• 제목/요약/키워드: W Substituted

검색결과 151건 처리시간 0.025초

Synthesis and Evaluation of the Analgesic and Antiinflammatory Activities of O-Substituted Salicylamides

  • Fahmy, H.H.;El-Eraky, W.
    • Archives of Pharmacal Research
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    • 제24권3호
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    • pp.171-179
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    • 2001
  • The present investigation deals with the synthesis of some new salicylamidoacetyl sulfonamides 3a,b, salicylamido ethylacetate 4, salicylamido acetic acid hydrazide 5, which is considered as the key intermediate for the synthesis of several series of new compounds such as salicylamido pyrazol 6 and pyrazolone 1. N-imido-derivatives 9, 10, 11, thiadiazole 13, oxadiazole 14, 15, Schiffs bases 16a-f. Cyclocondensation of Schiffs bases with thioglycolic acid gave thiazolidinone 18a-c while with acetylchloride afforded azitidinones 19a-c and with acetic anhydride gave 1,4-benzoxazepine-3,5-dione. Some of the compounds were tested for their analgesic and antiinflammatory activities as well as ulcerogenic effects. Some derivatives were more effective than salicylamide and ulcerogenic activity was variably lowered .

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실리카겔을 활용한 흡착 경화체의 열전도율 특성 (Thermal Conductivity Properties of Adsorption Matrix According to Silica Gel)

  • 권오한;임현웅;이동훈;이상수
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2017년도 추계 학술논문 발표대회
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    • pp.109-110
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    • 2017
  • In recent years, it has been urgently required to develop and study a product that adsorbs and reduces lardon gas due to the risk of lardon gas in Korea. Therefore, this study develops a board for adsorbing lardon gas into the inside and outside of the room. The thermal conductivity was measured in order to carry out an adiabatic test for satisfying the following conditions. Experimental level and factors were substituted with silica gel. In addition, silica gel was used by dry mixing and prewetting, and 10, 20, and 30% of cement was substituted for each. As a result of the test, the thermal conductivity decreased to 0.45 W/mK with increasing the amount of replacement, and reached a similar level when compared with diatomite.

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Synthesis and Properties of Thermotropic Compounds with Two Terminal Mesogenic Units and a Central Spacer (Ⅱ). Homologous Series of $\alpha,\;\omega$-Bis (4-p-substituted phenoxycarbonyl)phenoxyalkanes

  • Jin, Jung-Il;Chung, Yong-Seog;Lenz, R.W.;Ober, C.
    • Bulletin of the Korean Chemical Society
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    • 제4권3호
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    • pp.143-148
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    • 1983
  • Two series of thermotropic compounds were prepared and their thermal and liquid crystal properties were examined by differential scanning calorimetry and on the hot-stage of a cross-polarizing microscope. The first series of the compounds has two terminal mesogenic units based on unsubstituted and substituted p-(phenoxycarbonyl) phenyl ethers bracketing a central decamethylene spacer, and the second has 4-(p-phenylphenoxycarbonyl) phenyl ether moiety as the two terminal mesogenic units and central polymethylene spacers of varying lengths. A thermodynamic analysis of the phase transitions was made and explained in relation to structures and thermotropic behavior of the compounds.

1kW급 수소리니어 발전기 열해석 (A Thermal Analysis of 1 kW Hydrogen Linear Generator)

  • 양시원;이재성;권기영
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2006년도 춘계학술대회
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    • pp.29-32
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    • 2006
  • Recently, many researches of the alternative and renewable energy have introduced due to the increasing oil price, the limited natural resources and the environmental pollution. In case of hydrogen energy, it has some merits, which can be substituted the existing the fossil fuel because of no contaminants from the combustion and the chemical reaction. We have been developing 1kW Hydrogen Linear Generator. In this paper, the thermal characteristic of this prototype linear generator has been investigated and obtained reliable analysis results comparing with experimental measurements. Especially, it is predicted that in case of 1kW, 60Hz test sample, the results satisfy with the temperature standards of H type insulation, which is shown average $69.0^{\circ}C$ temperature distribution at the coil.

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Microwave Sintering of FLY Ash Substituted Body and Numerical Analysis

  • Kim, S. B.;J. W. Han;Kim, Y.
    • 한국결정성장학회:학술대회논문집
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    • 한국결정성장학회 1998년도 PROCEEDINGS OF THE 14TH KACG TECHNICAL MEETING AND THE 5TH KOREA-JAPAN EMGS (ELECTRONIC MATERIALS GROWTH SYMPOSIUM)
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    • pp.75-76
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    • 1998
  • Fly ash 70wt% contained green bodies were sintered by using a 2.45 Ghz microwave oven and their properties were investigated. Samples were sintered at 1,150$^{\circ}C$ and kept at that temperature up 50 minutes by 10 minutes intervals. Numerical analysis on the microwave heated system was carried out in order to figure out the heat transfer phenomena in the cavity.

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H2S를 포함하는 연료를 사용하기 위한 고체산화물 연료전지용 Sr0.92Y0.08Ti1-xVxO3-δ 연료극 특성 (Characteristics of Sr0.92Y0.08Ti1-xVxO3-δ (x = 0.01, 0.04, 0.07, 0.12) Anode for Using H2S Containing Fuel in Solid Oxide Fuel Cells)

  • 장근영;김준호;모수인;박광선;윤정우
    • Korean Chemical Engineering Research
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    • 제59권4호
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    • pp.557-564
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    • 2021
  • 페로브스카이트 구조를 갖는 Sr0.92Y0.08Ti1-xVxO3-δ (SYTV)는 고체산화물 연료 전지(Solid oxide fuel cell, SOFC)에서 H2S를 포함하는 연료를 사용하기 위한 대체 연료극으로 연구되었다. Sr0.92Y0.08TiO3-δ (SYT)의 전기화학적 성능을 향상시키기 위해 페로브스카이트의 B-사이트에 위치한 티타늄을 바나듐으로 치환하였다. 페치니법을 통해 합성된 SYTV는 작동 온도 조건에서 추가적인 부산물의 형성 없이 YSZ(yttria-stabilized zirconia) 전해질과 화학적으로 안정했다. 바나듐의 치환량이 증가함에 따라 산소 공공 결함(Oxygen vacancy)이 증가하였으며, 생성된 산소 공공 결함으로 인해 연료극의 이온 전도도가 증가했다. 전지 성능은 850 ℃ 순수한 H2 연료 조건에서 바나듐 치환 정도에 따라 1 mol.%의 바나듐이 치환된 경우 19.30 mW/cm2 이고 7 mol.%의 바나듐이 치환된 경우 34.87 mW/cm2이다. 1000 ppm의 H2S를 포함하는 H2 연료조건에서 cell의 최대 전력밀도는 1 mol.%의 경우 22.34 mW/cm2이고 7 mol.%의 경우 73.11 mW/cm2로 증가하였다.