• 한국수소및신에너지학회논문집
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• 제33권1호
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• pp.67-76
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• 2022

We developed a technology that can measure the hydrogen uptake and diffusivity of rubber materials by using the volumetric analysis method and diffusivity analysis program through the measurement of the water level in the graduated cylinder. In this method, hydrogen gas is charged at a certain pressure for a certain period of time for a rubber material exposed to a high-pressure hydrogen gas environment, and then the pressure is reduced to measure the change in the water level in the graduated cylinder in real time, and based on the measured value, it is a technology that can evaluate hydrogen uptake and diffusivity using diffusivity analysis program. Using this method, the hydrogen uptake and diffusivity of the NBR material were measured with respect to the change in the type and weight ratio of the filler used to improve the physical properties of the rubber material. In addition, uncertainty analysis was performed on the diffusivity measurement method.

• 대한토목학회논문집
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• 제30권4C호
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• pp.185-191
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• 2010

축전이기법을 사용하는 체적압력판추출기(이하 체적압력판)로 실내시험실에서 함수특성곡선을 구할 수 있다. 체적압력판을 사용하면, 매 단계마다 공기압을 차단하지 않고 시험하는 동안 흙시료로부터 추출되는 간극수의 부피를 연속적으로 측정할 수 있는 장점이 있다. 반면에, 시료내 간극수압을 일정하게 유지하기 위하여, 에어 트랩, 발라스트 튜브, 저장뷰렛, 진공펌프 등을 사용하는 체적압력판의 추출수 부피측정은 매우 복잡하고 지루한 작업을 수반한다. 이러한 문제점을 개선하고자 수정체적압력판을 개발하여 풍화잔류토에 대한 시험을 수행하였다. 수정 시험기는 매트릭석션의 범위에 따라 ASTM D 6836-02의 Method A와 Method B 두 방법 모두 사용하여 추출수의 부피를 측정할 수 있다. 본 논문에서는 수정 시험기의 측정원리, 개선점, 시험결과 및 토의를 서술하였다.

• Coupled systems mechanics
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• 제2권4호
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• pp.389-410
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• 2013

Three-dimensional Lagrangian fluid finite element is applied to seismic response analysis of an oil storage tank with a floating roof. The fluid element utilized in the present analysis is formulated based on the displacement finite element method considering only volumetric elasticity and its element stiffness matrix is derived by using one-point integration method in order to avoid volumetric locking. The method usually adds a rotational penalty stiffness to satisfy the irrotational condition for fluid motion and modifies element mass matrices through the projected mass method to suppress spurious hourglass-mode appeared in compensation for one-point integration. In the fluid element utilized in the present paper, a small hourglass stiffness is employed. The fluid and structure domains for the objective oil storage tank are modeled by eight-node solid elements and four-node shell elements, respectively, and the transient response of the floating roof structure or the free surface are evaluated by implicit direct time integration method. The results of seismic response analyses are compared with those by other method and the validation of the present analysis using three-dimensional Lagrangian fluid finite elements is shown.

• 한국수소및신에너지학회논문집
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• 제29권1호
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• pp.25-31
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• 2018

To apply Sievert's type apparatus to thermal analysis of hydrogen absorption materials, the dehydrogenation of $LaNi_5$ system was investigated. As the initial wt% of hydrogen was increased from 0.44 to 1.24 wt%, the peak temperature of evolution rate shifted to higher temperature. However, with the initial wt% of hydrogen higher than 0.95 wt%, the peak temperature of evolution rate did not change. As the heating rate was increased, the peak temperature increased; the peak temperatures for heating rates 0.5, 1.0 and 1.5 K/min were 262.2, 264.1, and 265.9 K respectively. The Sievert's type automatic apparatus can be successively applied to the thermal analysis of $LaNi_5$ hydride.

• Journal of international Conference on Electrical Machines and Systems
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• 제3권3호
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• pp.325-330
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• 2014

Eddy current induction is used in a wide range of electronic devices, for example in detection sensors. Due to the advances in computer hardware and software, the need for 3D computation and system comprehension is a requirement to develop and optimize such devices nowadays. Pure theoretical models are mostly limited to special cases. On the other hand, the classical use of commercial Finite Element (FE) electromagnetic 3D models is not computationally efficient and lacks modeling flexibility or robustness. The proposed approach focuses on: (1) implementing theoretical formulations in 3D (FE) model of a detection device as well as (2) an automatic Volumetric Estimation Method (VEM) developed to selectively model the target finite elements. Due to these two approaches, this model is suitable for parametric studies and optimization of the number, location, shape, and size of PCB receivers in order to get the desired target discrimination information preserving high accuracy with tenfold reduction in computation time compared to commercial FE software.

• 한국건축시공학회지
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• 제4권2호
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• pp.81-88
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• 2004

The purpose of this study is to investigate the chemical shrinkage and autogenous shrinkage of high strength cement paste and silica fume and fly ash and sand to cement ratio by the method of volumetric tests, and also investigate the autogenous shrinkage of high measurement method, and compare the results of volumetric test and linear length measurement test. A series of cement paste which have W/C ratio of 25%, 35%, 45% respectively were planed to study the effect of the W/C ratio to the shrinkages, and a series of cement paste which were replaced the cement by the silica fume and fly ash with 5%, 10%, 15% as the mass of cement respectively were planed to investigate the effects of poazolana to the shrinkages. A series of mortar which have a C/S ratio of 1:1, 1:1.5, 1:2 respectively were planed to investigate the shrinkage resistant effect of aggregate.

• 대한화학회지
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• 제7권2호
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• pp.186-188
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• 1963

An attempt to improve the method of volumetric determination of tungsten developed by Luke has been made successfully. Using amalgam coated lead instead of pure metallic lead in the reduction procedure. W(VI)-W(III) reduction has been found to be quantitative in rather concentrated hydrochloric acid. Since there was no excessive dissolution of lead via reduction of hydrogen ion, lead surface was totally accessible for the reduction of tungsten and no trouble was caused by dereposition of $PbCl_2$ crystals at the nozzle of Jones reductor. Furthermore, it has been confirmed that almost 100 mg. of $WO_3$ can be handled easily if the chloride concentration of the HCl is increased by adding solid $NH_4Cl$.

• 대한화학회지
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• 제8권3호
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• pp.109-112
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• 1964

A volumetric method of the determination of calcium carbonate and calcium fluoride in fluorspar concentrate is described. The carbonate is converted into solution by treatment of the sample in HNO$_3$-acetone (l% by volume) mixture, and the fluoride by treating the residue with H$_3BO_3$-HCl mixture. The calcium in the solution is determined volumetrically using EDTA standard solution. The selective dissolution of calcium carbonate by HNO$_3$-acetone mixture is superior to Bidtel's acetic method and little correction for the dissolution of calcium fluoride is needed. Triethanolamine is found to be superior to KCN in masking heavy metal ions.

• 지질공학
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• 제18권2호
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• pp.127-136
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• 2008

지반의 수분량 분포 및 강우에 의한 침윤선 거동과 지하수 수위 분포조사와 같이 광역지역을 대상으로 한 물리탐사기법인 지하투과 레이다탐사(ground penetrating radar, GPR) 및 전기비저항탐사(electrical resistivity survey)등을 이용해 광역조사가 이루어지며, 이에 반해 지반의 유전 반응(dielectric responses)을 이용한 유전율 측정법(permittivity method)은 협소한 지점에 대한 보다 정확한 지반의 물성 파악을 위해 다양한 연구분야에서 적용되어 왔다. 본 연구에서는 불포화 지반에 인공강우를 내려 침윤선의 침투거동을 파악하기 위하여 토층의 수분량 변화를 frequency domain reflectometry 시험법을 적용하여 측정하고, 간극수압과 간극 공기압의 변화는 간극수압계로 측정하였다. 이들 측정센서는 일정 깊이의 불포화 화강풍화토 공시체 몰드에 매설하고, 상단부에서부터 강우의 침투수 거동을 계측하여 물성치 변화로부터 수분분포 및 침윤선 분포특성을 평가하는 기법을 제안하였다. 지반 변형을 효율적으로 평가하기 위해 지반의 체적함수비, 간극수압 및 간극공기압의 측정 기술을 기존의 측정법과 비교해 신속하고 정량적으로 파악할 수 있는 측정방법에 대한 연구를 진행할 예정이다.

• 천문학회보
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• 제11권
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• pp.5.3-6
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• 1986