on DCL film/Al substrate, developing the transverse film cracks perpendicular to loading direction. Since this film cracking behavior depends on the relative magnitude of adhesion strength to film fracture strength, the quantification of adhesion strength was given a trial through the micromechanical analysis of adhesion-dependence of film cracking patterns. The interface shear strength can be quantified from the measurement of strain $\varepsilon$s and crack spacing $\lambda$ at the cessation of film cracking.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2007년도 춘계학술대회A
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• pp.1744-1748
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• 2007

In this study, the Johnson-Kendall-Roberts (JKR) theory was combined with the instrumented indentation technique (IIT) to evaluate work of adhesion and modulus of elastomeric polymer. Indentation test was used to obtain the load-displacement data for contacts between Tungsten Carbide indenter and elastomeric polymer. And the JKR contact model, contrived to take viscoelastic effects of polymer into account, was applied to compensate the contact area and the elastic modulus which Hertzian contact model would underestimate and overestimate, respectively. Besides, we could obtain the thermodynamic work of adhesion by considering the surface energy in this contact model. In order to define the relation between JKR contact area and applied load without optical measuring of contact area, we used the relation between applied load and contact stiffness by examining the correlation between JKR contact area and stiffness through dimensional analysis with 14 kinds of elastomeric polymer. From this work, it could be demonstrated that the interfacial work of adhesion and elastic modulus of compliant polymer can be obtained from a simple instrumented indentation testing without area measurement, and provided as the main algorithm of compliant polymer characterization.

• 한국표면공학회지
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• 제36권4호
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• pp.347-355
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• 2003

Roughening of metal surfaces frequently enhances the adhesion strength of metals to polymers by mechanical interlocking. When a failure occurs at a roughened metal/polymer interface, the failure prone to be cohesive. In a previous work, an adhesion study on a roughened metal (oxidized copper-based leadframe)/polymer (Epoxy Molding Compound, EMC) interface was carried out, and the correlation between adhesion strength and failure path was investigated. In the present work, an attempt to interpret the failure path was made under the assumption that microvoids are formed in the EMC as well as near the roots of the CuO needles during compression-molding process. A simple adhesion model developed from the theory of fiber reinforcement of composite materials was introduced to explain the adhesion behavior of the oxidized copper-based leadframe/EMC interface and failure path. It is believed that this adhesion model can be used to explain the adhesion behavior of other similarly roughened metal/polymer interfaces.

• 접착 및 계면
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• 제5권3호
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• pp.18-22
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• 2004

본 실험에서는 Johnson-Kendall-Roberts (JKR) 기법을 이용하여 고체물질의 표면에너지 및 두 물질 사이의 고유접착에너지를 측정하였다. JKR 기법의 원리는 기본적으로 접촉역학(contact mechanics)에 기본을 두고 있으며 이를 통하여 기존의 접촉각 측정 방식을 통한 고체 표면에너지 측정 및 peel test와 같은 고전적인 방법을 통한 접착에너지의 측정에서의 한계점을 극복할 수 있는 새로운 방법으로 받아들여지고 있다. 본 연구에서는 polydimethylsiloxane (PDMS)를 이용하여 표면에너지를 측정함으로써 JKR 기법을 통한 측정 결과와 이의 응용가능성에 대해 알아보고자 하였다.

• Tribology and Lubricants
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• 제18권4호
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• pp.267-272
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• 2002

Nano adhesion between SPM(scanning probe microscope) tips and DDPO$_4$(octadecylphosphoric acid ester.) and ODPO$_4$(octadecylphosphoric acid ester) SAM(self-assembled monolayer.) was experimentally studied. Tests were performed to measure the nano adhesion and friction in both AFM(atomic force microscope) and LFM(lateral force microscope) modes with the applied normal load. DDPO$_4$ and ODPO$_4$ SAM were formed on Ti and TiOx surfaces. Ti and TiOx were coated on the Si wafer by ion sputtering. Adhesion and friction of DDPO$_4$ and ODPO$_4$ SAM surfaces were compared with those of OTS(octadecyltrichlorosilane) SAM and DLC surfaces. DDPO$_4$ and ODPO$_4$ SAM converted the Ti and TiOx surfaces to be hydrophobic. When the surface was hydrophobic, the adhesion and friction forces were found lower than those of bare surfaces. Work of adhesion was also discussed to explain how the surface was converted into hydrophobic Results also showed that tribological characteristics of DDPO$_4$ and ODPO$_4$ SAM had good properties in the adhesion, friction, wetting angle and work of adhesion. DDPO$_4$ and ODPO$_4$ SAM could be one of the candidates for the bio-MEMS elements.

• Tribology and Lubricants
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• 제13권2호
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• pp.68-73
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• 1997

The adhesion between wheel and rail plays an important role in the braking performance of trains. Though there have been numerous studies on the characteristics of adhesion phenomenon, a general understanding from the physical point of view is still lacking. In this work, the adhesion mechanism between wheel and rail was investigated by studying the mechanisms of pure rolling and sliding experiments. Tests were performed under various conditions to determine the physical phenomenon responsible for adhesion between wheel and rail. The results of this study is expected to aid in improving the braking performance of trains.

• 폴리머
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• 제25권3호
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• pp.435-440
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• 2001

본 연구에서는 일방향 탄소/탄소 복합재료에 산화억제제로 사용된 $MoSi_2$의 첨가량에 따른 복합재료의 부착력, 파괴인성 그리고 충격강도와의 관계를 고찰하였다. 산화억제제로 사용한 이규화 몰리브덴 (MoSi$_2$)은 복합재료의 내산화 특성을 향상시키기 위하여 각각 4, 12, 20wt%의 중량비로 페놀수지에 함침시켰다. 본 연구에 있어서 복합재료의 부착력은 접촉각 측정에 의한 Wilhelmy 방정식을 사용하여 계산하였다. 파괴인성과 충격강도는 임계 세기인자 측정을 위한 3점 굴곡 시험 방법과 Izod 충격시험에 의해 각각 측정하였다. 그 결과, $MoSi_2$가 첨가된 탄소/탄소 복합재료의 파괴인성과 충격강도는 증가하였다. 특허 l2wt%의 $MoSi_2$가 첨가된 복합재료가 London dispersive 요소($W_A\;^L$)의 증가에 의한 가장 큰 부착력을 나타내었으며, 이는 복합재료의 각 구성요소간의 계면결합력 증가에 따른 결과라 사료된다.

• 대한기계학회논문집A
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• 제31권9호
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• pp.951-959
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• 2007

In this study, the Johnson-Kendall-Roberts(JKR) theory was combined with the instrumented indentation technique (IIT) to evaluate work of adhesion and modulus of elastomeric polymer. Indentation test was used to obtain the load-displacement data for contacts between Tungsten Carbide indenter and elastomeric polymer. And the JKR contact model, contrived to take viscoelastic effects of polymer into account, was applied to compensate the contact area and the elastic modulus which Hertzian contact model would underestimate and overestimate, respectively. Besides, we could obtain the thermodynamic work of adhesion by considering the surface energy in this contact model. In order to define the relation between JKR contact area and applied load without optical measuring of contact area, we used the relation between applied load and contact stiffness by examining the correlation between JKR contact area and stiffness through dimensional analysis with 14 kinds of elastomeric polymer. From this work, it could be demonstrated that the interfacial work of adhesion and elastic modulus of compliant polymer can be obtained from a simple instrumented indentation testing without area measurement, and provided as the main algorithm of compliant polymer characterization.

• 접착 및 계면
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• 제21권1호
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• pp.27-33
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• 2020

유리섬유강화 복합재료 (GFRC)의 표면거칠기에 따른 에폭시 접착제의 접착강도를 평가하였고 최적의 표면거칠기를 선정하였다. 서로 다른 입자크기의 알루미나 (Al2O3) 입자를 GFRC의 표면에 분사하였고 이를 통하여 서로 다른 표면거칠기를 부여하였다. 표면거칠기를 정량화 하였고 표면거칠기에 따른 표면관찰을 진행하였다. 각 표면거칠기에 따른 접촉각을 측정하였고 이를 통하여 표면에너지를 계산하였으며, 에폭시 접착제와의 접착일을 계산 및 비교하여 접착력을 예측하였다. 단일랩전단 시험을 통해 접착강도를 평가하였고 거칠기에 따라 접착강도가 증가된다는 것을 확인하였다. 박리 후 표면을 관찰해 보았을 때 기지재인 GFRC의 박리 정도가 다른 것을 확인하였고 최종적으로 표면거칠기의 최적조건을 확인할 수 있었다.